Palaeointensity just at the onset of the Cretaceous normal superchron
Highlights
► Basalt from Jianchang, Northeast China. ► Low palaeointensity at the onset of CNS. ► Detecting the thermal alteration on palaeointensity experiments.
Introduction
The long-term variations in the strength of the geomagnetic field provide important constraints on the chemical–physical processes of the Earth’s interior (Prévot and Perrin, 1992, Coe et al., 2000). Especially, the intensity of the geomagnetic field during the Cretaceous normal superchron (CNS) is crucial to understand the geodynamo. Glatzmaier et al. (1999) have suggested that the Earth’s dipole moment correlates negatively with the geomagnetic reversal rate, which implies that the geomagnetic field during the CNS should be strong. However, there exist arguments about the measured palaeointensity data, e.g., high palaeointensities obtained from plagioclase single crystals (Tarduno et al., 2001, Tarduno et al., 2002) versus low palaeointensities from whole rocks and submarine basalt glass (SBG) (e.g., Prévot et al., 1990, Pick and Tauxe, 1993, Tanaka and Kono, 2002, Riisager et al., 2003, Zhu et al., 2004a, Zhu et al., 2004b, Zhu et al., 2008, Pan et al., 2004, Zhao et al., 2004, Shi et al., 2005). Although it has been reported that palaeointensities near the onset and the termination of the CNS are only half of the present day field strength (Pick and Tauxe, 1993), debates still remain due to the insufficient palaeointensity data (Goguitchaichvili et al., 2002a, Ruiz et al., 2006). Therefore, the palaeointensity during the geomagnetic field switching from a reversing to a non-reversing state at the onset of the CNS is particularly interesting. In this paper, we present the first palaeointensity results obtained from Jianchang basalts, NE China, erupted at ∼119 Ma.
Section snippets
Geological setting
Mesozoic volcanic rocks are extensively distributed in west Liaoning Province and its adjacent areas. Previous geochronologic and geochemical investigations in this region showed that the main eruptions occurred during four major eruption periods from the early Jurassic to early Cretaceous: (1) the Xinglonggou formation, 180–170 Ma; (2) the Lanqi formation, 160–150 Ma; (3) the Yixian formation, 126–120 Ma; and (4) the Yingchengzi formation, 110–100 Ma (Chen et al., 1992, Yang and Li, 2008). These
40Ar/39Ar dating
Basalt samples were crushed and sieved between 40 and 80 mesh (380–200 μm) and were washed with distilled water. Volcanic matrixes without phenocrysts were hand-picked under binocular microscope and were washed with acetone in an ultra-sonic bath for 20 min. To eliminate possible alterations, matrix samples were washed with 5% HNO3 in an ultra-sonic bath for 20 min. Then the grains were rinsed with distilled water, dried, wrapped in aluminum foil and irradiated together with TCR-sanidine
Rock magnetic experiments
Magnetic hysteresis loops and the stepwise backfield demagnetization of the saturation isothermal remanence (SIRM) were measured on the MMVFTB with a maximum field of 1.0 T. At least nine samples from each flow (a total of 81 samples) were carried out in experiments. The hysteresis parameters (saturation magnetization, Ms, saturation remanence, Mrs, coercivity, Hc) were obtained after correcting the high-field slopes. The remanent coercivity (Hcr) was obtained using the backfield demagnetization
Palaeomagnetic direction
The cylinder samples with diameter of 2.5 cm were cut to shorter cylinders with length of 1.0 cm in the laboratory, and then the shorter specimens were further drilled to two parts: the small inner cylinders with diameter of 1.0 cm for palaeointensity experiments and the hollow rings for stepwise thermal or alternating field (AF) demagnetizations, respectively. At least 10 samples from each lava flow were subjected to thermal or AF demagnetizations. In most cases, stepwise thermal demagnetization
Palaeointensity determination
All together, 286 samples including some parallel samples were experimented for palaeointensity determinations. The Coe version (Coe, 1967) of the Thellier method with sliding pTRM checks (Prévot et al., 1985) and pTRM-tail checks (Riisager and Riisager, 2001) was used in this study. In order to perform the pTRM-tail check, samples were heated in zero field again after in-field heatings to the same temperatures. The standard pTRM checks were obtained after the pTRM-tail checks by heating to the
Rock magnetism during palaeointensity experiments
The palaeointensity results vary significantly with a factor of ∼4 even in the same lava flow. The concave-up NRM–TRM curves in Arai plots can be caused either by MD effects (Levi, 1977, Fabian, 2001, Shcherbakov and Shcherbakova, 2001, Biggin and Thomas, 2003, Coe et al., 2004) or by thermal alteration during heating (Haag et al., 1995, Calvo et al., 2002). In order to determine the exact mechanism, more systematic rock magnetism measurements were carried out for samples with positive pTRM
Discussion
Although a stable ChRM was obtained from the majority of sample, it is crucial to consider the origin of magnetization. As discussed above, thermomagnetic analysis shows that the remanence is mainly carried by Ti-poor titanomagnetite or pure magnetite, which is probably resulted from high temperature oxyexsolution during the flow emplacement and indicates primary magnetization of thermoremanent origin (Buddington and Lindsley, 1964, Dunlop and Özdemir, 1997, Goguitchaichvili et al., 2002b).
Conclusion
The ideal magnetic carriers for palaeointensity studies are SD particles that can remain stable during heating in palaeointensity. However, the chemical alteration is common during heatings. Although pTRM check as a conventional method, is widely used to judge the chemical alteration, our results supports the idea that pTRM checks at certain temperatures (e.g., JC1) cannot detect the newly-formed magnetic particles with Tub > T1. The newly proposed rock magnetic experiment can be an auxiliary
Acknowledgments
We thank S.M. Ren and S. Huang for assistance in field work. We thank Huapei Wang for proof reading the initial manuscript. The manuscript was greatly improved by the constructive comments of the editor Dr. M. Hill and by the comments of reviewer Dr. P. Camps and another anonymous reviewer. This work is supported by NSFC Grants (40821091 and 40634024) and China MOST 973 Program (2006CB701403).
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