Diaza-polyoxa-macrocycles et macrobicycles
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Coordination/metal–organic cages inside out
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2022, Tetrahedron LettersCitation Excerpt :For cage synthesis, the same two main synthetic strategies described to prepare macrocycles depending on the type of reaction employed for the assembly of the building blocks, irreversible and reversible bond formation, can also be employed to prepare cage molecules. Although irreversible bonds were used to prepare the first examples of molecular cages back in 1969 by Lehn, Sauvage, and Dietrich in 25% overall yield [17], irreversible bonds do not allow self-correction of mistakes produced during the cage formation, resulting in low overall yields. The low-efficiency results in extremely low yields for more complex cage structures.
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