##############################################################################
###                                                                        ###
###        Electronic paper (Acta Crystallographica Section E)             ###
###                                                                        ###
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#                                                                            #
# This CIF contains the data in a paper accepted for publication in Acta     #
# Crystallographica Section E. It conforms to the requirements of Notes      #
# for Authors for Section E, and has been peer reviewed under the auspices   #
# of the IUCr Commission on Journals.                                        #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic. The current version number is 2.4.    #
#                                                                            #
# Software is freely available for graphical display of the structure(s) in  #
# this CIF.  For information consult the CIF home page http://www.iucr.org/  #
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# This file may be used for bona fide research purposes within the           #
# scientific community so long as proper attribution is given to the journal # 
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data_I
_audit_creation_method     SHELXL-97
_chemical_name_systematic
;
Benzyl N-(4-pyridyl)carbamate
;
_chemical_name_common     ?
_chemical_formula_moiety     'C13 H12 N2 O2'
_chemical_formula_sum     'C13 H12 N2 O2'
_chemical_formula_iupac     'C13 H12 N2 O2'
_chemical_formula_weight     228.25
_chemical_melting_point     ?
_symmetry_cell_setting     'monoclinic'
_symmetry_space_group_name_H-M     'P 21/c'
_symmetry_space_group_name_Hall     '-P 2ybc'
loop_
    _symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, y+1/2, -z+1/2'
    '-x, -y, -z'
    'x, -y-1/2, z-1/2'
_cell_length_a     11.9439(5)
_cell_length_b     13.2120(6)
_cell_length_c     14.6574(7)
_cell_angle_alpha     90.00
_cell_angle_beta     98.418(4)
_cell_angle_gamma     90.00
_cell_volume     2288.06(18)
_cell_formula_units_Z     8
_cell_measurement_reflns_used     2895
_cell_measurement_theta_min     2.12
_cell_measurement_theta_max     26.35
_cell_measurement_temperature     293(2)
_exptl_crystal_description     chunk
_exptl_crystal_colour     colorless
_exptl_crystal_size_max     0.30
_exptl_crystal_size_mid     0.22
_exptl_crystal_size_min     0.18
_exptl_crystal_density_diffrn     1.325
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000     960
_exptl_absorpt_coefficient_mu     0.091
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details     '(SADABS; Bruker, 2001)'
_exptl_absorpt_correction_T_min     0.9731
_exptl_absorpt_correction_T_max     0.9837
_exptl_special_details
;
;
_diffrn_ambient_temperature     293(2)
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_source     'fine-focus sealed tube'
_diffrn_radiation_monochromator     graphite
_diffrn_measurement_device_type     'Bruker APEX area-detector diffractometer'
_diffrn_measurement_method     'φ and ω scan'
_diffrn_detector_area_resol_mean     ?
_diffrn_reflns_number     11332
_diffrn_reflns_av_R_equivalents     0.0386
_diffrn_reflns_av_sigmaI/netI     0.0489
_diffrn_reflns_theta_min     2.31
_diffrn_reflns_theta_max     25.00
_diffrn_reflns_theta_full     25.00
_diffrn_measured_fraction_theta_max     1.000
_diffrn_measured_fraction_theta_full     1.000
_diffrn_reflns_limit_h_min     -14
_diffrn_reflns_limit_h_max     12
_diffrn_reflns_limit_k_min     -15
_diffrn_reflns_limit_k_max     15
_diffrn_reflns_limit_l_min     -17
_diffrn_reflns_limit_l_max     17
_diffrn_standards_number     0
_diffrn_standards_interval_count     .
_diffrn_standards_interval_time     .
_diffrn_standards_decay_%     ?
_refine_special_details
;
Refinement of F² against ALL reflections. The weighted R-factor
wR and goodness of fit S are based on F², conventional
R-factors R are based on F, with F set to zero for
negative F². The threshold expression of F² >
σ(F²) is used only for calculating R-factors(gt) etc.
and is not relevant to the choice of reflections for refinement.
R-factors based on F² are statistically about twice as large
as those based on F, and R- factors based on ALL data will be
even larger.
