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Spectrophotometric determination of the total concentration of sulfonamides in milk after adsorption separation using magnetic hypercrosslinked polystyrene

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Abstract

An approach is proposed to the estimation of the total concentration of sulfonamides in milk based on their adsorption isolation and preconcentration from whole milk with magnetic hypercrosslinked polystyrene followed by the spectrophotometric determination in an acetonitrile eluate by the reaction with p-dimethylaminocinnamaldehyde. The procedure was used for the determination of the total concentration of sulfonamides in milk at a level of the maximum residue limits.

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Authors and Affiliations

  1. Department of Chemistry, Moscow State University, Moscow, 119991, Russia

    V. V. Tolmacheva, V. V. Apyari, D. I. Yarykin & S. G. Dmitrienko

Authors
  1. V. V. Tolmacheva
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  2. V. V. Apyari
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  3. D. I. Yarykin
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  4. S. G. Dmitrienko
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Corresponding author

Correspondence to S. G. Dmitrienko.

Additional information

Original Russian Text © V.V. Tolmacheva, V.V. Apyari, D.I. Yarykin, S.G. Dmitrienko, 2016, published in Zhurnal Analiticheskoi Khimii, 2016, Vol. 71, No. 8, pp. 867–873.

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Tolmacheva, V.V., Apyari, V.V., Yarykin, D.I. et al. Spectrophotometric determination of the total concentration of sulfonamides in milk after adsorption separation using magnetic hypercrosslinked polystyrene. J Anal Chem 71, 834–839 (2016). https://doi.org/10.1134/S1061934816080153

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  • DOI: https://doi.org/10.1134/S1061934816080153

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