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Synthesis of titanium containing silica ZSM-48 (TS-48) using hexamethonium hydroxide as template

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Abstract

Titanium containing silica analog of ZSM-48 (TS-48) has been synthesized by a new method using hexamethonium hydroxide as a template. Titanium incorporation in the framework was evidenced from unit cell volume expansion, framework IR spectra and diffuse reflectance UV-Vis spectra.

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References

  1. S. Kaliaguine, J.B. Nagy and Z. Gabelica, Stud. Surf. Sci. Catal. 35 (1988) 381.

    Google Scholar 

  2. M. Taramasso, G. Perego and B. Notari, US Patent 4 410 510 (1983).

  3. A. Esposito, C. Neri, F. Buonomo and M. Taramasso, UK Patent 2 116 974 (1983).

  4. D.R.C. Huybrechts, L. De Bruycker and P.A. Jacobs, Nature 345 (1990) 240.

    Google Scholar 

  5. B. Notari, Stud. Surf. Sci. Catal. 37 (1987) 413.

    Google Scholar 

  6. J.S. Reddy and R. Kumar, J. Catal. 130 (1991) 440.

    Google Scholar 

  7. A. Thangaraj, S. Sivasanker and P. Ratnasamy, J. Catal. 131 (1991) 294.

    Google Scholar 

  8. D. Trongon, L. Bonneviot, A. Bittar, A. Sayari and S. Kaliaguine, J. Mol. Catal. 74 (1992) 233.

    Google Scholar 

  9. G. Bellussi and V. Fattore, Stud. Surf. Sci. Catal. 69 (1991) 79.

    Google Scholar 

  10. A. Thangaraj and S. Sivasanker, J. Chem. Soc. Chem. Commun. (1992) 123.

  11. M.G. Clerici, A. Bartolomeo and G. Bellussi, EP 0 412 596 A1 (1990).

  12. D.P. Serrano, H.X. Li and M.E. Davis, J. Chem. Soc. Chem. Commun. (1992) 745.

  13. K.M. Reddy, S. Kaliaguine, A. Sayari, A.V. Ramaswamy, V.S. Reddy and L. Bonneviot, Catal. Lett. 23 (1994) 175.

    Google Scholar 

  14. J.L. Schlenker, W.J. Rohrbaugh, P. Chu, E.W. Valyocsik and G.T. Kokotailo, Zeolites 5 (1985) 355.

    Google Scholar 

  15. P. Chu, EPA 23,089 (1980); USP 4,397,827 (1983).

  16. L.D. Rollman and E.W. Valyocsik, EPA 15,132 (1980).

  17. J.L. Casci, B.M. Lowe and T.V. Whittam, UK PA GB 2,077,709A (1981).

  18. G.W. Godwell, R.P. Denkewiez and L.B. Sand, Zeolites 5 (1985) 153.

    Google Scholar 

  19. M. Boccuti, K.M. Rao, A. Zecchina, G. Leofanti and G. Petrini, Stud. Surf. Sci. Catal. 48 (1989) 133.

    Google Scholar 

  20. M.A. Camblor, A. Corma and J. Pérez-Pariente, J. Chem. Soc. Chem. Commun. (1993) 557.

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Authors and Affiliations

  1. Department of Chemical Engineering and CERPIC, Université Laval, G1K7P4, SteFoy, Quebec, Canada

    K. Madhusudan Reddy, S. Kaliaguine & A. Sayari

Authors
  1. K. Madhusudan Reddy
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  2. S. Kaliaguine
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  3. A. Sayari
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Madhusudan Reddy, K., Kaliaguine, S. & Sayari, A. Synthesis of titanium containing silica ZSM-48 (TS-48) using hexamethonium hydroxide as template. Catal Lett 23, 169–173 (1994). https://doi.org/10.1007/BF00812145

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  • DOI: https://doi.org/10.1007/BF00812145

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