;
_reflns_number_total     4028
_reflns_number_gt     2831
_reflns_threshold_expression     I>2σ(I)
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.0614
_refine_ls_R_factor_gt     0.0358
_refine_ls_wR_factor_gt     0.0664
_refine_ls_wR_factor_ref     0.0695
_refine_ls_goodness_of_fit_ref     1.049
_refine_ls_restrained_S_all     1.049
_refine_ls_number_reflns     4028
_refine_ls_number_parameters     307
_refine_ls_number_restraints     0
_refine_ls_hydrogen_treatment     constr
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
         'calc w=1/[σ²(Fo²)+(0.0229P)²+0.1100P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     0.000
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     0.169
_refine_diff_density_min     -0.168
_refine_ls_extinction_method     none
_refine_ls_extinction_coef     ?
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0106 0.0060
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'N' 'N' 0.0061 0.0033
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection     'SMART (Bruker, 2001)'
_computing_cell_refinement     'SMART (Bruker, 2001)'
_computing_data_reduction     'SAINT (Bruker, 2001)'
_computing_structure_solution     'SHELXS97 (Sheldrick, 2008)'
_computing_structure_refinement     'SHELXL97 (Sheldrick, 2008)'
_computing_molecular_graphics
                              'ORTEP-3 (Farrugia, 1997) and PLATON (Spek, 2009)'
_computing_publication_material     'SHELXL97 (Sheldrick, 2008)'
loop_
    _atom_site_type_symbol
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_refinement_flags
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    N N2' 0.16150(9) 0.18181(9) -0.00328(9) 0.0227(3) Uani d . 1 . .
    H H2'C 0.2140 0.1458 -0.0216 0.027 Uiso calc R 1 . .
    O O1 0.42587(8) 0.17805(9) 0.26686(8) 0.0335(3) Uani d . 1 . .
    O O2 0.24197(8) 0.13329(8) 0.22775(8) 0.0330(3) Uani d . 1 . .
    O O1' 0.13791(8) 0.32072(8) 0.08678(8) 0.0301(3) Uani d . 1 . .
    O O2' 0.30953(8) 0.27290(8) 0.05366(8) 0.0288(3) Uani d . 1 . .
    N N2 0.36888(9) 0.04846(9) 0.16579(9) 0.0240(3) Uani d . 1 . .
    H H2C 0.3088 0.0179 0.1403 0.029 Uiso calc R 1 . .
    C C1 0.35408(12) 0.12531(12) 0.22453(11) 0.0241(4) Uani d . 1 . .
    N N1' -0.16725(10) 0.07480(10) -0.09588(10) 0.0297(3) Uani d . 1 . .
    C C9 0.47128(11) 0.01402(12) 0.14254(10) 0.0217(4) Uani d . 1 . .
    C C3' 0.48132(13) 0.36576(11) 0.08454(12) 0.0269(4) Uani d . 1 . .
    C C13 0.57368(12) 0.06602(13) 0.16021(12) 0.0292(4) Uani d . 1 . .
    H H13A 0.5789 0.1278 0.1909 0.035 Uiso calc R 1 . .
    C C10 0.47072(12) -0.07770(12) 0.09719(11) 0.0254(4) Uani d . 1 . .
    H H10A 0.4040 -0.1147 0.0844 0.031 Uiso calc R 1 . .
    C C1' 0.19585(12) 0.26347(12) 0.04966(11) 0.0229(4) Uani d . 1 . .
    C C9' 0.05051(12) 0.14969(11) -0.03138(11) 0.0200(4) Uani d . 1 . .
    C C10' 0.03345(12) 0.07278(12) -0.09590(11) 0.0244(4) Uani d . 1 . .
    H H10B 0.0948 0.0447 -0.1193 0.029 Uiso calc R 1 . .
    C C13' -0.04470(12) 0.18983(12) 0.00023(11) 0.0257(4) Uani d . 1 . .
    H H13B -0.0382 0.2421 0.0432 0.031 Uiso calc R 1 . .
    N N1 0.66870(10) -0.06576(10) 0.08657(9) 0.0290(3) Uani d . 1 . .
    C C11' -0.07391(12) 0.03782(12) -0.12545(12) 0.0281(4) Uani d . 1 . .
    H H11A -0.0827 -0.0144 -0.1684 0.034 Uiso calc R 1 . .
    C C3 0.09174(12) 0.16792(12) 0.31022(11) 0.0243(4) Uani d . 1 . .
