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Effects of processing temperature and number of passes on the microstructure and mechanical properties of AA 6063 processed by cyclic expansion extrusion

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Abstract

The effects of the working temperatures (260 °C, 200 °C and 130 °C) on microstructure formation in the AA 6063 alloy, processed upto ten passes by cyclic expansion extrusion (CEE) was studied. The microstructures of the CEE-processed specimens in the convergent and extrusion regions (center and edge) were examined after every two passes. The EBSD analysis revealed a decrease in the average grain size from 22 ± 5 µm to 2 ± 0.5 µm after four passes, with a simultaneous presence of a large fraction of HAGBs (45%) at 130 °C processing temperature. The TEM observations also confirmed the presence of nano-grains of sizes in the range of 50–100 nm. The CEE-processed specimen showed the highest improvement in hardness and ultimate tensile strength from 38 ± 3.4 HV and 118 ± 6 MPa to 122 ± 1 HV and 267 ± 2 MPa, respectively, after four passes at 130 °C. The specimens processed at 260 °C (ten passes), and 200 °C (four passes) showed moderate improvement in strength of 184 ± 3 MPa and 216 ± 3 MPa, respectively. On further straining (at 200 °C and 130 °C after six to ten passes), continuous dynamic recovery and dynamic re-crystallization took place which led to grain growth during SPD and, as a result, the alloy lost its strain hardening capacity and there was a decrease in the mechanical properties. At higher number of passes, the grains were elongated and coarsened, i.e., a non-equiaxed microstructure was seen after ten passes at 200 °C and 130 °C. In contrast, the specimen processed at 260 °C after ten passes, showed a homogeneous microstructure with near-equiaxed grains with 38% of HAGBs. A lower processing temperature produced a microstructure with a fine grain size distribution after a lower number of passes.

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References

  1. Sert A, Gürgen S, Çelik QN, Kuşhan MC. Effect of heat treatment on the bending behavior of aluminum alloy tubes. J Mech Sci Technol. 2017;31:5273–8.

    Article  Google Scholar 

  2. Babu V, Shanmugavel BP, Padmanabhan KA. On the microstructural homogeneity and mechanical properties of Al 6063 alloy processed by the cyclic expansion extrusion process. J Mater Eng Perform. 2020;29:6870–80. https://doi.org/10.1007/s11665-020-05151-8.

    Article  CAS  Google Scholar 

  3. Zhu YT, Lowe TC, Langdon TG. Performance and applications of nanostructured materials produced by severe plastic deformation. Scr Mater. 2004;51:825–30.

    Article  CAS  Google Scholar 

  4. Bay B, Hansen N, Hughes DA, Kuhlmann-Wilsdorf D. Overview no. 96 evolution of fcc deformation structures in polyslip. Acta Metall Mater. 1992;40:205–19.

    Article  ADS  CAS  Google Scholar 

  5. Hughes DA, Hansen N. High angle boundaries formed by grain subdivision mechanisms. Acta Mater. 1997;45:3871–86.

    Article  ADS  CAS  Google Scholar 

  6. Liu Q, Jensen DJ, Hansen N. Effect of grain orientation on deformation structure in cold-rolled polycrystalline aluminium. Acta Mater. 1998;46:5819–38.

    Article  ADS  CAS  Google Scholar 

  7. Panigrahi SK, Jayaganthan R, Pancholi V. Effect of plastic deformation conditions on microstructural characteristics and mechanical properties of Al 6063 alloy. Mater Des. 2009;30:1894–901.

    Article  CAS  Google Scholar 

  8. Valiev RZ, Langdon TG. Principles of equal-channel angular pressing as a processing tool for grain refinement. Prog Mater Sci. 2006;51:881–981.

    Article  CAS  Google Scholar 

  9. Mazurina I, Sakai T, Miura H, Sitdikov O, Kaibyshev R. Effect of deformation temperature on microstructure evolution in aluminum alloy 2219 during hot ECAP. Mater Sci Eng A. 2008;486:662–71.

    Article  Google Scholar 

  10. Das M, Das G, Ghosh M, Wegner M, Rajnikant V, GhoshChowdhury S, Pal TK. Microstructures and mechanical properties of HPT processed 6063 Al alloy. Mater Sci Eng A. 2012;558:525–32.

    Article  CAS  Google Scholar 

  11. Rao PN, Singh D, Jayaganthan R. Mechanical properties and microstructural evolution of Al 6061 alloy processed by multidirectional forging at liquid nitrogen temperature. Mater Des. 2014;56:97–104.

    Article  CAS  Google Scholar 

  12. Lee SH, Saito Y, Sakai T, Utsunomiya H. Microstructures and mechanical properties of 6061 aluminum alloy processed by accumulative roll-bonding. Mater Sci Eng A. 2002;325:228–35.

