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Certification of SRM 1589a PCBs, pesticides, PBDEs, and dioxins/furans in human serum

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Abstract

The Certificate of Analysis for SRM 1589a PCBs, Pesticides, PBDEs, and Dioxins/Furans in Human Serum has been updated to include certified concentration values for 27 polychlorinated biphenyl (PCB) congeners, three chlorinated pesticides, and four polybrominated diphenyl ether (PBDE) congeners as well as reference concentration values for 27 additional PCB congeners, six additional chlorinated pesticides, three additional PBDE congeners, and selected polychlorinated dibenzo-p-dioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs). This represents an addition of concentration values for 29 PCB congeners and for PBDE congeners that were not quantified in the previous issue of SRM 1589a. With the increased number of certified and reference concentration values for PCBs and the inclusion of certified and reference concentration values for PBDEs, this serum material will be more useful as a reference material for contaminant monitoring in human tissues and fluids.

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Disclaimer

Certain commercial equipment, instruments, or materials are identified in this paper to specify adequately the experimental procedure. Such identification does not imply recommendation or endorsement by the National Institute of Standards and Technology, nor does it imply that the materials or equipment identified are necessarily the best available for the purpose.

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Authors and Affiliations

  1. Analytical Chemistry Division, National Institute of Standards and Technology, 100 Bureau Drive, Gaithersburg, MD, 20899, USA

    Michele M. Schantz, Katherine E. Sharpless, Heather M. Stapleton & Stephen A. Wise

  2. Analytical Chemistry Division, National Institute of Standards and Technology, Charleston, SC, 29412, USA

    Jennifer M. Keller & Robert Swarthout

  3. Statistical Engineering Division, National Institute of Standards and Technology, 100 Bureau Drive, Gaithersburg, MD, 20899, USA

    Stefan Leigh

  4. Organic Analytical Toxicology, Division of Laboratory Sciences, National Center for Environmental Health, Centers for Disease Control and Prevention, 4770 Buford Highway, Atlanta, GA, 30341, USA

    Donald G. Patterson Jr, Andreas Sjödin & Wayman E. Turner

Authors
  1. Michele M. Schantz
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  2. Jennifer M. Keller
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  3. Stefan Leigh
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  4. Donald G. Patterson Jr
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  5. Katherine E. Sharpless
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  6. Andreas Sjödin
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  7. Heather M. Stapleton
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  8. Robert Swarthout
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  9. Wayman E. Turner
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  10. Stephen A. Wise
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Corresponding author

Correspondence to Michele M. Schantz.

Electronic supplementary material

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Table S-1

Concentrations (ng/kg) from the different methods used in the certification of SRM 1589a. (PDF 15 kb)

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Schantz, M.M., Keller, J.M., Leigh, S. et al. Certification of SRM 1589a PCBs, pesticides, PBDEs, and dioxins/furans in human serum. Anal Bioanal Chem 389, 1201–1208 (2007). https://doi.org/10.1007/s00216-007-1519-1

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  • DOI: https://doi.org/10.1007/s00216-007-1519-1

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