Abstract
Pure copper of 99.99 % purity was processed by high-pressure torsion under a pressure of 6.0 GPa at room temperature through various numbers of turns from 1/4 to 10. Microhardness measurements show that the hardness initially increases to a maximum value at a strain of ~5.6, decreases to a strain of ~8.4, and then increases slowly to a saturation condition at strains at and above ~80. These data are interpreted in terms of the advent of dynamic recrystallization. The results have similarities and differences to the softening with recovery that is well established in high-purity aluminum.
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Acknowledgements
This work was supported by the National Natural Science Foundation of China under Grant Nos. 51375111 and 51475124, the National Science Foundation of the United States under Grant No. DMR-1160966, and the European Research Council under ERC Grant Agreement No. 267464-SPDMETALS. Partial support was also provided by the National Basic Research Program of China under Grant No. 2012CB934100.
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Xu, J., Li, J., Wang, C.T. et al. Evidence for an early softening behavior in pure copper processed by high-pressure torsion. J Mater Sci 51, 1923–1930 (2016). https://doi.org/10.1007/s10853-015-9499-6
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DOI: https://doi.org/10.1007/s10853-015-9499-6