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Microstructure and Texture Evolution During Sub-Transus Thermo-Mechanical Processing of Ti-6Al-4V-0.1B Alloy: Part II. Static Annealing in (α + β) Regime

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Abstract

The first part of this study describes the evolution of microstructure and texture in Ti-6Al-4V-0.1B alloy during sub-transus rolling vis-à-vis the control alloy Ti-6Al-4V. In the second part, the static annealing response of the two alloys at self-same conditions is compared and the principal micromechanisms are analyzed. Faster globularization kinetics has been observed in the Ti-6Al-4V-0.1B alloy for equivalent annealing conditions. This is primarily attributed to the α colonies, which leads to easy boundary splitting via multiple slip activation in this alloy. The other mechanisms facilitating lamellar to equiaxed morphological transformations, e.g., termination migration and cylinderization, also start early in the boron-modified alloy due to small α colony size, small aspect ratio of the α lamellae, and the presence of TiB particles in the microstructure. Both the alloys exhibit weakening of basal fiber (ND||〈0001〉) and strengthening of prism fiber (RD||〈\( 10\bar{1}0 \)〉) upon annealing. A close proximity between the orientations of fully globularized primary α and secondary α phases during α → β → α transformation has accounted for such a texture modification.

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Notes

  1. JXA-8530F, JEOL, Japan.

References

  1. S. Roy and S. Suwas: Metall. Mater. Trans A, 2013. DOI: 10.1007/s11661-013-1672-4.

  2. G. Lütjering: Mater. Sci. Eng. A, 1998, vol. 243, pp. 32-45.

    Article  Google Scholar 

  3. G. Lütjering: Mater. Sc. Eng. A, 1999, vol. 263, pp. 117-126.

    Article  Google Scholar 

  4. M. Peters, G. Lütjering and G. Ziegler: Z. Metallkd., 1983, vol. 74, pp. 274-82.

    CAS  Google Scholar 

  5. N. Stefansson, S.L. Semiatin and D. Eylon: Metall. Mater. Trans. A, 2002, vol. 33, pp. 3527-3534.

    Article  CAS  Google Scholar 

  6. N. Stefansson and S.L. Semiatin: Metall. Mater. Trans. A, 2003, vol. 34, pp. 691-698.

    Article  CAS  Google Scholar 

  7. S.L. Semiatin, S.L. Knisley, P.N. Fagin, D.R. Barker and F. Zhang: Metall. Mater. Trans. A, 2003, vol. 34, pp. 2377-2386.