    C C11 0.56904(12) -0.11411(12) 0.07098(12) 0.0283(4) Uani d . 1 . .
    H H11B 0.5662 -0.1760 0.0406 0.034 Uiso calc R 1 . .
    C C2' 0.36095(12) 0.36077(12) 0.10249(12) 0.0333(4) Uani d . 1 . .
    H H2'A 0.3585 0.3543 0.1681 0.040 Uiso calc R 1 . .
    H H2'B 0.3206 0.4218 0.0804 0.040 Uiso calc R 1 . .
    C C12 0.66733(12) 0.02252(13) 0.13053(12) 0.0328(4) Uani d . 1 . .
    H H12A 0.7352 0.0579 0.1422 0.039 Uiso calc R 1 . .
    C C8 -0.00463(13) 0.21433(13) 0.26577(12) 0.0320(4) Uani d . 1 . .
    H H8A 0.0015 0.2712 0.2294 0.038 Uiso calc R 1 . .
    C C4 0.08082(15) 0.08481(13) 0.36471(12) 0.0367(4) Uani d . 1 . .
    H H4A 0.1454 0.0542 0.3961 0.044 Uiso calc R 1 . .
    C C2 0.20694(13) 0.20348(13) 0.29487(12) 0.0348(5) Uani d . 1 . .
    H H2A 0.2034 0.2721 0.2711 0.042 Uiso calc R 1 . .
    H H2B 0.2594 0.2017 0.3520 0.042 Uiso calc R 1 . .
    C C4' 0.50592(14) 0.36917(12) -0.00500(13) 0.0351(4) Uani d . 1 . .
    H H4'A 0.4472 0.3691 -0.0543 0.042 Uiso calc R 1 . .
    C C8' 0.56941(14) 0.36833(13) 0.15684(13) 0.0388(5) Uani d . 1 . .
    H H8'A 0.5545 0.3653 0.2173 0.047 Uiso calc R 1 . .
    C C12' -0.14897(12) 0.14942(12) -0.03432(12) 0.0309(4) Uani d . 1 . .
    H H12B -0.2119 0.1767 -0.0127 0.037 Uiso calc R 1 . .
    C C5' 0.61669(16) 0.37268(13) -0.02173(15) 0.0465(5) Uani d . 1 . .
    H H5'A 0.6322 0.3726 -0.0821 0.056 Uiso calc R 1 . .
    C C6 -0.12000(16) 0.09262(18) 0.32858(15) 0.0521(6) Uani d . 1 . .
    H H6A -0.1911 0.0671 0.3345 0.063 Uiso calc R 1 . .
    C C7 -0.11059(14) 0.17636(16) 0.27524(14) 0.0453(5) Uani d . 1 . .
    H H7A -0.1754 0.2079 0.2453 0.054 Uiso calc R 1 . .
    C C7' 0.68094(15) 0.37554(14) 0.13934(17) 0.0522(6) Uani d . 1 . .
    H H7'A 0.7400 0.3799 0.1882 0.063 Uiso calc R 1 . .
    C C6' 0.70368(16) 0.37628(14) 0.05031(18) 0.0524(6) Uani d . 1 . .
    H H6'A 0.7782 0.3792 0.0388 0.063 Uiso calc R 1 . .
    C C5 -0.02418(18) 0.04609(15) 0.37357(14) 0.0495(6) Uani d . 1 . .
    H H5A -0.0304 -0.0110 0.4096 0.059 Uiso calc R 1 . .
_geom_special_details
;
All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell e.s.d.'s are taken
into account individually in the estimation of e.s.d.'s in distances, angles
and torsion angles; correlations between e.s.d.'s in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s.
planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    N2' C1' . 1.3569(19) ?
    N2' C9' . 1.3954(17) ?
    N2' H2'C . 0.8600 ?
    O1 C1 . 1.2042(18) ?
    O2 C1 . 1.3509(16) ?
    O2 C2 . 1.4572(17) ?
    O1' C1' . 1.2072(17) ?
    O2' C1' . 1.3561(16) ?
    O2' C2' . 1.4520(17) ?
    N2 C1 . 1.3595(19) ?
    N2 C9 . 1.3932(17) ?
    N2 H2C . 0.8600 ?
