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Low-voltage scanning electron microscopy of multilayer polymer systems

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Abstract

The possibilities of low-voltage scanning electron microscopy for visualization of specific features of the microstructure in internal layers of multilayer polymer films are demonstrated by the example of “chitosan–polyelectrolyte complex–alginic acid” composite. The process of electron beam interaction with a sample at low electron energies is considered. The key parameters of low-voltage electron microscopy, which make it possible to increase the resolution of SEM images of polymer systems, are discussed.

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References

  1. V. Zworykin, J. Hillier, R. L. Snyder, et al., ASTM 117, 15 (1942).

    Google Scholar 

  2. D. McMullan, Scanning 17 (3), 175 (2006).

    Article  MathSciNet  Google Scholar 

  3. V. Crewe, J. Wall, and J. Langmore, Science 168 (3937), 1338 (1970).

    Article  ADS  Google Scholar 

  4. J. Goldstein, Scanning Electron Microsc. X-ray Microanal. 44, 684 (2003).

    Google Scholar 

  5. W. C. Lane, Scanning Electron Microsc. 1970, 43 (1970).

    Google Scholar 

  6. D. Drouin, A. R. Couture, D. Joly, et al., Scanning 29 (3), 92 (2007).

    Article  Google Scholar 

  7. J. H. Butler, D. C. Joy, G. F. Bradley, et al., Polymer 36 (9), 1781 (1995).

    Article  Google Scholar 

  8. D. L. Vezie, E. L. Thomas, and W. W. Adams, Polymer 36 (9), 1761 (1995).

    Article  Google Scholar 

  9. Yu. G. Baklagina, S. V. Kononova, V. A. Petrova, et al., Crystallogr. Rep. 58 (2), 287 (2013).

    Article  ADS  Google Scholar 

  10. V. A. Petrova, A. S. Orekhov, D. D. Chernyakov, et al., Crystallogr. Rep. 61 (6), 945 (2016).

    Article  ADS  Google Scholar 

  11. S. V. Kononova, Yu. G. Baklagina, E. V. Kruchinina, et al., Proc. XIII All-Russia Sci. Conf. with Int. Participation MEMBRANES-2016, Nizhny Novgorod, October 10–14, 2016, p. 199.

    Google Scholar 

  12. Low-Voltage Electron Microscopy: Principles and Applications, Ed. by D. C. Bell and N. Erdman (Wiley, New York, 2012), p. 207.

  13. O. Arnould and F. Hild, Microsc. Anal. 33, 13 (2007).

    Google Scholar 

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Correspondence to V. V. Klechkovskaya.

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Original Russian Text © A.S. Orekhov, V.V. Klechkovskaya, S.V. Kononova, 2017, published in Kristallografiya, 2017, Vol. 62, No. 5, pp. 735–740.

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Orekhov, A.S., Klechkovskaya, V.V. & Kononova, S.V. Low-voltage scanning electron microscopy of multilayer polymer systems. Crystallogr. Rep. 62, 710–715 (2017). https://doi.org/10.1134/S1063774517050145

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  • DOI: https://doi.org/10.1134/S1063774517050145

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