Structural assignment of n3-acylated uridine derivatives by means of 13c nmr spectroscopy
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2016, European Journal of Medicinal ChemistryCitation Excerpt :Formation of the bisacylated by-products 6 was studied in detail using benzoyl chloride 2a as an acylating agent in pyridine [34]. The structure of the isolated 6a was unambiguously assigned as a 3′-O, 3-N-bisacyl derivative on the basis of comparative 13C NMR spectroscopic analysis of compounds 5a, 6a and 7a [35,36]. The use of a stoichiometric amount of acylating reagent 2a reduced significantly formation of the undesired N-acylation products, but at the same time a considerable portion of the starting nucleoside 1 remained unreacted.
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