    N1' C12' . 1.333(2) ?
    N1' C11' . 1.3457(18) ?
    C9 C10 . 1.382(2) ?
    C9 C13 . 1.394(2) ?
    C3' C4' . 1.387(2) ?
    C3' C8' . 1.380(2) ?
    C3' C2' . 1.500(2) ?
    C13 C12 . 1.383(2) ?
    C13 H13A . 0.9300 ?
    C10 C11 . 1.3749(19) ?
    C10 H10A . 0.9300 ?
    C9' C10' . 1.383(2) ?
    C9' C13' . 1.3940(19) ?
    C10' C11' . 1.372(2) ?
    C10' H10B . 0.9300 ?
    C13' C12' . 1.381(2) ?
    C13' H13B . 0.9300 ?
    N1 C12 . 1.334(2) ?
    N1 C11 . 1.3407(19) ?
    C11' H11A . 0.9300 ?
    C3 C4 . 1.375(2) ?
    C3 C8 . 1.380(2) ?
    C3 C2 . 1.502(2) ?
    C11 H11B . 0.9300 ?
    C2' H2'A . 0.9700 ?
    C2' H2'B . 0.9700 ?
    C12 H12A . 0.9300 ?
    C8 C7 . 1.387(2) ?
    C8 H8A . 0.9300 ?
    C4 C5 . 1.378(2) ?
    C4 H4A . 0.9300 ?
    C2 H2A . 0.9700 ?
    C2 H2B . 0.9700 ?
    C4' C5' . 1.381(2) ?
    C4' H4'A . 0.9300 ?
    C8' C7' . 1.396(2) ?
    C8' H8'A . 0.9300 ?
    C12' H12B . 0.9300 ?
    C5' C6' . 1.369(3) ?
    C5' H5'A . 0.9300 ?
    C6 C7 . 1.369(3) ?
    C6 C5 . 1.379(3) ?
    C6 H6A . 0.9300 ?
    C7 H7A . 0.9300 ?
    C7' C6' . 1.371(3) ?
    C7' H7'A . 0.9300 ?
    C6' H6'A . 0.9300 ?
    C5 H5A . 0.9300 ?
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    C1' N2' C9' . . 127.25(12) ?
    C1' N2' H2'C . . 116.4 ?
    C9' N2' H2'C . . 116.4 ?
    C1 O2 C2 . . 117.22(12) ?
    C1' O2' C2' . . 116.32(11) ?
    C1 N2 C9 . . 126.80(13) ?
    C1 N2 H2C . . 116.6 ?
    C9 N2 H2C . . 116.6 ?
    O1 C1 O2 . . 124.86(14) ?
    O1 C1 N2 . . 127.57(13) ?
    O2 C1 N2 . . 107.58(13) ?
    C12' N1' C11' . . 115.17(13) ?
    C10 C9 N2 . . 117.48(13) ?
    C10 C9 C13 . . 117.66(13) ?
    N2 C9 C13 . . 124.85(14) ?
    C4' C3' C8' . . 118.84(15) ?
    C4' C3' C2' . . 120.56(16) ?
    C8' C3' C2' . . 120.59(15) ?
    C12 C13 C9 . . 117.70(15) ?
    C12 C13 H13A . . 121.2 ?
    C9 C13 H13A . . 121.2 ?
    C9 C10 C11 . . 119.81(14) ?
    C9 C10 H10A . . 120.1 ?
    C11 C10 H10A . . 120.1 ?
    O1' C1' O2' . . 124.01(14) ?
    O1' C1' N2' . . 127.63(14) ?
    O2' C1' N2' . . 108.35(12) ?
    C10' C9' N2' . . 117.64(12) ?
    C10' C9' C13' . . 117.46(14) ?
    N2' C9' C13' . . 124.90(14) ?
    C9' C10' C11' . . 120.04(13) ?
    C9' C10' H10B . . 120.0 ?
    C11' C10' H10B . . 120.0 ?
    C12' C13' C9' . . 117.82(15) ?
    C12' C13' H13B . . 121.1 ?
    C9' C13' H13B . . 121.1 ?
    C12 N1 C11 . . 115.19(12) ?
    N1' C11' C10' . . 123.78(16) ?
    N1' C11' H11A . . 118.1 ?
