Abstract
The paper is focused on the ability of using two complementary photothermal techniques for the measurement of all thermal parameters of some porous and/or semi-transparent solid samples whose composition, structure, and geometry do not allow a complete thermal characterization using a single technique. In this work, we combine a contact technique, photopyroelectric (PPE) calorimetry, with a non-contact one, infrared lock-in IR thermography (IRT), in order to investigate some solid samples such as dental composites, building materials, drugs, and semiconductors. The composition and the geometry of the investigated samples make the PPE method (in “front” detection configuration together with thermal-wave resonator cavity (TWRC) technique as scanning procedure) suitable for thermal effusivity measurements and IRT for thermal diffusivity investigations. In such a way, this combination of methods leads to a complete thermal characterization of the investigated materials.
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Dadarlat D, Pop MN, Streza M, Longuemart S, Depriester M, Sahraoui AH, Simon V. Combined FPPE–PTR calorimetry involving TWRC technique. Theory and mathematical simulations. Int J Thermophys. 2010;31:2275–82.
Dadarlat D, Pop MN, Streza M, Longuemart S, Depriester M, Sahraoui AH, Simon V. Combined FPPE-PTR calorimetry involving TWRC technique II. Experimental: application to thermal effusivity measurements of solids. Int J Thermophys. 2011;32:2092–101.
Dadarlat D. Contact and non-contact photothermal calorimetry for investigation of condensed matter. Trends and recent developments. J Therm Analysis Calor. 2012;110:27–35.
Dadarlat D, Pop MN, Onija O, Streza M, Pop MM, Longuemart S, Depriester M, Sahraoui AH, Simon V. Photopyroelectric (PPE) calorimetry of composite materials. J Therm Analysis Calor. 2013;111:1129–32.
Silaghi-Dumitrescu L, Dadarlat D, Streza M, Buruiana T, Prodan D, Hodisan I, Prejmerean C. Preparation of a new type of giomers and their thermal characterization by photopyroelectric calorimetry. Comparison with commercially available materials. J Therm Analysis Calor. 2014;. doi:10.1007/s10973-013-3561-x.
Mandelis A, Zver MM. Theory of the photopyroelectric effect in solids. J Appl Phys. 1985;57:4421–30.
Chirtoc M, Mihailescu G. Theory of the photopyroelectric method for investigation of optical and thermal materials properties. Phys Rev. 1989;B40:9606–17.
Dadarlat D, Chirtoc M, Neamtu C, Candea R, Bicanic D. Inverse photopyroelectric detection method. Phys Stat Sol. 1990;121:K231–4.
Dadarlat D, Frandas A. Inverse photopyroelectric detection of phase transitions. Appl Phys. 1993;A56:235–9.
Mandelis A, Matvienko A. Pyroelectric Materials and Sensors. 2007 (Kerala: D. Remiens): 61.
Delenclos S, Chirtoc M, Sahraoui AH, Kolinsky C, Buisine JM. Assessment of calibration procedures for accurate determination of thermal parameters of liquids and their temperature dependence using the photopyroelectric method. Rev Sci Instrum. 2002;73:2773–80.
Shen J, Mandelis A. Thermal-wave resonator cavity. Rev Sci Instrum. 1995;66:4999–5005.
Shen J, Mandelis A, Tsai H. Signal generation mechanism, intercavity-gas thermal diffusivity temperature dependence and absolute infrared emissivity measurements in a thermal-waveresonant cavity. Rev Sci Instrum. 1998;69:197–203.
Busse G, Wu D, Karpen W. Thermal wave imaging with phase sensitive modulated thermography. J Appl Phys. 1992;71:3962–5.
Breiteinstein O, Warta W, Langenkamp M. Lock-in thermography: basics and use for evaluating electronic devices and materials. Berlin: Springer. 2012, ISBN: 3642024165.
Streza M, Pop MN, Kovacs K, Simon V, Longuemart S, Dadarlat D. Thermal effusivity investigations of solid materials by using the thermal-wave-resonator-cavity (TWRC) configuration. Theory and mathematical simulations. Laser Phys. 2009;19:1340–4.
Dadarlat D. Photopyroelectric calorimetry of liquids. Recent development and applications. Laser Phys. 2009;19:1330–9.
Salazar A, Oleaga A. Overcoming the influence of the coupling fluid in photopyroelectric measurements of solid samples. Rev Sci Instrum. 2012;83:014903.
Reiter M, Hartman H. A new steady-state method for determining thermal conductivity. J Geophys Res. 2012;76:7047–51.
Madelung O. Semiconductors: data handbook. Springer-Verlag; 2003.
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The authors acknowledge the financial support supported by the Ministry of Education Research and Youth of Romania, through the National Research Programs, PN-II-ID-PCE-2011-3-0036 and PN-II-PT-PCCA-2-11-3.
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Dadarlat, D., Streza, M., Onija, O. et al. Complementary photothermal techniques for complete thermal characterization of porous and semi-transparent solids. J Therm Anal Calorim 119, 301–308 (2015). https://doi.org/10.1007/s10973-014-4091-x
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DOI: https://doi.org/10.1007/s10973-014-4091-x