A series of highly crystalline β-sialons prepared by self-propagating high-temperature synthesis (SHS) has been characterized by powder X-ray diffraction, 29Si and 27Al MAS NMR spectroscopy. The microdomain-type structure of the products (with general composition Si6 –zAlzOzN8 –z where 0.5 ⩽z⩽ 2.0) is very similar to that of β-sialons prepared using conventional synthesis methods.
Y. Yue, H. He, J. Klinowski, Y. Wu and H. Zhuang, J. Mater. Chem., 1996, 6, 1391 DOI: 10.1039/JM9960601391
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