    C10' C11' H11A . . 118.1 ?
    C4 C3 C8 . . 119.03(15) ?
    C4 C3 C2 . . 120.24(15) ?
    C8 C3 C2 . . 120.62(16) ?
    N1 C11 C10 . . 123.99(15) ?
    N1 C11 H11B . . 118.0 ?
    C10 C11 H11B . . 118.0 ?
    O2' C2' C3' . . 107.20(12) ?
    O2' C2' H2'A . . 110.3 ?
    C3' C2' H2'A . . 110.3 ?
    O2' C2' H2'B . . 110.3 ?
    C3' C2' H2'B . . 110.3 ?
    H2'A C2' H2'B . . 108.5 ?
    N1 C12 C13 . . 125.66(14) ?
    N1 C12 H12A . . 117.2 ?
    C13 C12 H12A . . 117.2 ?
    C7 C8 C3 . . 120.14(17) ?
    C7 C8 H8A . . 119.9 ?
    C3 C8 H8A . . 119.9 ?
    C3 C4 C5 . . 121.07(18) ?
    C3 C4 H4A . . 119.5 ?
    C5 C4 H4A . . 119.5 ?
    O2 C2 C3 . . 105.19(12) ?
    O2 C2 H2A . . 110.7 ?
    C3 C2 H2A . . 110.7 ?
    O2 C2 H2B . . 110.7 ?
    C3 C2 H2B . . 110.7 ?
    H2A C2 H2B . . 108.8 ?
    C3' C4' C5' . . 120.68(18) ?
    C3' C4' H4'A . . 119.7 ?
    C5' C4' H4'A . . 119.7 ?
    C3' C8' C7' . . 120.08(18) ?
    C3' C8' H8'A . . 120.0 ?
    C7' C8' H8'A . . 120.0 ?
    N1' C12' C13' . . 125.71(14) ?
    N1' C12' H12B . . 117.1 ?
    C13' C12' H12B . . 117.1 ?
    C6' C5' C4' . . 120.17(19) ?
    C6' C5' H5'A . . 119.9 ?
    C4' C5' H5'A . . 119.9 ?
    C7 C6 C5 . . 120.11(17) ?
    C7 C6 H6A . . 119.9 ?
    C5 C6 H6A . . 119.9 ?
    C6 C7 C8 . . 120.13(18) ?
    C6 C7 H7A . . 119.9 ?
    C8 C7 H7A . . 119.9 ?
    C6' C7' C8' . . 120.2(2) ?
    C6' C7' H7'A . . 119.9 ?
    C8' C7' H7'A . . 119.9 ?
    C5' C6' C7' . . 119.99(17) ?
    C5' C6' H6'A . . 120.0 ?
    C7' C6' H6'A . . 120.0 ?
    C6 C5 C4 . . 119.50(19) ?
    C6 C5 H5A . . 120.2 ?
    C4 C5 H5A . . 120.2 ?
loop_
    _geom_torsion_atom_site_label_1
    _geom_torsion_atom_site_label_2
    _geom_torsion_atom_site_label_3
    _geom_torsion_atom_site_label_4
    _geom_torsion_site_symmetry_1
    _geom_torsion_site_symmetry_2
    _geom_torsion_site_symmetry_3
    _geom_torsion_site_symmetry_4
    _geom_torsion
    _geom_torsion_publ_flag
    C2 O2 C1 O1 . . . . -7.0(2) ?
    C2 O2 C1 N2 . . . . 173.09(13) ?
    C9 N2 C1 O1 . . . . 0.4(3) ?
    C9 N2 C1 O2 . . . . -179.66(14) ?
    C1 N2 C9 C10 . . . . 166.73(15) ?
    C1 N2 C9 C13 . . . . -14.4(2) ?
    C10 C9 C13 C12 . . . . 0.5(2) ?
    N2 C9 C13 C12 . . . . -178.37(15) ?
    N2 C9 C10 C11 . . . . 178.65(15) ?
    C13 C9 C10 C11 . . . . -0.3(2) ?
    C2' O2' C1' O1' . . . . -3.0(2) ?
    C2' O2' C1' N2' . . . . 175.94(13) ?
    C9' N2' C1' O1' . . . . 4.4(3) ?
    C9' N2' C1' O2' . . . . -174.45(13) ?
