Palaeointensity just at the onset of the Cretaceous normal superchron

https://doi.org/10.1016/j.pepi.2011.05.009Get rights and content

Abstract

A combined palaeomagnetic and geochronologic study has been conducted on a basaltic lava sequence of five flows at Jianchang in Liaoning Province, northeastern China. Radiometric 40Ar/39Ar dating indicates that the volcanism occurred at about 119 Ma within the marine anomaly C34n in Cretaceous normal superchron (CNS). Rock magnetic investigations show that pseudo-single domain (PSD) or a mixture of single domain and multi-domain grain titanium-poor titanomagnetite is dominant in the studied lava flows. Both stepwise thermal and alternating field demagnetizations isolate the well-defined normal characteristic remanent magnetization (ChRM) in five independent lava flows with a mean direction of D/I = 11.1°/57.2° (α95 = 5.7°). Palaeointensity was determined using the Coe modified Thellier method with systematic partial thermoremanent magnetization (pTRM) checks. All together, 61 samples from 286 samples with positive pTRM and tail checks yield palaeointensities ranging between 10.1 and 73.6 μT. To further check the effects of thermal alteration on the palaeointensity results, a new ratio (Mrs,480°C/Mrs,25°C, where Mrs,25°C and Mrs,480°C are the room temperature saturation isothermal remanent magnetizations for the raw sample and the product after a 480 °C thermal treatment, respectively) is proposed. Results show that the ratio changes significantly even for those samples with positive pTRM check. We further put forward that palaeointensity results are acceptable with ratio between 0.9 and 1.1. With this new criteria, 17 samples show consistent palaeointensity results with an average of 20.0 ± 3.2 μT. This value corresponds to the virtual dipole magnetic moments (VDM) of (3.5 ± 0.6) × 1022 Am2, which is about half of the value of present field. This finding, combined with other available results, suggests that magnetic field of the Earth just at the onset of the CNS is characterized by a weak palaeointensity.

Highlights

Basalt from Jianchang, Northeast China. ► Low palaeointensity at the onset of CNS. ► Detecting the thermal alteration on palaeointensity experiments.

Introduction

The long-term variations in the strength of the geomagnetic field provide important constraints on the chemical–physical processes of the Earth’s interior (Prévot and Perrin, 1992, Coe et al., 2000). Especially, the intensity of the geomagnetic field during the Cretaceous normal superchron (CNS) is crucial to understand the geodynamo. Glatzmaier et al. (1999) have suggested that the Earth’s dipole moment correlates negatively with the geomagnetic reversal rate, which implies that the geomagnetic field during the CNS should be strong. However, there exist arguments about the measured palaeointensity data, e.g., high palaeointensities obtained from plagioclase single crystals (Tarduno et al., 2001, Tarduno et al., 2002) versus low palaeointensities from whole rocks and submarine basalt glass (SBG) (e.g., Prévot et al., 1990, Pick and Tauxe, 1993, Tanaka and Kono, 2002, Riisager et al., 2003, Zhu et al., 2004a, Zhu et al., 2004b, Zhu et al., 2008, Pan et al., 2004, Zhao et al., 2004, Shi et al., 2005). Although it has been reported that palaeointensities near the onset and the termination of the CNS are only half of the present day field strength (Pick and Tauxe, 1993), debates still remain due to the insufficient palaeointensity data (Goguitchaichvili et al., 2002a, Ruiz et al., 2006). Therefore, the palaeointensity during the geomagnetic field switching from a reversing to a non-reversing state at the onset of the CNS is particularly interesting. In this paper, we present the first palaeointensity results obtained from Jianchang basalts, NE China, erupted at ∼119 Ma.

