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1,2-Bis(diphenylphosphino)ethane-containing commo-ferracarboranes of unusual structure

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Abstract

commo-Ferracarboranes and [8-{(nido-7″,8″-C2B9H11-9″(11″)-)Ph2PCH2CH2PPh2}-commo-3,3′-Fe-{1,2-C2H9B10}{1′2′-C2B9H11}] were prepared as minor products in the metallation reaction of [K]+[nido-7,8-C2B9H12]− with the 14-electron iron complex [Ph2P(CH2)2PPh2]FeCl2. The structures of the complexes were determined by single-crystal X-ray diffraction.

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Authors and Affiliations

  1. A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 ul. Vavilova, 119991, Moscow, Russian Federation

    E. V. Balagurova, F. M. Dolgushin, A. F. Smol’yakov & I. T. Chizhevsky

  2. Gause Institute of New Antibiotics, 11 ul. Bolshaya Pirogovskaya, 119021, Moscow, Russian Federation

    A. P. Tyurin

  3. Faculty of Science, Peoples’ Friendship University of Russia (RUDN University), 6 ul. Miklukho-Maklaya, 117198, Moscow, Russian Federation

    A. F. Smol’yakov

Authors
  1. E. V. Balagurova
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  2. F. M. Dolgushin
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  3. A. P. Tyurin
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  4. A. F. Smol’yakov
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  5. I. T. Chizhevsky
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Correspondence to E. V. Balagurova.

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Deceased.

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Balagurova, E.V., Dolgushin, F.M., Tyurin, A.P. et al. 1,2-Bis(diphenylphosphino)ethane-containing commo-ferracarboranes of unusual structure. Russ Chem Bull 68, 1542–1547 (2019). https://doi.org/10.1007/s11172-019-2589-x

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  • DOI: https://doi.org/10.1007/s11172-019-2589-x

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