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Synthesis and Properties of Some Sulfur-Containing Derivatives of Phosphorylated Sterically Hindered Phenols

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Abstract

The addition of thioacetic acid to 2,6-di-tert-butyl-4-(phosphorylmethylidene)cyclohexa-2,5-dien-1-ones has been accomplished for the first time. The resulting adduct is readily hydrolyzed with hydrazine hydrate to give 2,6-di-tert-butyl-4-[phosphoryl(sulfanyl)methyl]phenols, and the latter reacted with the initial quinomethanes, yielding 4,4′-[sulfanediylbis(phosphorylmethylene)]bis(2,6-di-tert-butylphenols).

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Authors and Affiliations

  1. Kazan National Research Technological University, ul. K. Marksa 68, Kazan, Tatarstan, 420015, Russia

    M. B. Gazizov, R. K. Ismagilov, A. L. Pistsova, N. S. Tikhonova, L. P. Shamsutdinova, R. N. Burangulova & R. F. Karimova

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  1. M. B. Gazizov
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  2. R. K. Ismagilov
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  3. A. L. Pistsova
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  4. N. S. Tikhonova
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  5. L. P. Shamsutdinova
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  6. R. N. Burangulova
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  7. R. F. Karimova
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Correspondence to M. B. Gazizov.

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Dedicated to B.I. Buzykin on the 80th Anniversary of His Birth

Original Russian Text © M.B. Gazizov, R.K. Ismagilov, A.L. Pistsova, N.S. Tikhonova, L.P. Shamsutdinova, R.N. Burangulova, R.F. Karimova, 2017, published in Zhurnal Obshchei Khimii, 2017, Vol. 87, No. 12, pp. 2080–2083.

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Gazizov, M.B., Ismagilov, R.K., Pistsova, A.L. et al. Synthesis and Properties of Some Sulfur-Containing Derivatives of Phosphorylated Sterically Hindered Phenols. Russ J Gen Chem 87, 2891–2894 (2017). https://doi.org/10.1134/S1070363217120246

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  • DOI: https://doi.org/10.1134/S1070363217120246

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