Abstract
This work is devoted to studying the structural and morphological properties of a silver colloidal solution obtained by the method of electrical-spark discharge in distilled water. Silver nanoparticles are formed as a result of metal sputtering from the surfaces of silver electrodes, between which a high-voltage electric discharge is generated. The solution is stabilized by forming a layer of anions around the nanoparticles. The structural characteristics of the colloidal solution are studied by small-angle X-ray scattering and transmission electron microscopy. The ionic composition is determined qualitatively using electrospray ionization mass spectrometry, while silver concentration is measured by inductively coupled plasma atomic emission spectrometry.
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ACKNOWLEDGMENTS
We a grateful to E.S. Popova and S.V. Morzhukhina for the determination of the total silver content in the colloidal solution by inductively coupled plasma atomic emission spectrometry.
Funding
This work was supported by the grant for young scien-tists and specialists JINR no. 20-502-03.
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Translated by A. Kirilin
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Kristavchuk, O.V., Sohatsky, A.S., Kozlovskiy, V.I. et al. Structural Characteristics and Ionic Composition of a Colloidal Solution of Silver Nanoparticles Obtained by Electrical-Spark Discharge in Water. Colloid J 83, 448–460 (2021). https://doi.org/10.1134/S1061933X21040049
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DOI: https://doi.org/10.1134/S1061933X21040049