    Article  CAS  Google Scholar 

  8. I. Weiss, F.H. Froes, D. Eylon and G.E. Welsch: Metall. Trans. A, 1985, vol. 17, pp. 1935-1947.

    Google Scholar 

  9. S.L. Semiatin, B.C. Kirby and G.A. Salishchev: Metall. Mater. Trans. A, 2004, vol. 35, pp. 2809-2819.

    Article  CAS  Google Scholar 

  10. R.L. Fullman: J. Metals, 1993, vol. 3, pp. 447-452.

    Google Scholar 

  11. S.L. Semiatin, V. Seetharaman and I. Weiss: Mater. Sci. Eng. A, 1999, vol. 263, pp. 257-271.

    Article  Google Scholar 

  12. S. Suwas and A. K. Singh: Mater. Sci. Eng. A, 2003, vol. 355, pp. 331-37.

    Article  Google Scholar 

  13. S. Suwas and A.K. Sing: Metal. Mater. Trans. A, 2004, vol. 35, pp. 925-38.

    Article  CAS  Google Scholar 

  14. S. Suwas, R.K. Ray, A. K. Singh and S. Bhargava: Acta Mater., 1999, vol. 47, pp. 4585-98.

    Article  CAS  Google Scholar 

  15. S. Suwas, A. K. Singh, R.K. Ray and S. Bhargava: Scripta Mater., 1996, vol. 35, pp. 897-02.

    Article  CAS  Google Scholar 

  16. S. Suwas and R. K. Ray: Acta Mater., 1999, vol. 47, pp. 4599-14.

    Article  CAS  Google Scholar 

  17. N.P. Gurao, A. A. Ali and S. Suwas: Mater. Sc. Eng. A, 2009, vol. 504, pp. 24-35.

    Article  Google Scholar 

  18. H. Inagaki: Z. Metallkunde: 1990, vol. 81, pp. 433-45.

    CAS  Google Scholar 

  19. S. Roy, S. Suwas, S. Tamirisakandala, D.B. Miracle and R. Srinivasan: Acta Mater., 2011, vol. 59, pp. 5494-5510.

    Article  CAS  Google Scholar 

  20. S. Roy, V. Tungla and S. Suwas, Metall. Mater. Trans. A, 2011, vol. 42(9), pp. 2535-41.

    Article  Google Scholar 

  21. S. Roy and S. Suwas: Mater. Sc. Eng. A, 2012, vol. 540, pp. 152-63.

    Article  CAS  Google Scholar 

  22. S. Roy and S. Suwas: J. Alloys Comp., 2013, vol. 548, pp. 110-125.

    Article  CAS  Google Scholar 

  23. S. Zherebtsov, M. Murzinova, G. Salishchev and S.L. Semiatin: Acta Mater., 2011, vol. 59, pp. 4138-4150.

    Article  CAS  Google Scholar 

  24. G. Sharma, R.V. Ramanujan and G.P. Tiwari: Acta Mater., 2000, vol. 48, pp. 875-889.

    Article  CAS  Google Scholar 

  25. Y.L. Tian and R.W. Kraft: Metall. Trans. A, 1987, vol. 18, pp. 1403-14.

    CAS  Google Scholar 

  26. J.C.M. Kampe, T.H. Courtney and Y. Leng: Acta Metall., 1989, vol. 37, pp. 1735-1745.

    Article  CAS  Google Scholar 

  27. M.F. Bartholomeusz and J.A. Wert: Metall. Mater. Trans. A, 1994, vol. 25, pp. 2371-2381.

    Article  CAS  Google Scholar 

  28. T.H. Courtney and J.C.M. Kampe: Acta Metall., 1989, vol. 37, pp. 1747-1758.

    Article  CAS  Google Scholar 

  29. S. Mironov, M. Murzinova, S. Zherebtsov, G.A. Salishchev and S.L. Semiatin: Acta Mater., 2009, vol. 57, pp. 2470-2481.

    Article  CAS  Google Scholar 

  30. S.L Semiatin and T.R Bieler: Acta Mater., 2001, vol. 49, pp. 3565–73.

  31. T.R. Bieler and S.L. Semiatin: Inter. J. Plast., 2002, vol. 18, pp. 1165-1189.

    Article  CAS  Google Scholar 

  32. T.R. Bieler, M.G. Glavicic and S.L. Semiatin: J. Metals, 2002, vol. 54, pp. 31-36.

    CAS  Google Scholar 

  33. F. Cao, E.K. Cerreta, C.P. Trujillo and G.T. Gray III: Acta Mater., 2008, vol. 56, pp. 5804-5817.

    Article  CAS  Google Scholar 

  34. L. Zeng and T.R. Bieler: Mater. Sci. Eng. A, 2005, vol. 392, pp. 403-414.

    Article  Google Scholar 

  35. H. Feng, Y. Zhou, D. Jia and Q. Meng: Scripta Mater., 2006, vol. 55, pp. 667-670.

    Article  CAS  Google Scholar 

  36. S. Roy, A. Sarkar and S. Suwas: Mater. Sci. Eng. A 528 (2010) 449-458.

    Article  Google Scholar 

  37. A. Sarkar, S. Roy and S. Suwas: Mater. Charact., 2011, vol. 62, pp. 35-42.

    Article  CAS  Google Scholar 

  38. S. Roy, S. Suwas, S. Tamirisakandala, R. Srinivasan and D.B. Miracle: Supplemental Proceedings TMS, 2009, vol. 3, pp. 63-70.

    Google Scholar 

  39. S.L. Semiatin, N. Stefansson and R.D. Doherty: Metall. Mater. Trans. A, 2005, vol. 36, pp. 1372-1376.

    Article  CAS  Google Scholar 

  40. M. Peters and G. Luetjering: Titanium 80, H. Kimura, O. Izumi, Eds., Metallurgical Society of AIME, 1980, pp. 925–38.

  41. Z.S. Zhu, J.L. Gu and N.P. Chen: Scripta Mater., 1996, vol. 34, pp. 1281-1286.

    Article  Google Scholar 

  42. A.W. Bowen: Mater. Sci. Eng. A, 1977, vol. 29, pp. 19-28.

    Article  CAS  Google Scholar 

  43. L. Germain, N. Gey, M. Humbert, P. Vo, M. Jahazi and P. Bocher: Acta Mater., 2008, vol. 56, pp. 4298-4308.

    Article  CAS  Google Scholar 

  44. M. Humbert, L. Germain, N. Gey, P. Bocher and M. Jahazi: Mater. Sci. Eng. A, 2006, vol. 430, pp. 157-164.

    Article  Google Scholar 

  45. L. Germain, N. Gey, M. Humbert, P. Bocher, and M. Jahazi: Acta Mater., 2005, vol. 53, pp. 3535–43.

  46. A.A. Salem, M.G. Glavicic and S.L. Semiatin: Mater. Sci. Eng. A, 2008, vol. 494, pp. 350-359.

    Article  Google Scholar 

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Acknowledgments

The authors acknowledge the Institute Nanoscience Initiative (INI) and Institute X-ray Facility at the Indian Institute of Science, Bangalore, India, and the National facility for orientation imaging microscopy and X-ray bulk texture at the Indian Institute of Technology Bombay for providing the required research facilities. The materials used for the study were originally provided by Dr. Dan Miracle of AFRL and Dr. S. Tamirisakandala of FMW Composites. The authors are thankful to Mr. Nataraj B.R., Mr. Ashranth, Mr. Atanu Chowdhury, and Mr. Nachiketa Ray for microstructural measurements.

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Correspondence to Satyam Suwas.

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Manuscript submitted May 31, 2012.

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Roy, S., Karanth, S. & Suwas, S. Microstructure and Texture Evolution During Sub-Transus Thermo-Mechanical Processing of Ti-6Al-4V-0.1B Alloy: Part II. Static Annealing in (α + β) Regime. Metall Mater Trans A 44, 3322–3336 (2013). https://doi.org/10.1007/s11661-013-1673-3

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