    C1' N2' C9' C10' . . . . 171.04(15) ?
    C1' N2' C9' C13' . . . . -8.5(2) ?
    N2' C9' C10' C11' . . . . 179.55(14) ?
    C13' C9' C10' C11' . . . . -0.9(2) ?
    C10' C9' C13' C12' . . . . 0.6(2) ?
    N2' C9' C13' C12' . . . . -179.87(14) ?
    C12' N1' C11' C10' . . . . -0.1(2) ?
    C9' C10' C11' N1' . . . . 0.7(2) ?
    C12 N1 C11 C10 . . . . 0.1(2) ?
    C9 C10 C11 N1 . . . . 0.0(3) ?
    C1' O2' C2' C3' . . . . -170.42(13) ?
    C4' C3' C2' O2' . . . . 56.18(19) ?
    C8' C3' C2' O2' . . . . -124.65(17) ?
    C11 N1 C12 C13 . . . . 0.1(3) ?
    C9 C13 C12 N1 . . . . -0.4(3) ?
    C4 C3 C8 C7 . . . . -0.9(2) ?
    C2 C3 C8 C7 . . . . 175.37(15) ?
    C8 C3 C4 C5 . . . . 1.6(2) ?
    C2 C3 C4 C5 . . . . -174.66(15) ?
    C1 O2 C2 C3 . . . . -157.99(14) ?
    C4 C3 C2 O2 . . . . 77.04(18) ?
    C8 C3 C2 O2 . . . . -99.19(16) ?
    C8' C3' C4' C5' . . . . 1.5(2) ?
    C2' C3' C4' C5' . . . . -179.31(14) ?
    C4' C3' C8' C7' . . . . 0.8(3) ?
    C2' C3' C8' C7' . . . . -178.39(15) ?
    C11' N1' C12' C13' . . . . -0.2(2) ?
    C9' C13' C12' N1' . . . . -0.1(2) ?
    C3' C4' C5' C6' . . . . -2.2(3) ?
    C5 C6 C7 C8 . . . . 0.4(3) ?
    C3 C8 C7 C6 . . . . -0.1(3) ?
    C3' C8' C7' C6' . . . . -2.4(3) ?
    C4' C5' C6' C7' . . . . 0.5(3) ?
    C8' C7' C6' C5' . . . . 1.8(3) ?
    C7 C6 C5 C4 . . . . 0.3(3) ?
    C3 C4 C5 C6 . . . . -1.3(3) ?
loop_
    _geom_hbond_atom_site_label_D
    _geom_hbond_atom_site_label_H
    _geom_hbond_atom_site_label_A
    _geom_hbond_site_symmetry_A
    _geom_hbond_distance_DH
    _geom_hbond_distance_HA
    _geom_hbond_distance_DA
    _geom_hbond_angle_DHA
    N2' H2'C N1 3_655 0.86 2.09 2.9460(16) 171.1
    N2 H2C N1' 3 0.86 2.11 2.9630(18) 170.4
data_global
_journal_date_recd_electronic     2010-01-06
_journal_date_accepted     2010-01-08
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2010
_journal_volume     66
_journal_issue      2
_journal_page_first     o401
_journal_page_last     o401
_journal_paper_category     QO
_journal_coeditor_code     JH2125
_publ_contact_author_name     'Fang, Mei-Juan'
_publ_contact_author_address
;
Department of Pharmaceutical Science, Medical College, Xiamen
University, Xiamen 361005, People's Republic of China.
;
_publ_contact_author_email     fangmj@xmu.edu.cn
_publ_contact_author_fax     '86-592-2199000'
_publ_contact_author_phone     '86-592-2199000'
_publ_section_title
;
Benzyl N-(4-pyridyl)carbamate
;
loop_
    _publ_author_name
    _publ_author_address
    'Fang, Hua'
;
The Third Institute of Oceanography of the State Oceanic Administration
Xiamen 361005, People's Republic of China
;
    'Fang, Mei-Juan'
;
Department of Pharmaceutical Science, Medical College
Xiamen University, Xiamen 361005, People's Republic of China
;
    'Zhang, Yi-Ping'
;
The Third Institute of Oceanography of the State Oceanic Administration
Xiamen 361005, People's Republic of China
;
