The title compounds 3 are formed in very high yield from a one-pot sequential reaction of 1,3,2-dithiaphospholane PIII derivatives 1, which are transformed into the corresponding PIV compounds 2 by addition of elemental sulfur and finally into fluoridodithioates 3 by TBAF.
I. Tworowska and W. Dąbkowski, Chem. Commun., 1998, 2611 DOI: 10.1039/A807029F
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