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Use of vibration treatment in crystallization and drying of 5(6)-amino-2-(p-aminophenyl)benzimidazole

  • Organic Synthesis and Industrial Organic Chemistry
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Abstract

The purity, crystal structure, polymorphism, and nature of phase transitions of 5(6)-amino-2-(p-aminophenyl) benzimidazole recrystallized and dried under vibration treatment were studied by single crystal X-ray diffraction, thermal analysis, IR spectroscopy, mass spectrometry, and high-performance liquid chromatography.

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References

  1. Shchel’tsin, V.K., Varnikova, G.V., Makova, E.A., et al., Zh. Org. Khim., 1972, vol. 15, no. 9, pp. 1915–1926.

    Google Scholar 

  2. Tudorovskaya, G.L., Shtol’ts, N.V., Konovalova, T.P., et al., Zh. Prikl. Khim., 1984, vol. 57, no. 4, pp. 865–870.

    CAS  Google Scholar 

  3. Shapirovskaya, T.P., Shchel’tsin, V.K., Sychev, E.A., et al., Zh. Org. Khim., 1979, vol. 15, no. 1, pp. 112–117.

    CAS  Google Scholar 

  4. Tudorovskaya, G.L., Soldatova, T.A., Novozhilova, N.V., et al., Zh. Fiz. Khim., 1975, vol. 49, no. 11, pp. 3005–3006.

    CAS  Google Scholar 

  5. Kravchenko, V.G., Mil’kova, L.I., Shablygin, M.V., et al., Zh. Fiz. Khim., 1977, vol. 51, no. 10, pp. 2708–2711.

    CAS  Google Scholar 

  6. Chistovalov, S.M. and Chernov, A.N., Khim. Prom-st., 1994, no. 3, pp. 59–64.

  7. Chistovalov, S.M. and Chernov, A.N., Khim. Neft. Mashinostr., 1966, no. 3, pp. 35–36.

  8. Chistovalov, S.M. and Chernov, A.N., Khim. Prom-st., 1997, no. 8, pp. 31–35.

  9. RF Patent 2287354.

  10. RF Patent 2290245.

  11. Matusevich, L.N., Kristallizatsiya iz rastvorov v khimicheskoi promyshlennosti (Crystallization from Solutions in Chemical Industry), Moscow: Khimiya, 1968.

    Google Scholar 

  12. Nickus, Ip and Scilius, A., Nauchn. Tr. Vyssh. Uchebn. Zaved. Lit. SSR, Khim. Khim. Tekhnol., 1965, no. 4, pp. 107–110.

  13. Varsanof’ev, V.D. and Kol’man-Ivanov, E.E., Vibratsionnaya tekhnika v khimicheskoi promyshlennosti (Vibration Technique in Chemical Engineering), Moscow: Khimiya, 1985.

    Google Scholar 

  14. Skoog, D.A. and West, D.M., Fundamentals of Analytical Chemistry, New York: Holt, 1976, 3rd ed.

    Google Scholar 

  15. Ansheles, O.M., Tatarskii, V.B., and Shtenberg, A.A., Skorostnoe vyrashchivanie kristallov iz rastvorov (High-Rate Crystal Growth from Solutions), Leningrad: Lenizdat, 1945.

    Google Scholar 

  16. Nikitina, G.V., Romanenko, V.N., and Tuskevich, V.M., Kristallizatsiya i fazovye perekhody (Crystallization and Phase Transitions), Minsk: Akad. Navuk Bel. SSR, 1962, pp. 221–223.

    Google Scholar 

  17. Korovkina, E.K. and Komarova, T.A., Vestn. Mosk. Gos. Univ., Khim., 1965, no. 5, pp. 34–36.

  18. Kuptsov, A.Kh. and Zhizhin, G.N., Fur’e-KR i Fur’e-IK spektry polimerov (Fourier Raman and Fourier IR Spectra of Polymers), Moscow: Fizmatlit, 2001.

    Google Scholar 

  19. Water in Polymers: Based on a Symp. Cosponsored by the ACS Macromolecular Secretariat and the Division of Biological Chemistry at the 178th Meet. of the American Chemical Society, Washington, DC, September 10–13, 1979, Rowland, S.P., Ed., Washington, DC: Am. Chem. Soc., 1980.

    Google Scholar 

  20. Saunders, J.H. and Frish, K.C., Polyurethanes. Chemistry and Technology, part 1: Chemistry, New York: Interscience, 1962.

    Google Scholar 

  21. Andrianov, V.F., Leonova, V.V., Soldatova, T.A., et al., in Trudy VNIIPIM. Tula. Analiticheskii kontrol’ polucheniya monomera (Proc. All-Union Research and Designing Inst. of Monomers, Tula. Analytical Control of Monomer Production), Moscow: VNIITEKhIM, 1981, pp. 82–86.

    Google Scholar 

  22. Krischer, O., Die wissenschaftlichen Grundlagen der Trocknungstechnik, Berlin: Springer, 1956.

    Google Scholar 

  23. Wendlandt, W.Wm., Thermal Methods of Analysis, New York: Interscience, 1964. Translated under the title Termicheskie metody analiza, Moscow: Mir, 1978, pp. 261–265.

    Google Scholar 

  24. Spravochnik khimika (Chemist’s Handbook), Nikol’skii, B.P., Ed., Moscow: Khimiya, 1964, vol. 3.

    Google Scholar 

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Authors and Affiliations

  1. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow, Russia

    K. A. Kochetkov, S. M. Chistovalov, G. G. Ivanova & A. N. Tavtorkin

Authors
  1. K. A. Kochetkov
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  2. S. M. Chistovalov
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  3. G. G. Ivanova
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  4. A. N. Tavtorkin
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Additional information

Original Russian Text © K.A. Kochetkov, S.M. Chistovalov, G.G. Ivanova, A.N. Tavtorkin, 2009, published in Zhurnal Prikladnoi Khimii, 2009, Vol. 82, No. 12, pp. 2031–2037.

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Kochetkov, K.A., Chistovalov, S.M., Ivanova, G.G. et al. Use of vibration treatment in crystallization and drying of 5(6)-amino-2-(p-aminophenyl)benzimidazole. Russ J Appl Chem 82, 2174–2181 (2009). https://doi.org/10.1134/S1070427209120167

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  • DOI: https://doi.org/10.1134/S1070427209120167

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