Skip to main content
Log in

Nuclear Magnetic Resonance Study on Concrete Pore Structure Evolution Under Different Curing Environments

  • Advances in Characterization of Functional Composite Materials
  • Published:
JOM Aims and scope Submit manuscript

Abstract

This study aimed to investigate the influence of environmental conditions on the evolution of concrete pore structures. Nuclear magnetic resonance technology was used to test the pore parameters of concrete under various curing conditions as well as to examine the meso-evolution process of concrete pore distribution with age. The results of the study indicated a similarity in the overall trend under different curing conditions. The pores were classified into four parts: micropores, mesopores, macropores, and microcracks. The test results of the T2 spectrum area showed that the hydration reaction in the concrete decreased with decreasing curing temperature and humidity. Additionally, the results showed that the pore volume proportion primarily remained unchanged. Finally, the fractal dimension was calculated using fractal theory, which showed that concrete has multi-fractal characteristics under different curing conditions and that low water-binder ratio (w/b) can increase the pore complexity of the concrete.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2

Similar content being viewed by others

References

  1. J. Ortiz, A. Aguado, L. Agulló, and T. Garcia, Cem Concr Res. 35, 1970 (2005)

    Article  Google Scholar 

  2. M. Du, X. Jin, H. Ye, N, Jin and Y. Tian, Constr Build Mater. 111, 689 (2016)

  3. C. Li, M. Wu, Q. Chen, and Z. Jiang, Cem Concrete Comp. 86, 139 (2018)

    Article  Google Scholar 

  4. J.M. Davila, A.M. Sarmiento, J.C. Fortes, M. Santisteban and J.A. Grande, Constr Build Mater. 269, 121817 (2021)

  5. V. Kodur and S. Banerji, Cem Concrete Comp. 117, 103902 (2021)

  6. Y. Qin, X.W. Zhang, J.R. Chai, Z.G. Xu, and S.Y. Li, Constr Build Mater. 194, 216 (2019)

    Article  Google Scholar 

  7. R. Wang, N. Yu and Y. Li, Constr Build Mater. 242, 118164 (2020)

  8. Y. Li, J. Chen, J. Wang, and K. Li, J Mater Civil Eng. 33, 04020441 (2021)

    Article  Google Scholar 

  9. Z. Liu, A. Sha, L. Hu, W. Jiao, Z. Tong, and J. Gao, Chem Pap. 71, 741 (2017)

    Article  Google Scholar 

  10. J. Liu, Y. Li, P. Ouyang, and Y. Yang, Constr Build Mater. 93, 919 (2015)

    Article  Google Scholar 

  11. R. Demirboğa, F. Karagöl, R. Polat, and M.A. Kaygusuz, Constr Build Mater. 64, 114 (2014)

    Article  Google Scholar 

  12. L. Xu, P. Wang, and G. Zhang, Constr Build Mater. 31, 347 (2012)

    Article  Google Scholar 

  13. W. Saengsoy, T. Nawa, and P. Termkhajornkit, J Struct Constr Eng. 73, 1433 (2008)

    Article  Google Scholar 

  14. J.M. Khatib and P.S. Mangat, Cem Concr Res. 32, 1743 (2002)

    Article  Google Scholar 

  15. Z. Mi, Y. Hu, Q. Li, X. Gao, and T. Yin, Constr Build Mater. 169, 403 (2018)

    Article  Google Scholar 

  16. I.G. Mathews, K. Dalesandro, M. Young and M. Soliman, Constr Build Mater. 280, 122545 (2021)

  17. T.C. Powers, Proceedings of the 4th International Symposium on the Chemistry of Cement (1960)

  18. I. Maruyama and G. Igarashi, J Adv Concr Technol. 12, 200 (2014)

    Article  Google Scholar 

  19. C.S. Poon, S.C. Kou, and L. Lam, Constr Build Mater. 20, 858 (2006)

    Article  Google Scholar 

  20. A.M. Gajewicz-Jaromin, P.J. McDonald, A.C. Muller, and K.L. Scrivener, Cem Concr Res 122, 147 (2019)

    Article  Google Scholar 

  21. H. Zhao, X. Qin, J. Liu, L. Zhou, Q. Tian, and P. Wang, Constr Build Mater. 189, 934 (2018)

    Article  Google Scholar 

  22. R.S. Holthausen and M. Raupach, Cem Concr Res. 111, 138 (2018)

    Article  Google Scholar 

  23. N. Li, N. Farzadnia, and C. Shi, Cem Concr Res. 100, 214 (2017)

    Article  Google Scholar 

  24. S. Xue, F. Meng, P. Zhang, J. Bao, J. Wang and K. Zhao, Constr Build Mater. 262, 120532 (2020)

  25. C. Nunes, L. Pel, J. Kunecký, and Z. Slížková, Constr Build Mater. 142, 395 (2017)

    Article  Google Scholar 

  26. M. Gussoni, F. Greco, F. Bonazzi, A. Vezzoli, D. Botta, G. Dotelli, I.N. Sora, R. Pelosato, and L. Zetta, Magn Reson Imaging. 22, 877 (2004)

