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Investigation of Properties of Powder Injection-Molded Steatites

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Abstract

In this study, the mechanical and micro-structural properties of injection-molded steatites were investigated experimentally. Initially, steatite powders and binders of polyethylene glycol (PEG), polypropylene (PP), and stearic aside (SA) were mixed to prepare the feedstock. The mixing powders were granulated using the extruder. The short granules in cylindrical shapes were used as the feedstock in the injection-molding operations. Solvent- and thermal-debinding processes were applied to the green samples after the molding. The samples were sintered at 1300 °C for 4 h, and a theoretical density of 98-99% was achieved. Three-point bending and tensile tests were performed on the samples which were sintered at 1200-1300 °C. The maximum three-point bending and tensile strength values were found as 154 and 47 MPa, respectively. The morphology of fractured surface was done by scanning electron microscopy whereas porosity investigations were carried out using the same microscopy. Grain growth and structure on the specimens were also investigated using transmission electron microscopy.

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References

  1. R.M. German, Powder Metallurgy and Particulate Materials Processing, Metal Powder Industries Federation, Princeton, NJ, 2005

  2. M.J. Edirisingle and J.R.G. Evans, Review: Fabrication of Engineering Ceramics by Injection Moulding. II. Tecnigues, Int. J. High Temp. Ceram., 1986, 2, p 249–278

    Article  Google Scholar 

  3. R.M. German, Powder Injection Molding, Metal Powder Industries Federation, Princeton, NJ, 1990

    Google Scholar 

  4. C. Karatas, “Rheology for Feedstocks Used Powder Injection Moulding,” Ph.D. thesis, Gazi University, Ankara, 1997

  5. R.M. German and A. Bose, Injection Molding of Metals and Ceramics, Metal Powder Industries Federation, Princeton, NJ, 1997

  6. R. Zauner, Micro Powder Injection Moulding, Microelectron. Eng., 2006, 83, p 1442–1444

    Article  CAS  Google Scholar 

  7. R.M. German, PIM Breaks the $1 bn Barrier, Met. Powder Rep., 2008, 63(3), p 8–10

    Article  Google Scholar 

  8. C. Karatas and S. Sarıtas, Powder Injection Molding: A High Technology Manufacturing Process, J. Fac. Eng. Archit. Gazi Univ., 1998, 13(2), p 193

    Google Scholar 

  9. L. Urtekin, “Investigation of the Effect of Molding and Sintering Parameters on Properties of Powder Injection Molded Steatite Ceramics,” Ph.D. thesis, Gazi University, Ankara, 2008

  10. C. Karatas, A. Kocer, H.I. Unal, and S. Sarıtas, Rheological Properties of Feedstocks Prepared with Steatite Powder and Polyethylene-Based Thermoplastic Binders, J. Mater. Process. Technol., 2004, 152, p 77–83

    Article  CAS  Google Scholar 

  11. C. Karatas, M. Gokten, H.I. Unal, S. Sarıtas, and I. Uslan, Investigation of Reological Properties of the Feedstocks Composed of Steatite and 316L Stainless Steel Powder and PEG Based Resins, Euro PM, 2005, p 367–373

  12. W. Mielcarek, D.N. Wozny, and K. Prociow, Correlation Between MgSiO3 Phases and Mechanical Durability of Steatite Ceramics, J. Eur. Ceram. Soc., 2004, 24, p 3817–3821

    Article  CAS  Google Scholar 

  13. C.F. Yang and C.M. Cheng, The Influence of B2O3 on the Sintering of MgO-CaO-Al2O3-SiO2 Composite Glass Powder, Ceram. Int., 1999, 25(4), p 383–387

    Article  CAS  Google Scholar 

  14. Vogt Ceramic Component “Material properties”, 2008, http://www.vogt-ceramic.de/en/mproperties.htm

  15. E. Vela, M. Peiteado, F. Garcia, A.C. Cabellero, and J.F. Fernandez, Sintering Behaviour of Steatite Materials with Barium Carbonate Flux, Ceram. Int., 2007, 33, p 1325–1329

    Article  CAS  Google Scholar 

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Acknowledgments

The authors are grateful to Prof. Dr. Suleyman Saritas. The authors acknowledge the support of Gazi University (DPT Projects Nos. 2001K120590 and 2003K120470) labs for facilitating the experimental studies.

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Correspondence to L. Urtekin.

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Urtekin, L., Uslan, I. & Tuc, B. Investigation of Properties of Powder Injection-Molded Steatites. J. of Materi Eng and Perform 21, 358–365 (2012). https://doi.org/10.1007/s11665-011-9901-8

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  • DOI: https://doi.org/10.1007/s11665-011-9901-8

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