Issue 3, 1993
From the journal:

Journal of the Chemical Society, Chemical Communications

High-resolution solid-state 13C and 29Si NMR investigations of the dynamic properties of tetrakis(trimethylsilyl)silane

Abil E. Aliev,   Kenneth D. M. Harris  and  David C. Apperley  

Abstract

High-resolution solid-state 13C and 29Si NMR spectroscopy have been used to investigate the dynamic properties of tetrakis(trimethylsilyl)silane (TTMSS) as a function of temperature; from the temperature dependence of the spectra, it is clear that TTMSS is not useful as a chemical shift reference material below ca. 238K, but the spectral changes associated with the phase transition at this temperature nevertheless provide a precise method for controlling temperature calibration in low-temperature solid-state 13C NMR studies.

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Article information

DOI
https://doi.org/10.1039/C39930000251
Article type
Paper

J. Chem. Soc., Chem. Commun., 1993, 251-253

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High-resolution solid-state 13C and 29Si NMR investigations of the dynamic properties of tetrakis(trimethylsilyl)silane

A. E. Aliev, K. D. M. Harris and D. C. Apperley, J. Chem. Soc., Chem. Commun., 1993, 251 DOI: 10.1039/C39930000251

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