31P,89Y Shift correlation. Application to the speciation of yttrium complexes with triphenylphosphine oxide

Ignacio Fernández; Víctor Yañez-Rodríguez; Fernando López Ortiz

doi:10.1039/C0DT01733G

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³¹P,⁸⁹Y Shift correlation. Application to the speciation of yttrium complexes with triphenylphosphine oxide†

Ignacio Fernández,^a Víctor Yañez-Rodríguez^a and Fernando López Ortiz*^a

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* Corresponding authors

^a Área de Química Orgánica, Universidad de Almería, Carretera de Sacramento, Almería, Spain
E-mail: flortiz@ual.es
Fax: +34 950 015481
Tel: +34 950 015478

Abstract

Correlation experiments between ⁸⁹Y and ³¹P nuclei through scalar coupling using ³¹P detection are described for the first time. The utility of the new method of characterizing ⁸⁹Y is demonstrated by identifying the species formed in the reaction of yttrium nitrate with triphenylphosphine oxide in THF solution.

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Article information

DOI: https://doi.org/10.1039/C0DT01733G
Article type: Communication
Submitted: 09 Dec 2010
Accepted: 17 Dec 2010
First published: 19 Jan 2011

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Dalton Trans., 2011,40, 2425-2428

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³¹P,⁸⁹Y Shift correlation. Application to the speciation of yttrium complexes with triphenylphosphine oxide

I. Fernández, V. Yañez-Rodríguez and F. L. Ortiz, Dalton Trans., 2011, 40, 2425 DOI: 10.1039/C0DT01733G

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Dalton Transactions