Abstract
The present work aimed to assess the combination of the use of an empirical-statistical model and design of experiments (DoE) to minimally validate the geometrical characteristics (dilution, coating height, waviness and porosity) of a laser-induced Inconel 625 coating on AISI 316L substrate. Employing the estimated laser processing parameters, a verification coating was deposited to assess its microstructure, microhardness and bending resistance. The statistical model showed to be an efficient computational tool for the planning of the design of experiments (DoE), resulting in errors less than 15% for all geometrical characteristics evaluated. The presence of some pores along the verification Inconel 625 coating was observed. Additionally, the verification coating showed good dilution and low waviness. Regarding the microstructure and microhardness, the verification coating showed a columnar dendritic microstructure, and its microhardness was about 110% higher than that observed for the AISI 316L substrate. Its resistance to bending was 30% higher when compared to that of the uncoated samples. By considering the experimental conditions explored within this work, one can state that the laser-cladded Inconel 625 coatings performed well on AISI 316L stainless steel substrate.











Similar content being viewed by others
Explore related subjects
Discover the latest articles and news from researchers in related subjects, suggested using machine learning.References
M. Alizadeh-Sh, S.P.H. Marashi, E. Ranjbarnodeh, R. Shoja-Razavi and J.P. Oliveira, Dissimilar Laser Cladding of Inconel 718 Powder on A-286 Substrate: Microstructural Evolution, J. Laser Appl., 2020, 32, 022048. https://doi.org/10.2351/1.5124932
W. Yuan, R. Li, Z. Chen, J. Gu and Y. Tian, A Comparative Study on Microstructure and Properties of Traditional Laser Cladding and High-speed Laser Cladding of Ni45 Alloy Coatings, Surf. Coatings Technol., 2021, 405, 126582. https://doi.org/10.1016/j.surfcoat.2020.126582
L. Zhu, S. Wang, H. Pan, C. Yuan and X. Chen, Research on Remanufacturing Strategy for 45 Steel Gear Using H13 Steel Powder Based on Laser Cladding Technology, J. Manuf. Process., 2020, 49, p 344–354. https://doi.org/10.1016/j.jmapro.2019.12.009
C. Chen, G. Lian, J. Jiang and Q. Wang, Simplification and Experimental Investigation of Geometrical surface smoothness model for multi-track laser cladding processes, J. Manuf. Process., 2018, 36, p 621–628. https://doi.org/10.1016/j.jmapro.2018.11.004
F. Weng, C. Chen and H. Yu, Research Status of Laser Cladding on titanium and its Alloys: A Review, Mater. Des., 2014, 58, p 412–425. https://doi.org/10.1016/j.matdes.2014.01.077
L. Song, G. Zeng, H. Xiao, X. Xiao and S. Li, Repair of 304 Stainless Steel by Laser Cladding with 316L Stainless Steel Powders Followed by Laser Surface Alloying with WC Powders, J. Manuf. Process., 2016, 24, p 116–124. https://doi.org/10.1016/j.jmapro.2016.08.004
R.A. Rahman Rashid, C.J. Barr, S. Palanisamy, K.A. Nazari, N. Orchowski, N. Matthews and M.S. Dargusch, Effect of Clad Orientation on the Mechanical Properties of Laser-clad Repaired Ultra-high Strength 300 M Steel, Surf. Coat. Technol., 2019, 380, p 125090.
