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A 36-membered macrocycle, H313+, crystallizes with a mixture of five phosphates with valences HPO42−, H2PO4−, and H3PO4. The macrocycles form sandwich-like channels for clusters of six phosphates interconnected through oligomeric chains of water-linked phosphates and phosphoric acid molecules. Binding studies indicate 3 : 1 phosphate : macrocycle associations in keeping with 6 : 2 phosphate : macrocycle “sandwiches.”
S. Pramanik, P. Thordarson, V. W. Day and K. Bowman-James, CrystEngComm, 2022, 24, 8047 DOI: 10.1039/D2CE00756H
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