    Article  Google Scholar 

  13. Estrin Y, Vinogradov A. Extreme grain refinement by severe plastic deformation: a wealth of challenging science. Acta Mater. 2013;61:782–817.

    Article  ADS  CAS  Google Scholar 

  14. Babu V, Shanmugavel BP, Padmanabhan KA. On the influence of strain rate and number of passes on grain refinement in Al-Mg-Si alloy processed by cyclic expansion extrusion. J Mater Eng Perform. 2020. https://doi.org/10.1007/s11665-020-05264-0.

    Article  Google Scholar 

  15. Lianxi H, Yuping L, Erde W, Yang Y. Ultrafine grained structure and mechanical properties of a LY12 Al alloy prepared by repetitive upsetting-extrusion. Mater Sci Eng A. 2006;422:327–32.

    Article  Google Scholar 

  16. Zendehdel H, Hassani A. Influence of twist extrusion process on microstructure and mechanical properties of 6063 aluminum alloy. Mater Des. 2012;37:13–8.

    Article  CAS  Google Scholar 

  17. Babu V, Shanmugavel BP, Padmanabhan KA. On the influence of temperature and number of passes on the mechanical properties of an Al–Mg alloy processed by cyclic expansion extrusion. Met Mater Int. 2020. https://doi.org/10.1007/s12540-020-00781-y.

    Article  Google Scholar 

  18. Sitdikov O, Sakai T, Miura H, Hama C. Temperature effect on fine-grained structure formation in high-strength Al alloy 7475 during hot severe deformation. Mater Sci Eng A. 2009;516:180–8.

    Article  Google Scholar 

  19. Thangapandian N, Prabu SB, Padmanabhan KA. Effect of temperature and velocity of pressing on grain refinement in AA5083 aluminum alloy during repetitive corrugation and straightening process. Metall Mater Trans A. 2016;47:6374–83.

    Article  CAS  Google Scholar 

  20. Pardis N, Talebanpour B, Ebrahimi R, Zomorodian S. Cyclic expansion-extrusion (CEE): a modified counterpart of cyclic extrusion-compression (CEC). Mater Sci Eng A. 2011;528:7537–40.

    Article  CAS  Google Scholar 

  21. Pardis N, Chen C, Shahbaz M, Ebrahimi R, Toth LS. Development of new routes of severe plastic deformation through cyclic expansion–extrusion process. Mater Sci Eng A. 2014;613:357–64.

    Article  CAS  Google Scholar 

  22. Babu V, Balasivanandha Prabu S, Padmanabhan KA. Microstructure homogeneity in AA6063 alloy processed by cyclic expansion extrusion. Defect Diffus Forum. 2018;385:223–7.

    Article  Google Scholar 

  23. Málek P, Cieslar M, Islamgaliev RK. The influence of ECAP temperature on the stability of Al–Zn–Mg–Cu alloy. J Alloys Comp. 2004;378:237–41.

    Article  Google Scholar 

  24. Yamashita A, Yamaguchi D, Horita Z, Langdon TG. Influence of pressing temperature on microstructural development in equal-channel angular pressing. Mater Sci Eng A. 2000;287:100–6.

    Article  Google Scholar 

  25. Goloborodko A, Sitdikov O, Kaibyshev R, Miura H, Sakai T. Effect of pressing temperature on fine-grained structure formation in 7475 aluminum alloy during ECAP. Mater Sci Eng A. 2004;381:121–8.

    Article  Google Scholar 

  26. Wang YY, Sun PL, Kao PW, Chang CP. Effect of deformation temperature on the microstructure developed in commercial purity aluminum processed by equal channel angular extrusion. Scr Mater. 2004;50:613–7.

    Article  CAS  Google Scholar 

  27. Shaeri MH, Shaeri M, Ebrahimi M, Salehi MT, Seyyedein SH. Effect of ECAP temperature on microstructure and mechanical properties of Al–Zn–Mg–Cu alloy. Prog Nat Sci Mater Int. 2016;26:182–91.

    Article  CAS  Google Scholar 

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Acknowledgements

The authors thank Prof. Indradev Samajdar, IIT Bombay, for extending the use of the EBSD facility. The authors also acknowledge the help of PSG College of Technology, Coimbatore, India for making available the TEM facility for this work.

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This research received no specific grant from any funding agency in the public, commercial or not-for profit sectors.

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Babu, V., Shanmugavel, B.P. & Padmanabhan, K.A. Effects of processing temperature and number of passes on the microstructure and mechanical properties of AA 6063 processed by cyclic expansion extrusion. Archiv.Civ.Mech.Eng 21, 38 (2021). https://doi.org/10.1007/s43452-020-00160-9

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