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The Mechanisms of Deformation and Damage of Mudstones: A Micro-scale Study Combining ESEM and DIC

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Abstract

Combining environmental scanning electron microscopy (ESEM) and digital image correlation techniques, the mechanical behaviour of mudstones is studied at the scale of their composite microstructure (that is, grains of carbonate and quartz embedded in a clay matrix). A specially designed apparatus is developed to allow in-situ uniaxial compression tests on samples with controlled humidity states in the ESEM chamber. As the mechanical behavior of mudstones is sensitive to water content, two tests on samples with contrasting water contents (3.8 and 7.4 %) are performed to identify the unified mechanisms of deformation and damage. We illustrate heterogeneous local strain fields that well correlate with the microstructure of mudstones. Three types of deformation bands involving different mechanisms have been classified: orthogonal (compaction of macro-pores and closure of pre-existing cracks), parallel (micro-cracking) and inclined (shear deformation) to the uniaxial compression direction. These deformation modes are activated at different stress levels, and they strongly interact: for instance, a high-strained shear band may result in tensile micro-cracks at its tip. We also illustrate damage phenomena, particularly at the inclusion-matrix interface, which is found to be a hazardous position for nucleation of micro-cracks.

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References

  • Abou-Chakra Guéry A, Cormery F, Shao JF, Kondo D (2008) A micromechanical model of elasto-plastic and damage behavior of a cohesive geomaterial. Int J Solids Struct 45(5):1406–1429

    Article  Google Scholar 

  • Allais L, Bornert M, Bretheau T, Caldemaison D (1994) Experimental characterization of the local strain field in a heterogeneous elastoplastic material. Acta Metall et Mater 42(11):3865–3880

    Article  Google Scholar 

  • ANDRA (2005) Rfrentiel du Site Meuse/Haute-Marne: Tome 2

  • Bemer E, Longuemare P, Vinck O (2004) Poroelastic parameters of Meuse/Haute Marne argillites: effect of loading and saturation states. Appl Clay Sci 26:359–366

    Article  Google Scholar 

  • Bésuelle P (2001) Compacting and dilating shear bands in porous rock: Theoretical and experimental conditions. J Geophys Res 106:13435–13442

    Article  Google Scholar 

  • Bobko C, Ulm F-J (2008) The nano-mechanical morphology of shale. Mech Mater 40:318–337

    Article  Google Scholar 

  • Bornert M, Valès F, Gharbi H, Nguyen Minh D (2010) Multiscale full-field strain measurements for micromechanical investigations of the hydromechanical behaviour of clayey rocks. Strain 46:33–46

    Article  Google Scholar 

  • Bornert M, Orteu JJ, Roux S (2011) Corrélation d’images. In: Grédiac et M, Hild F (eds) Mesures de champs et identification Hermès Science, Chap 6, pp 175–208

  • Carrier B, Vandamme M, Pellenq RJM, Van Damme H (2014) Elastic properties of swelling clay particles at finite temperature upon hydration. J Phy Chem C 118:8933–8943

    Article  Google Scholar 

  • Chiarelli AS, Shao JF, Hoteit N (2003) Modelling of elastic-plastic damage behaviour of a claystone. Int J Plast 19:23–45

    Article  Google Scholar 

  • Chu T, Ranson W, Sutton M, Peters W (1985) Applications of the digital-image-correlation techniques to experimental mechanics. Exp Mech 25:232–244

    Article  Google Scholar 

  • Djran-Maigre I, Tessier D, Grunberger D, Velde B, Vasseur G (1998) Evolution of microstructures and macroscopic properties of some clays during experimental compaction. Marine Pet Geol 15:109–128

    Article  Google Scholar 

  • Doumalin P, Bornert M (2000) Micromechanical applications of digital image correlation techniques. In: Jacquot P, Fournier JM (eds) Proceedings of Interferometry in Speckle Light, Theory and Applications, Springer, pp 67–74

  • Ebrahimi D, Whittle AJ, Pellenq RJM (2014) Mesoscale properties of clay aggregates from potential of mean force representation of interactions between nanoplatelets. J Chem Phy 140:154309

    Article  Google Scholar 

  • Gaucher E, Robelin C, Matray JM, Ngrel G, Gros Y, Heitz JF, Vinsot A, Rebours H, Cassagnabre A, Bouchet A (2004) ANDRA underground research laboratory: interpretation of the mineralogical and geochemical data acquired in the Callovian-Oxfordian formation by investigative drilling. Phy Chem Earth 29:55–77

