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Crystal structure and characterization of 1,2-N,N-disallicydene-phenylamineato nickel(II) complex

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Abstract

A new complex has been synthesized and characterized by elemental analysis, IR, TGA, and single-crystal X-ray analysis. The crystal is orthorhombic and the space group is chiral (P212121) with a = 6.620(3) Å, b = 17.300(4) Å,, c = 5.450(1) Å,, α = 90°, β = 90°, γ = 90°, z = 4. In the crystal lattice, the molecules create a two-dimensional network structure through hydrogen bonds. The C–H⋅⋅⋅O intermolecular hydrogen bonds connect the title complex to form a supermolecular structure.

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Correspondence to Xin Wang.

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Wang, J., Bei, FL., Xu, XY. et al. Crystal structure and characterization of 1,2-N,N-disallicydene-phenylamineato nickel(II) complex. Journal of Chemical Crystallography 33, 845–849 (2003). https://doi.org/10.1023/A:1027453612243

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  • DOI: https://doi.org/10.1023/A:1027453612243

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