Issue 1, 2014
From the journal:

New Journal of Chemistry

New strategies for the synthesis of lactones using peroxymonosulphate salts, ionic liquids and microwave or ultrasound irradiation†

Karolina Matuszek,a   Przemysław Zawadzki,b   Wojciech Czardybonb  and  Anna Chrobok*a  

* Corresponding authors

a Silesian University of Technology, Faculty of Chemistry, Department of Chemical Organic Technology and Petrochemistry, ul. Krzywoustego 4, 44-100 Gliwice, Poland
E-mail: anna.chrobok@polsl.pl
Fax: +48 322371032
Tel: +48 322372917

b Selvita S.A., Park Life Science, Bobrzyńskiego 14, 30-348 Kraków, Poland
E-mail: wojciech.czardybon@selvita.com
Fax: +48 122974701
Tel: +48 122974700

Abstract

A new method for the rapid synthesis of lactones via the one-pot oxidation of alcohols with potassium peroxymonosulphate in an ionic liquid was developed. The use of microwave or ultrasonic irradiation increased the reaction rates significantly. Additionally, new peroxymonosulphate ionic liquids were synthesised and used as effective oxidants in the synthesis of lactones.

Graphical abstract: New strategies for the synthesis of lactones using peroxymonosulphate salts, ionic liquids and microwave or ultrasound irradiation

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Article information

DOI
https://doi.org/10.1039/C3NJ01170D
Article type
Paper
Submitted
26 Sep 2013
Accepted
18 Oct 2013
First published
23 Oct 2013

New J. Chem., 2014,38, 237-241

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New strategies for the synthesis of lactones using peroxymonosulphate salts, ionic liquids and microwave or ultrasound irradiation

K. Matuszek, P. Zawadzki, W. Czardybon and A. Chrobok, New J. Chem., 2014, 38, 237 DOI: 10.1039/C3NJ01170D

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