    Article  Google Scholar 

  • Lenoir N, Bornert M, Desrues J, Bésuelle P, Viggiani G (2007) Volumetric digital image correlation applied to X-ray microtomography images from triaxial compression tests on argillaceous rock. Strain 43:193–205

    Article  Google Scholar 

  • Pham QT, Valès F, Malinsky L, Nguyen MD, Gharbi H (2007) Effets of desaturation-resaturation on mudstone. Phy Chem Earth 32:646–655

    Article  Google Scholar 

  • Robinet JC, Sardini P, Coelho D, Parneix JC, Prêt D, Sammartino S, Boller E, Altmann S (2012) Effects of mineral distribution at mesoscopic scale on solute diffusion in a clay-rich rock: Example of the Callovo-Oxfordian mudstone (Bure, France). Water Resour Res 48. doi:10.1029/2011WR011352

  • Rudnicki JW (2002) Conditions for compaction and shear bands in a transversely isotropic material. Int J Solids Struct 39:3741–3756

    Article  Google Scholar 

  • Rudnicki, JW, Rice JR (1975) Conditions for the localization of deformation in pressure-sensitive dilatant materials. J Mech Phy Solids 23:371–394.

  • Sammartino S, Bouchet A, Prêt D, Parneix J-C, Tevissen E (2003) Spatial distribution of porosity and minerals in clay rocks from the Callovo-Oxfordian formation (Meuse/Haute-Marne, Eastern France) implications on ionic species diffusion and rock sorption capability. App Clay Sci 23:157–166

  • Sone H, Zoback MD (2013) Mechanical properties of shale-gas reservoir rocks Part 1: Static and dynamic elastic properties and anisotropy. Geophysics 78:381–392

    Article  Google Scholar 

  • Sutton MA, Orteu J-J, Schreier HW (2009) Image correlation for shape, motion and deformation measurements : basic concepts, theory and applications. Springer press

  • Tang CA, Liu H, Lee PKK, Tsui Y, Tham LG (2000) Numerical studies of the influence of microstructure on rock failure in uniaxial compression—Part I: effect of heterogeneity. Int J Rock Mech Mining Sci 37:555–569

    Article  Google Scholar 

  • Valès F, Nguyen Minh D, Gharbi H, Rejeb A (2004) Experimental study of the influence of the degree of saturation on physical and mechanical properties in Tournemire shale (France). Appl Clay Sci 26:197–207

    Article  Google Scholar 

  • Wang LL, Bornert M, Chanchole S, Héripré E, Yang DS, Halphen B, Pouya A, Tanguy A, Caldemaison D (2013) Micro-scale experimental investigation of the swelling anisotropy of the Callovo-Oxfordian argillaceous rock. Clay Min 48:391–402

    Article  Google Scholar 

  • Wang LL, Bornert M, Héripré E, Chanchole S, Tanguy A (2013) Full-field measurements on low-strained geomaterials using environmental scanning electron microscopy and digital image correlation: improved imaging conditions. Strain 50:370–380

    Article  Google Scholar 

  • Wang LL, Bornert M, Héripré E, Yang DS, Chanchole S (2014) Irreversible deformation and damage in argillaceous rocks induced by wetting/drying. J Appl Geophy 107:108–118

  • Wenk HR, Voltolini M, Mazurek M, Van Loon LR, Vinsot A (2008) Preferred orientations and anisotropy in shales: Callovo-Oxfordian shale (France) and Opalinus Clay (Switzerland). Clays Clay Min 56:285–306

    Article  Google Scholar 

  • Yang DS, Bornert M, Chanchole S, Gharbi H, Valli P, Gatmiri B (2012) Dependence of elastic properties of argillaceous rocks on moisture content investigated with optical full-field strain measurement techniques. Int J Rock Mech Mining Sci 53:45–55

    Article  Google Scholar 

  • Zhang CL, Rothfuchs T (2004) Experimental study of the hydro-mechanical behaviour of the Callovo-Oxfordian argillite. Appl Clay Sci 26:325–336

    Article  Google Scholar 

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Correspondence to L. L. Wang.

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Wang, L.L., Bornert, M., Héripré, E. et al. The Mechanisms of Deformation and Damage of Mudstones: A Micro-scale Study Combining ESEM and DIC. Rock Mech Rock Eng 48, 1913–1926 (2015). https://doi.org/10.1007/s00603-014-0670-1

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  • DOI: https://doi.org/10.1007/s00603-014-0670-1

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