Section snippets

Geological setting

Mesozoic volcanic rocks are extensively distributed in west Liaoning Province and its adjacent areas. Previous geochronologic and geochemical investigations in this region showed that the main eruptions occurred during four major eruption periods from the early Jurassic to early Cretaceous: (1) the Xinglonggou formation, 180–170 Ma; (2) the Lanqi formation, 160–150 Ma; (3) the Yixian formation, 126–120 Ma; and (4) the Yingchengzi formation, 110–100 Ma (Chen et al., 1992, Yang and Li, 2008). These

40Ar/39Ar dating

Basalt samples were crushed and sieved between 40 and 80 mesh (380–200 μm) and were washed with distilled water. Volcanic matrixes without phenocrysts were hand-picked under binocular microscope and were washed with acetone in an ultra-sonic bath for 20 min. To eliminate possible alterations, matrix samples were washed with 5% HNO3 in an ultra-sonic bath for 20 min. Then the grains were rinsed with distilled water, dried, wrapped in aluminum foil and irradiated together with TCR-sanidine

Rock magnetic experiments

Magnetic hysteresis loops and the stepwise backfield demagnetization of the saturation isothermal remanence (SIRM) were measured on the MMVFTB with a maximum field of 1.0 T. At least nine samples from each flow (a total of 81 samples) were carried out in experiments. The hysteresis parameters (saturation magnetization, Ms, saturation remanence, Mrs, coercivity, Hc) were obtained after correcting the high-field slopes. The remanent coercivity (Hcr) was obtained using the backfield demagnetization

Palaeomagnetic direction

The cylinder samples with diameter of 2.5 cm were cut to shorter cylinders with length of 1.0 cm in the laboratory, and then the shorter specimens were further drilled to two parts: the small inner cylinders with diameter of 1.0 cm for palaeointensity experiments and the hollow rings for stepwise thermal or alternating field (AF) demagnetizations, respectively. At least 10 samples from each lava flow were subjected to thermal or AF demagnetizations. In most cases, stepwise thermal demagnetization

Palaeointensity determination

All together, 286 samples including some parallel samples were experimented for palaeointensity determinations. The Coe version (Coe, 1967) of the Thellier method with sliding pTRM checks (Prévot et al., 1985) and pTRM-tail checks (Riisager and Riisager, 2001) was used in this study. In order to perform the pTRM-tail check, samples were heated in zero field again after in-field heatings to the same temperatures. The standard pTRM checks were obtained after the pTRM-tail checks by heating to the

Rock magnetism during palaeointensity experiments

The palaeointensity results vary significantly with a factor of ∼4 even in the same lava flow. The concave-up NRM–TRM curves in Arai plots can be caused either by MD effects (Levi, 1977, Fabian, 2001, Shcherbakov and Shcherbakova, 2001, Biggin and Thomas, 2003, Coe et al., 2004) or by thermal alteration during heating (Haag et al., 1995, Calvo et al., 2002). In order to determine the exact mechanism, more systematic rock magnetism measurements were carried out for samples with positive pTRM

Discussion

Although a stable ChRM was obtained from the majority of sample, it is crucial to consider the origin of magnetization. As discussed above, thermomagnetic analysis shows that the remanence is mainly carried by Ti-poor titanomagnetite or pure magnetite, which is probably resulted from high temperature oxyexsolution during the flow emplacement and indicates primary magnetization of thermoremanent origin (Buddington and Lindsley, 1964, Dunlop and Özdemir, 1997, Goguitchaichvili et al., 2002b).

Conclusion

The ideal magnetic carriers for palaeointensity studies are SD particles that can remain stable during heating in palaeointensity. However, the chemical alteration is common during heatings. Although pTRM check as a conventional method, is widely used to judge the chemical alteration, our results supports the idea that pTRM checks at certain temperatures (e.g., JC1) cannot detect the newly-formed magnetic particles with Tub > T1. The newly proposed rock magnetic experiment can be an auxiliary

Acknowledgments

We thank S.M. Ren and S. Huang for assistance in field work. We thank Huapei Wang for proof reading the initial manuscript. The manuscript was greatly improved by the constructive comments of the editor Dr. M. Hill and by the comments of reviewer Dr. P. Camps and another anonymous reviewer. This work is supported by NSFC Grants (40821091 and 40634024) and China MOST 973 Program (2006CB701403).