Y. Sun and M. Hao, Statistical Analysis and Optimization of Process Parameters in Ti6Al4V Laser Cladding Using Nd: YAG Laser Opt. Lasers Eng., 2012, 50, p 985–995. https://doi.org/10.1016/j.optlaseng.2012.01.018
F. Weng, H. Yu, C. Chen, J. Liu, L. Zhao and J. Dai, Effect of Process Parameters on the Microstructure Evolution and Wear Property of the Laser Cladding Coatings on Ti-6Al-4V alloy, J. Alloys Compd., 2016 https://doi.org/10.1016/j.jallcom.2016.09.071
H. El Cheikh, B. Courant, J.Y. Hascoët and R. Guillén, Prediction and Analytical Description of the Single Laser Track Geometry in Direct Laser Fabrication from Process Parameters and Energy Balance Reasoning, J. Mater. Process. Technol., 2012, 212, p 1832–1839. https://doi.org/10.1016/j.jmatprotec.2012.03.016
C. Chen, X. Zeng, Q. Wang, G. Lian, X. Huang and Y. Wang, Statistical Modelling and Optimization of Microhardness Transition Through Depth of Laser Surface Hardened AISI 1045 Carbon Steel, Opt. Laser Technol., 2020, 124, 105976. https://doi.org/10.1016/j.optlastec.2019.105976
P. Shayanfar, H. Daneshmanesh and K. Janghorban, Parameters Optimization for Laser Cladding of Inconel 625 on ASTM A592 Steel, J. Mater. Res. Technol., 2020, 9, p 8258–8265. https://doi.org/10.1016/j.jmrt.2020.05.094
Y. Zhao, C. Guan, L. Chen, J. Sun and T. Yu, Effect of Process Parameters on the Cladding Track Geometry Fabricated by Laser Cladding, Optik (Stuttg)., 2020, 223, 165447. https://doi.org/10.1016/j.ijleo.2020.165447
M. Alizadeh-Sh, S.P.H. Marashi, E. Ranjbarnodeh and R. Shoja-Razavi, Laser Cladding of Inconel 718 Powder on a Non-weldable Substrate: Clad Bead Geometry-Solidification Cracking Relationship, J. Manuf. Process., 2020, 56, p 54–62. https://doi.org/10.1016/j.jmapro.2020.04.045
T. Yu, L. Yang, Y. Zhao, J. Sun and B. Li, Experimental Research and Multi-response Multi-parameter Optimization of Laser Cladding Fe313, Opt. Laser Technol., 2018, 108, p 321–332. https://doi.org/10.1016/j.optlastec.2018.06.030
J.T. Pacheco, L.J. da Silva, L.D. Barbetta, H.S. Ferreira, M.T. Veiga, R. Forni and M.F. Teixeira, Laser Cladding of Stellite-6 on AISI 316 L Austenitic Stainless Steel: Empirical-Statistical Modeling and Parameter Optimization, Lasers Manuf. Mater. Process., 2020 https://doi.org/10.1007/s40516-020-00132-0
C. Zhong, J. Chen, S. Linnenbrink, A. Gasser, S. Sui and R. Poprawe, A Comparative Study of Inconel 718 Formed by High Deposition Rate Laser Metal Deposition with GA Powder and PREP Powder, Mater. Des., 2016, 107, p 386–392. https://doi.org/10.1016/j.matdes.2016.06.037
S.E. Aghili and M. Shamanian, Investigation of Powder Fed Laser Cladding of NiCr-Chromium Carbides Single-Tracks on Titanium Aluminide Substrate, Opt. Laser Technol., 2019, 119, 105652. https://doi.org/10.1016/j.optlastec.2019.105652
Y. Javid, Multi-response Optimization in Laser Cladding Process of WC Powder on Inconel 718, CIRP J. Manuf. Sci. Technol., 2020, 31, p 406–417. https://doi.org/10.1016/j.cirpj.2020.07.003
M. Zhang, G.L. Zhao, X.H. Wang, S.S. Liu and W.L. Ying, Microstructure Evolution and Properties of In-situ Ceramic Particles Reinforced Fe-based Composite Coating Produced by Ultrasonic Vibration Assisted Laser Cladding Processing, Surf. Coatings Technol., 2020, 403, 126445. https://doi.org/10.1016/j.surfcoat.2020.126445
M. Alizadeh-Sh, S.P.H. Marashi, E. Ranjbarnodeh, R. Shoja-Razavi and J.P. Oliveira, Prediction of Solidification Cracking by an Empirical-Statistical Analysis for Laser Cladding of Inconel 718 Powder on a Non-weldable Substrate, Opt. Laser Technol., 2020, 128, 106244. https://doi.org/10.1016/j.optlastec.2020.106244
