Abstract
In this study, an off-line coupling of dispersive solid-phase extraction (DSPE) and ion mobility spectrometry (IMS) was introduced to extract and determine bupropion (BUP). A magnetic nanocomposite adsorbent (Fe3O4@CuO&GO) was fabricated by combining graphene oxide (GO) sheets with Fe3O4 and CuO through coprecipitation method. The synthesized adsorbent was characterized and analyzed using the analytical techniques. The effect of extraction parameters including desorption solvent (type and volume), pH, adsorbent amount, contact time, temperature, and the volume of analyte solution on the extraction efficiency was investigated and optimized. The operational parameters of IMS method were also investigated. Under the optimum conditions (DSPE–IMS), the proposed method provided a linear range 4.0–24.0 ng for BUP with a determination coefficient R2 ≥ 0.98. LOD and LOQ values were 0.7 and 2.2 ng for BUP. The repeatability of proposed method was evaluated and reported as relative standard deviation (RSD% ≤ 5.5). The developed method was applied to determine BUP in different biological samples, in which satisfactory results were obtained (93.0–98.0%).
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References
S.M. Stahl, J.F. Pradko, B.R. Haight, J.G. Modell, C.B. Rockett, S. Learned-Coughlin, Prim Care Companion J. Clin. Psychiatry 6(4), 159 (2004)
L.P. Dwoskin, A.S. Rauhut, K.A. King-Pospisil, M.T. Bardo, CNS Drug Rev. 12(3–4), 178 (2006)
H.J. Aubin, A. Luquiens, I. Berlin, Br. J. Clin. Pharmacol. 77(2), 324 (2014)
A.R. Masters, M. McCoy, D.R. Jones, Z. Desta, J. Chromatogr. B. 1015, 201 (2016)
D.H.K. Reddy, Y.S. Yun, Coord. Chem. Rev. 315, 90 (2016)
K.K. Loboz, A.S. Gross, J. Ray, A.J. McLachlan, J. Chromatogr. B. 823(2), 115 (2005)
M. Castro-Puyana, M.Á. García, M.L., J. Chromatogr. B. 875(1), 260 (2008)
S. Jafari, M. Dehghani, N. Nasirizadeh, M. Azimzadeh, F.D. Banadaki, Bull. Mater. Sci. 44(1), 1 (2021)
I. Halkevych, L. Ivanauskas, Y. Bidnychenko, Z. Barsteigiene, Chem. Chem. Technol. 9(2), 245 (2015)
S.A. Abdel-Gawad, R.M. El-Gamal, Saudi Pharma. J. 26(2), 169 (2018)
K.K. Kefeni, B.B. Mamba, T.A.M. Msagati, Sep. Purif. Technol. 188, 399 (2017)
J. Gómez-Pastora, E. Bringas, I. Ortiz, Biochem. Eng. J. 256, 187 (2014)
J. Gómez-Pastora, S. Dominguez, E. Bringas, M.J. Rivero, I. Ortiz, D.D. Dionysiou, Chem. Eng. J. 310, 407 (2017)
S. Lata, S.R. Samadder, J. Environ. Manage. 166, 387 (2016)
D. Ramimoghadam, S. Bagheri, S.B. Abd Hamid, Colloids Surf. 133, 388–411 (2015)
K. Kalantari, M.B. Ahmad, K. Shameli, M.Z.B. Hussein, R. Khandanlou, H. Khanehzaei, J. Nanomater. 2014, 181 (2015)
L. Chen, C.H. Zhou, S. Fiore, D.S. Tong, H. Zhang, C.S. Li, S.F. Ji, W.H. Yu, Appl. Clay Sci. 127–128, 143 (2016)
B. Peng, T. Song, T. Wang, L. Chai, W. Yang, X. Li, C. Li, H. Wang, Chem. Eng. J. 299, 15 (2016)
C. Cha, S.R. Shin, N. Annabi, M.R. Dokmeci, A. Khademhosseini, ACS Nano 7(4), 2891 (2013)
R. Sitko, B. Zawisza, E. Malicka, TrAC-Trends. Anal. Chem. 51, 33 (2013)
M. Tabrizchi, V. ILbeigi, J. hazard. Mater. 176(1–3), 692 (2010)
T. Keller, A. Keller, E. Tutsch-Bauer, F. Monticelli 161(2–3), 130 (2006)
W.S. Jr Hummers, R.E. Offeman, J. Amer. Chem. Soc. 80(6), 1339 (1958)
K. Wu, C. Jing, J. Zhang, T. Liu, S. Yang, W. Wang, Appl. Surf. Sci. 466, 746 (2019)
M. Safari, M. Shahlaei, Y. Yamini, M. Shakorian, E. Arkan, Anal. Chim. Acta 1034, 204 (2018)
T.M. Alshammari, A.A. Al-Hassan, T.B. Hadda, M. Aljofan, Saudi Pharm. J. 23(6), 689 (2015)
S. Liu, Q. Xu, S. Latthe, A. Gurav, R. Xing, R.S.C. Adv. 5, 68293 (2015)
Y. Jain, M. Kumari, R.P. Singh, D. Kumar, R. Gupta, Catal. Lett. 150(4), 1142 (2020)
A.Q. Alorabi, M.S. Hassan, M. Azizi, Arab. J. Chem. 13(11), 8080 (2020)
S. Stankovich, R.D. Piner, S.T. Nguyen, R.S. Ruoff, Carbon 44(15), 3342 (2006)
M. Kidwai, V. Bansal, N.K. Mishra, A. Kumar, S. Mozumdar, Synlett 2007(10), 1581 (2007)
T. Khayamian, M. Tabrizchi, M.T. Jafari, Talanta 69, 795 (2006)
Y. Valadbeigi, V. Ilbeigi, A. Afgar, M. Soleimani, Int. J. Mass Spectrom. 470, 116699 (2021)
T. Sun, M. Mujahid Ali, D. Wang, Z. Du, J. Chromatogr. A. 1610, 460547 (2020)
W. Stumm, J. Morgan, Particle-particle interaction: colloids, coagulation, and filtration Aquatic Chemistry, 3rd edn. (John Wiley, New York, 1996), p.818
Z. Ren, G. Zhang, J.P. Chen, J. Colloid Interf. Sci. 358(1), 230 (2011)
B. Shao, Y. Guan, Z. Tian, X. Guan, D. Wu, Colloids Surfac. A. 506, 703 (2016)
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This work was financially supported by Yazd Branch, Islamic Azad University (IAU), Yazd, Iran.
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Shamsi, F., Sheibani, A. & Shishehbore, M.R. Determination of bupropion by off-line coupling Fe3O4@CuO&GO nanocomposite and ion mobility spectrometry with application to biological samples. ANAL. SCI. 39, 1521–1529 (2023). https://doi.org/10.1007/s44211-023-00371-z
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DOI: https://doi.org/10.1007/s44211-023-00371-z