Journal of Photochemistry and Photobiology A: Chemistry
Singlet- and triplet-state photodissociation of CO and CN bonds in aromatic acetones studied by 1H-CIDNP spectroscopy
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2017, Tetrahedron LettersCitation Excerpt :This process has been performed often within a solvent cage. Microcavities of zeolites,9 cyclodextrins,10 polyethylene film,11 liquid crystals,12 Nafion membranes13 and silica surfaces along with a magnetic field14 have been utilized to control the ratio of the ortho and para regioisomers produced and the reaction efficiency. Moreover, rearrangement reactions of 1-naphthyl and 2-naphthyl esters generate 2- and 4-acyl15 and 1-, 3-, 6- and 8-acyl naphthols,15f, h,n,16 respectively.
Chapter 3 Photo-CIDNP Spectroscopy
2009, Annual Reports on NMR SpectroscopyCitation Excerpt :If a variation of the experimental conditions affects the balance between these two entry channels to the radical-pair mechanism, the “logical box” evolves into a “mathematical box” that allows a separation of the contributions of singlet and triplet precursors. A spectacular example of that has been reported91 for the β-cleavage of (N-methylanilino)acetone (Chart 3). The radical pair formed upon excitation at 308 nm yields a variety of products.
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