J.G. Lopes, C.M. Machado, V.R. Duarte, T.A. Rodrigues, T.G. Santos and J.P. Oliveira, Effect of Milling Parameters on HSLA Steel Parts Produced by Wire and Arc Additive Manufacturing (WAAM), J. Manuf. Process., 2020, 59, p 739–749. https://doi.org/10.1016/j.jmapro.2020.10.007
L. Reddy, S.P. Preston, P.H. Shipway, C. Davis and T. Hussain, Process Parameter Optimisation of Laser Clad Iron based Alloy: Predictive Models of Deposition Efficiency, Porosity and Dilution, Surf. Coatings Technol., 2018, 349, p 198–207. https://doi.org/10.1016/j.surfcoat.2018.05.054
X. Zhan, C. Qi, Z. Gao, D. Tian and Z. Wang, The Influence of Heat Input on Microstructure and Porosity during Laser Cladding of Invar Alloy, Opt. Laser Technol., 2019, 113, p 453–461. https://doi.org/10.1016/j.optlastec.2019.01.015
T.E. Abioye, J. Folkes and A.T. Clare, A Parametric Study of Inconel 625 Wire Laser Deposition, J. Mater. Process. Technol., 2013, 213, p 2145–2151. https://doi.org/10.1016/j.jmatprotec.2013.06.007
H. Liu, J. Hao, Z. Han, G. Yu, X. He and H. Yang, Microstructural Evolution and Bonding Characteristic in Multi-layer Laser Cladding of NiCoCr Alloy on Compacted Graphite Cast Iron, J. Mater. Process. Technol., 2016, 232, p 153–164. https://doi.org/10.1016/j.jmatprotec.2016.02.001
N. Jeyaprakash, C.H. Yang and S.P. Tseng, Characterization and Tribological Evaluation of NiCrMoNb and NiCrBSiC Laser Cladding on Near-α Titanium Alloy, Int. J. Adv. Manuf. Technol., 2020, 106, p 2347–2361. https://doi.org/10.1007/s00170-019-04755-2
K. Feng, Y. Chen, P. Deng, Y. Li, H. Zhao, F. Lu, R. Li, J. Huang and Z. Li, Improved High-temperature Hardness and Wear Resistance of Inconel 625 Coatings Fabricated by Laser Cladding, J. Mater. Process. Technol., 2017, 243, p 82–91. https://doi.org/10.1016/j.jmatprotec.2016.12.001
T.E. Abioye, P.K. Farayibi and A.T. Clare, A Comparative Study of Inconel 625 Laser Cladding by Wire and Powder Feedstock, Mater. Manuf. Process., 2017, 32, p 1653–1659. https://doi.org/10.1080/10426914.2017.1317787
D. Verdi, M.A. Garrido, C.J. Múnez and P. Poza, Mechanical Properties of Inconel 625 Laser Cladded Coatings: Depth Sensing Indentation Analysis, Mater. Sci. Eng. A, 2014, 598, p 15–21. https://doi.org/10.1016/j.msea.2014.01.026
Z. Li, H. Zhao, Y. Gu, M. Zhong, B. Zhang, H. Zhang, W. Liu, Z. Ren, M. Yang and H. Lin, Fatigue Crack Propagation in Laser Alloyed Ductile Cast Iron Surface, J. Laser Appl., 2013, 25, 012003. https://doi.org/10.2351/1.4773250
Acknowledgments
The authors would like to thank the Agência Nacional do Petróleo, Gás Natural e Biocombustíveis (ANP) and the Empresa Brasileira de Pesquisa e Inovação Industrial (EMBRAPII) for funding the present applied research project focused on digital additive manufacturing for the oil & gas industry. The authors also acknowledge both the Petróleo Brasileiro S.A. (PETROBRAS) and the SENAI Innovation Institute in Manufacturing Systems and Laser Processing for providing the laboratorial infrastructure, target industrial components, as well as all the technical support in the scope of this work.
Author information
Authors and Affiliations
Corresponding author
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Bloemer, P.R.A., Pacheco, J.T., Cunha, A. et al. Laser Cladding of Inconel 625 on AISI 316L: Microstructural and Mechanical Evaluation of Parameters Estimated by Empirical-Statistical Model. J. of Materi Eng and Perform 31, 211–220 (2022). https://doi.org/10.1007/s11665-021-06147-8
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-021-06147-8