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Structural studies of supported tin catalysts

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Abstract

Tin oxide was supported on aluminium oxide, titanium oxide, magnesium oxide and silicon oxide, and the resulting interactions between the components in the prepared samples and after reduction were characterized by Mössbauer spectroscopy. It was observed that in the oxide state, tin is present as SnO2 on alumina, magnesia and silica, but on titania tin occupies Ti sites in the structure. After hydrogen treatment at high temperatures, tin is reduced from Sn(4) to Sn(2) on alumina and titania; it is reduced from Sn(4) to Sn(0) on silica, and is practically not reduced on magnesia. These results reveal the degree of interaction between tin and the different supports studied.

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Authors and Affiliations

  1. Instituto Mexicano del Petróleo, Gerencia de Catalizadores, Eje Central Lázaro Cárdenas 152, México D.F, 07730

    Noel Nava

  2. Universidad Autonoma Metropolitana-Iztapalapa, Area de Ingeniería Química, Av. Michoacán y Purísima S/N, Col. Vicentina, México D.F, 09340

    Noel Nava & Tomás Viveros

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  1. Noel Nava
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  2. Tomás Viveros
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Nava, N., Viveros, T. Structural studies of supported tin catalysts. Hyperfine Interactions 122, 147–153 (1999). https://doi.org/10.1023/A:1012601924217

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