Abstract
Hydrated amorphous calcium pyrophosphate powder was synthesized from an aqueous solution containing pyrophosphoric acid and calcium acetate with the addition of an aqueous solution of ammonia. A distinctive feature of the proposed synthesis consisted in the use of pyrophosphoric acid synthesized by treatment of a sodium pyrophosphate solution with ion exchange resin (H+ form). The phase composition of ceramic fabricated from the powder after the calcination at 600–1000°C was represented by β-Ca2P2O7. The synthesized powder can be recommended for the fabrication of porous biocompatible resorbable ceramic.
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Original Russian Text © T.V. Safronova, S.A. Kurbatova, T.B. Shatalova, A.V. Knotko, P.V. Yevdokimov, V.I. Putlyayev, 2016, published in Materialovedenie, 2016, No. 7, pp. 41–48.
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Safronova, T.V., Kurbatova, S.A., Shatalova, T.B. et al. Calcium pyrophosphate powder for production of bioceramics synthesized from pyrophosphoric acid and calcium acetate. Inorg. Mater. Appl. Res. 8, 118–125 (2017). https://doi.org/10.1134/S2075113317010348
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DOI: https://doi.org/10.1134/S2075113317010348