    Article  Google Scholar 

  27. E, Grunewald and R. Knight, Geophysics. 74, 215 (2009)

  28. M. Fourmentin, P. Faure, S. Rodts, U. Peter, D. Lesueur, D. Daviller, and P. Coussot, Cem Concr Res. 95, 56 (2017)

    Article  Google Scholar 

  29. J.Z. Zhang, J. Guo, D.H. Li, Y.R. Zhang, F. Bian, and Z.F. Fang, Ocean Eng. 142, 94 (2017)

    Article  Google Scholar 

  30. L. Liu, Z. He, X. Cai, and S. Fu, Appl Magn Reson. 52, 15 (2020)

    Article  Google Scholar 

  31. Y. Yang, B. Chen, W. Zeng, Y. Li, Q. Chen, and W. Guo, Int J Concr Struct M. 15, 1 (2021)

    Article  Google Scholar 

  32. S.C. Kou, C.S. Poon, and M. Etxeberria, Cem Concrete Comp. 33, 286 (2011)

    Article  Google Scholar 

  33. GB/T 14902-2002, Standard for Test Method of Mechanical Properties on Ordinary Concrete, China (2002) (in Chinese)

  34. L. Li and Y. Zhang, Sci Total Environ. 615, 875 (2018)

    Article  Google Scholar 

  35. F. Shi, C. Zhao, X. Zhou, and X. Li, Asia-Pac J Atmos Sci. 55, 221 (2019)

    Article  Google Scholar 

  36. D. Chen, W. Liu, F. Huang, Q. Li, F. Uchenna-Ochege, and L. Li, J Arid Land. 12, 397 (2020)

    Article  Google Scholar 

  37. GB/T50081-2002, Standard for Test Method of Mechanical Properties on Ordinary Concrete, China (2002) (in Chinese)

  38. B.T. Tamtsia and J.J. Beaudoin, Cem Concr Res. 30, 1465 (2000)

    Article  Google Scholar 

  39. W.P. Halperin, S. Bhattacharja, and F. D’Orazio, Magn Reson Iaging. 9, 733 (1991)

    Article  Google Scholar 

  40. F. Xu, S. Wang, T. Li, B. Liu, B. Li and Y. Zhou, J Build Eng. 33, 101572 (2021)

  41. Y. Li, R. Wang, S. Li, Y. Zhao, and Y. Qin, Constr Build Mater. 166, 23 (2018)

    Article  Google Scholar 

  42. J. Liu, C. Shi, N. Farzadnia, and X. Ma, Constr Build Mater. 204, 276 (2019)

    Article  Google Scholar 

  43. P. Suwanmaneechot, A. Aili, I. Maruyama, Cem Concr Res. 132, 106036 (2020)

  44. Z. Ouyang, D. Liu, Y. Cai, and Y. Yao, Energ Fuel. 30, 5449 (2016)

    Article  Google Scholar 

  45. S. Zhou, D. Liu, Y. Cai, and Y. Yao, Fuel 181, 218 (2016)

    Article  Google Scholar 

  46. S. Qiu, M. Yang, P Xu and B. Rao, J Hydrol. 586, 124890 (2020)

  47. J.H. Hu, Q.F. Ren, D.J. Yang, J.L. Shang, X.T. Ding, and Z.Q. Luo, T Nonferrr Metal Soc. 30, 1347 (2020)

    Article  Google Scholar 

  48. M. Gerstig and L. Wadsö, Cem Concr Res. 40, 867 (2010)

    Article  Google Scholar 

  49. R.G. Patel, D.C. Killoh, L.J. Parrott, and W.A. Gutteridge, Mater Struct. 21, 192 (1988)

    Article  Google Scholar 

  50. S.N. Shoukry, G.W. William, B. Downie, and M.Y. Riad, Constr Build Mater. 25, 688 (2011)

    Article  Google Scholar 

Download references

Funding

The authors acknowledge the National Natural Science Foundation of China (No. 52079109) and Doctoral Dissertation Innovation Fund of Xi’an University of Technology (No. 252072009) and editors and reviewers for their hard work.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Yanlong Li.

Ethics declarations

Conflict of interest

The authors declare that they have no conflict of interest

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Supplementary Information

Below is the link to the electronic supplementary material.

Supplementary file1 (PDF 1782 kb)

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Chen, J., Li, Y., Zhou, H. et al. Nuclear Magnetic Resonance Study on Concrete Pore Structure Evolution Under Different Curing Environments. JOM 74, 1819–1827 (2022). https://doi.org/10.1007/s11837-022-05221-3

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11837-022-05221-3

Navigation