Abstract
Nanorods of the three-dimensional coordination polymer, [Ag2(μ 2-py-4-c)2] n (1) [py-4-c− = pyridine-4-carboxylate], have been synthesized by sonochemical process. The single-crystal X-ray data of compound 1 shows the formation of a 3D interpenetrated silver(I) coordination polymer, which has agostic interactions around the silver(I) ions and two types of AgI ions with O2NAg1···O2H, N2 Ag2···O2H2 coordination spheres. Silver nanoparticles were fabricated from thermal decomposition of 1 nanorods. These nanostructures were characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The thermal stability of 1 was studied by thermo gravimetric (TG) and differential thermal (DT) analysis.
References
H. Li, M. Eddaoudi, M. O’Keeffe, O.M. Yaghi, Nature 402, 276 (1999)
T. Loiseau, C. Serre, C. Huguenard, G. Fink, F. Taulelle, M. Henry, T. Bataille, G. Férey, Chem. Eur. J. 10, 1373 (2004)
S.S.-Y. Chiu, S.M.-F. Lo, J.P.H. Charmant, A.G. Orpen, I.D. Williams, Science 283, 1148 (1999)
A.K. Cheetham, C.N.R. Rao, Science 318, 58 (2007)
A. Morsali, M.Y. Masoomi, Coord. Chem. Rev. 253, 1882 (2009)
K. Akhbari, A. Morsali, Coord. Chem. Rev. 254, 1977 (2010)
O.T. Ilkun, S.J. Archibald, C.L. Barnes, N. Gerasimchuk, R. Biagioni, S. Silchenko, O.A. Gerasimchuk, V.N. Nemykin, J. Chem. Soc. Dalton Trans. 5715 (2008)
E.A.H. Griffith, E.L. Amma, J. Am. Chem. Soc. 96, 743 (1974)
H.G. Smith, R.E. Rundle, J. Am. Chem. Soc. 80, 5075 (1958)
H. Schmidbaur, W. Bublak, B. Huber, G. Reber, G. Muller, Angew. Chem. Int. Ed. Engl. 25, 1089 (1986)
G.L. Ning, L.P. Wu, K. Sugimoto, M. Munakata, T. Kuroda-Sowa, M. Mackawa, J. Chem. Soc. Dalton Trans. 2529 (1999)
M. Munakata, L.P. Wu, T. Kuroda-Sowa, M. Maekawa, Y. Suenaga, G.L. Ning, T. Kojima, J. Am. Chem. Soc. 120, 8610 (1998)
P. Pyykkö, Chem. Rev. 97, 597 (1997)
M. Jansen, Angew. Chem. Int. Ed. 26, 1098 (1987)
C.-S. Liu, P.-Q. Chen, E.-C. Yang, J.-L. Tian, X.-H. Bu, Z.-M. Li, H.-W. Sun, Z. Lin, Inorg. Chem. 45, 5812 (2006) and references cited therein
C.-S. Liu, P.-Q. Chen, Z. Chang, J.-J. Wang, L.-F. Yan, H.-W. Sun, X.-H. Bu, Z. Lin, Z.-M. Li, S.R. Batten, Inorg. Chem. Commun. 11, 159 (2008)
C. Santini, C. Pettinari, G. Gioia Lobbia, R. Spagna, M. Pellei, F. Vallorani, Inorg. Chim. Acta 285, 81 (1999)
Q. Liu, Y. Bian, H. Liu, X. Wang, Y. Chen, X. Li, J. Jiang, J. Colloid Interface Sci. 304, 431 (2006)
R. Bashiri, K. Akhbari, A. Morsali, Inorg. Chim. Acta 362, 1035 (2009)
K. Akhbari, A. Morsali, Inorg. Chim. Acta 363, 1435 (2010)
D.M. Ciurtin, Y.-B. Dong, M.D. Smith, T. Barclay, H.-C. zur Loye, Inorg. Chem. 40, 2825 (2001)
H. Liang, Q. Tang, K. Yu, S. Li, J. Ke, Mater. Lett. 61, 1020 (2007)
S. Hünig, H. Meixner, T. Metzenthin, U. Langohr, J.U. Schütz, H.-C. Wolf, E. Tillmanns, Adv. Mater. 2, 361 (1990)
K. Akhbari, A. Morsali, Cryst. Growth Des. 7, 2024 (2007)
K. Akhbari, A. Morsali, J. Organomet. Chem. 692, 5141 (2007)
K. Akhbari, A. Morsali, Inorg. Chim. Acta 362, 1692 (2009)
K. Akhbari, A. Morsali, A.D. Hunter, M. Zeller, Inorg. Chem. Commun. 10, 178 (2007)
K. Akhbari, A. Morsali, J. Mol. Struct. 878, 65 (2008)
K. Akhbari, K. Alizadeh, A. Morsali, M. Zeller, Inorg. Chem. Acta 362, 2589 (2009)
K. Akhbari, A. Morsali, J. Organomet. Chem. 692, 5109 (2007)
K. Akhbari, A. Morsali, Inorg. Chem. Commun. 10, 1189 (2007)
K. Akhbari, A. Morsali, M. Zeller, J. Organomet. Chem. 692, 3788 (2007)
R. Bashiri, K. Akhbari, A. Morsali, M. Zeller, J. Organomet. Chem. 693, 1903 (2008)
K. Akhbari, A. Morsali, Sh. Rafiei, M. Zeller, J. Organomet. Chem. 693, 257 (2008)
N. Soltanzadeh, A. Morsali, Ultrason. Sonochem. 17, 139 (2010)
H. Ahmadzadi, F. Marandi, A. Morsali, J. Organomet. Chem. 694, 3565 (2009)
L. Tian, L.Y. Yep, T.T. Ong, J. Yi, J. Ding, J.J. Vittal, Cryst. Growth Des. 9, 352 (2009)
G.M. Sheldrick, SHELXS-97 and SHELXL-97 (Göttingen University, Göttingen, 1997)
Mercury 1.4.1, Copyright Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge, CB2 1EZ, UK (2001–2005)
L. Han, D. Yuan, B. Wu, C. Liu, M. Hong, Inorg. Chim. Acta 359, 2232 (2006)
P.-Y. Cheng, C.-Y. Chen, H.M. Lee, Inorg. Chim. Acta 362, 1840 (2009)
D. Sun, G.-G. Luo, Q.-J. Xu, N. Zhang, Y.-C. Jin, H.-X. Zhao, L.-R. Lin, R.-B. Huang, L.-S. Zheng, Inorg. Chem. Commun. 12, 782 (2009)
S.Q. Liu, H. Konaka, T. Kuroda-Sowa, M. Maekawa, Y. Suenaga, G.L. Ning, M. Munakata, Inorg. Chim. Acta 358, 919 (2005)
A. Bondi, J. Phys. Chem. 68, 441 (1964)
K. Akhbari, A. Morsali, CrystEngComm 12, 3394 (2010)
X. Liu, Angew. Chem. Int. Ed. 48, 3018 (2009)
Acknowledgment
Supporting of this investigation by Tarbiat Modares University is gratefully acknowledged.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Akhbari, K., Hemmati, M. & Morsali, A. Fabrication of Silver Nanoparticles and 3D Interpenetrated Coordination Polymer Nanorods from the Same Initial Reagents. J Inorg Organomet Polym 21, 352–359 (2011). https://doi.org/10.1007/s10904-010-9444-8
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s10904-010-9444-8