References (64)

  • P.R. Renne et al.

    Intercalibration of standards, absolute ages and uncertainties in 40Ar/39Ar dating

    Chem. Geol.

    (1998)
  • P. Riisager et al.

    Detecting multidomain magnetic grains in Thellier palaeointensity experiments

    Phys. Earth Planet. Inter.

    (2001)
  • R.P. Shi et al.

    40Ar/39Ar dating and preliminary paleointensity determination on a single lave flow from Chifeng, Inner Mongolia

    Phys. Earth Planet. Inter.

    (2005)
  • H. Tanaka et al.

    Paleointensities from a Cretaceous basalt platform in Inner Mongolia, northeastern China

    Phys. Earth Planet. Inter.

    (2002)
  • H. Tsunakawa et al.

    Paleointensity study of the middle Cretaceous Iritono granite in northeast Japan: implication for high field intensity of the Cretaceous normal superchron

    Phys. Earth Planet. Inter.

    (2009)
  • F. Wang et al.

    Timing of volcanism succession of the Great Xing’an Range, Northeastern Asia, and its tectonic significance

    Earth Planet. Sci. Lett.

    (2006)
  • F.Y. Wu et al.

    Nature and significance of the Early Cretaceous giant igneous event in eastern China

    Earth Planet. Sci. Lett.

    (2005)
  • Y. Yamamoto et al.

    Paleomagnetic and rock magnetic studies of the Sakurajima 1914 and 1946 andesitic lavas from Japan: a comparison of the LTD–DHT Shaw and Thellier paleointensity methods

    Phys. Earth Planet. Inter.

    (2008)
  • X.X. Zhao et al.

    New palaeointensity results from Cretaceous basalt of inner Mongolia, China

    Phys. Earth Planet. Inter.

    (2004)
  • R.X. Zhu et al.

    Geomagnetic palaeointensity just prior to the Cretaceous normal superchron

    Phys. Earth Planet. Inter.

    (2001)
  • R.X. Zhu et al.

    Evidence for weak geomagnetic field intensity prior to the Cretaceous normal superchron

    Phys. Earth Planet. Inter.

    (2003)
  • R.X. Zhu et al.

    Geomagnetic paleointensity and direct age determination of the ISEA (M0r?)

    Chron. Earth Planet. Sci. Lett.

    (2004)
  • R.X. Zhu et al.

    Paleointensities determined from the middle Cretaceous basalt in Liaoning Province, northeastern China

    Phys. Earth Planet. Inter.

    (2004)
  • R.X. Zhu et al.

    Palaeomagnetism and 40Ar/39Ar age from a Cretaceous volcanic sequence, Inner Mongolia, China: implications for the field variation during the Cretaceous normal superchron

    Phys. Earth Planet. Inter.

    (2008)
  • Baksi, A.K., 2007. A quantitative tool for detecting alteration in undisturbed rocks and mineral – I: water, chemical...
  • A.F. Buddington et al.

    Iron–titanium oxide minerals and synthetic equivalents

    J. Petrol.

    (1964)
  • M. Calvo et al.

    Investigating the reasons for the failure of palaeointensity experiments: a study on historical lava flows from Mt Etna (Italy)

    Geophys. J. Int.

    (2002)
  • Y.X. Chen et al.

    Volcanic Rocks in West Liaoning and its Adjacent Area: Chronology, Geochemistry and Tectonics

    (1997)
  • W.J. Chen et al.

    The age and geochemistry of basin basalt at Xialiaohe rift

  • R.S. Coe

    Paleointensity of the earth’s magnetic field determined from Tertiary and Quaternary rocks

    J. Geophys. Res.

    (1967)
  • R.S. Coe et al.

    Geomagnetic paleointensities from radiocarbon-dated lava flows on Hawaii and the question of the Pacific nondipole low

    J. Geophys. Res.

    (1978)
  • R. Coe et al.

    Geomagnetic paleointensities from excursion sequences in lavas on Oahu, Hawaii

    J. Geophys. Res.

    (1984)
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