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Structure refinement of cadmium cerium(IV) phosphate Cd0.5Ce2(PO4)3

  • Structure of Inorganic Compounds
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Abstract

Cadmium cerium orthophosphate Cd0.5Ce2(PO4)3 is synthesized by precipitation from aqueous solutions. The structure refinement from powder X-ray diffraction data is preceded by the sample preparation and structure solution. The refinement is carried out by the Rietveld method (ADP-2 diffractometer, Cu Kα radiation, Ni filter, 15° < 2θ < 120°, 2θ-scan step 0.02°, counting time 10 s per step). All calculations are carried out using the WYRIET program (version 3.3) within the sp. gr. P21/n. The structure is refined with anisotropic displacement parameters for cations and isotropic displacement parameters for oxygen atoms.

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Authors and Affiliations

  1. Faculty of Chemistry, Nizhni Novgorod State University, pr. Gagarina 23, Nizhni Novgorod, 603950, Russia

    M. P. Orlova, D. B. Kitaev, M. L. Spiridonova & A. I. Orlova

  2. Faculty of Geology, Moscow State University, Vorob’evy gory, Moscow, 119992, Russia

    N. V. Zubkova & Yu. K. Kabalov

Authors
  1. M. P. Orlova
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  2. D. B. Kitaev
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  3. M. L. Spiridonova
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  4. N. V. Zubkova
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  5. Yu. K. Kabalov
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  6. A. I. Orlova
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Translated from Kristallografiya, Vol. 50, No. 6, 2005, pp. 993–997.

Original Russian Text Copyright © 2005 by M. Orlova, Kitaev, Spiridonova, Zubkova, Kabalov, A. Orlova.

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Orlova, M.P., Kitaev, D.B., Spiridonova, M.L. et al. Structure refinement of cadmium cerium(IV) phosphate Cd0.5Ce2(PO4)3 . Crystallogr. Rep. 50, 918–922 (2005). https://doi.org/10.1134/1.2132396

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  • DOI: https://doi.org/10.1134/1.2132396

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