Abstract
Gardenia yellow pigment (GYP) loaded alginate beads were prepared by the ionic gelation technique, and the preparation parameters were optimized by response surface methodology for high encapsulation efficiency. The optimized parameters were alginate concentration of 3.3%, CaCl2 concentration of 2.4%, and GYP concentration of 3.2 mg/mL, under which the encapsulation efficiency was 73.61%. The surface morphology and bead size analysis showed that the GYP-loaded alginate beads had a roughly spherical morphology with a wrinkled surface, and their average diameter was 0.87 mm. In vitro release test revealed that the GYP release had a pH-dependent release profile and a two-step release process. The Rigter-Peppas model was the most proper model to assess the GYP release from alginate beads. The release mechanism of GYP at pH 1.2 and 7.4 was non-Fickian transport and case-II transport, respectively. The 2,2-diphenyl-1-picrylhydrazyl assay indicated that the encapsulated GYP had effectively maintained 82.56% of the antioxidant activity.
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This work was financially supported by the University Student Innovation and Entrepreneurship Training Program of Guangdong Province (No. 201610580058).
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Liu, Y., Zhou, Q., He, YM. et al. Optimization of preparation and properties of Gardenia yellow pigment-loaded alginate beads. Korean J. Chem. Eng. 38, 1669–1675 (2021). https://doi.org/10.1007/s11814-021-0807-3
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DOI: https://doi.org/10.1007/s11814-021-0807-3