ArticlesAn efficient water-soluble ruthenium hydroformylation catalyst for the exclusive formation of 1-heptaldehyde from 1-hexene
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Ruthenium-catalyzed hydroformylation of the functional unsaturated fatty nitrile 10-undecenitrile
2016, Journal of Molecular Catalysis A: ChemicalCitation Excerpt :Using Ru3(CO)12 or Ru(methylallyl)2(COD) as precursor, combined with 1 equiv. ( vs. Ru) of a 2-phosphino-substituted imidazole ligand, at a [olefin]/[Ru] ratio of 167, 130 °C and 60 bar CO/H2 (1:5), they achieved full conversion of 1-octene (overall TOF = 0.13 min−1) to provide 87% of alcohol (l/b = 10), along with 9% of octane and less than 1% of the intermediate aldehyde [13,14]. In previous studies, we reported the use of Rh-Biphephos [15] and Ir-Biphephos [5][5c] catalyst systems for the tandem isomerization-hydroformylation [16,17] of the unsaturated fatty nitrile 10-undecenitrile (1) (Scheme 1), as a route toward biosourced polyamide-12.
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1992, Advances in Organometallic ChemistryNovel dinuclear μ-carboxylatoruthenium complexes for the low pressure hydroformylation of terminal alkenes
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