Abstract
Ti2B5, TiB12, TiB≃25, TiB≃55, and TiB≃100 were prepared by self-propagating high-temperature synthesis and characterized by microstructural analysis, x-ray diffraction, and x-ray microanalysis. Data on the crystal structure, lattice parameters, and mechanical properties of the synthesized borides are presented.
Similar content being viewed by others
References
Kuz’ma, Yu.B. and Chaban, N.F.,Dvoinye i troinye sistemy, soderzhashchie bor. Spravochnik (Binary and Ternary Boron Systems: A Handbook), Moscow: Metallurgiya, 1990, p. 317.
Murray, J.L., Liao, P.K., and Spear, K.E., The B-Ti (Boron-Titanium) System,Bull. Alloy Phase Diagrams, 1986, vol. 7, no. 6, pp. 550–557.
Post, B. and Glaser, F.W., Borides of Some Transition Metals,J. Chem. Phys., 1952, vol. 20, no. 5, pp. 1050–1055.
Schwarzkopf, P. and Glaser, P.M., Structure and Chemical Properties of Borides of Transition Metals of the Fourth, Fifth, and Sixth Groups,Z. Metallkd., 1953, vol. 44, pp. 353–358.
Powder Diffraction File, Swarthmore: Joint Committee on Powder Diffraction Standards, 1989.
Brewer, L., Sawyer, D.L., Templeton, D.H., and Dauben, C.H., A Study of the Refractory Borides,J. Am. Ceram. Soc., 1951, vol. 34, no. 2, pp. 173–179.
Palty, A.E., Margolin, H., and Nielsen, J.P., Titanium-Nitrogen and Titanium-Boron Systems,Trans. Am. Soc. Met., 1954, vol. 46, no. 3, pp. 312–328.
Greenhourse, H., Accountis, O., and Sisler, H., High-Temperature Reactions in the System Titanium Carbide-Boron Carbide,J. Am. Chem. Soc., 1951, vol. 73, no. 11, pp. 5086–5089.
Amberger, E. and Polborn, K., Struktur de tetragonalen (B12)4B2Ti1.3.2.0,Acta Crystallogr., Sect. B: Struct. Crystallogr. Cryst. Chem., 1975, vol. 31, pp. 949–953.
Serebryakova, T.I., Neronov, V.A., and Peshev, P.D.,Vysokotemperaturnye boridy (Refractory Borides), Moscow: Metallurgiya, 1991, p. 367.
Borovinskaya, I.P., Merzhanov, A.G., Novikov, N.P., and Filonenko, A.K., Gas-Free Combustion of Transition Metal-Boron Powder Mixtures,Fiz. Goreniya Vzryva, 1974, no. 1, pp. 4–15.
Maksimov, Yu.M., Lepakova, O.K., and Raskolenko, L.G., Study of the Combustion Mechanism in the Titanium-Boron System by Quenching the Combustion Front,Fiz. Goreniya Vzryva, 1988, no. 1, pp. 48–53.
Novikov, N.P., Borovinskaya, I.P., and Merzhanov, A.G., Composition of Reaction Products and Combustion Rate in Metal-Boron Systems at Various Ratios of Components,Fiz. Goreniya Vzryva, 1974, no. 2, pp. 201–206.
Lepakova, O.K., Raskolenko, L.G., Maksimov, Yu.M., and Braverman B.Sh., Phase Composition and Microstructure of Titanium-Boron Alloys,Izv. Akad. Nauk SSSR, Neorg. Mater., 1986, vol. 22, no. 12, pp. 1980–1983.
Raskolenko, L.G., Maksimov, Yu.M., and Lepakova, O.K., Construction of a Hypothetical Ti-B Diagram by Analysis of Combustion Products of Three-Component Systems,J. Mater. Synth. Process., 1995, vol. 3, no. 3, pp. 153–163.
Kovba, L.M. and Trunov, V.K.,Rentgenofazovyi analiz (X-ray Diffraction Analysis), Moscow: Mosk. Gos. Univ., 1976, p. 231.
Lepakova, O.K., Raskolenko, L.G., and Kasatskii, N.G., RF Patent 1770433,Byull. Izobret., 1992, no. 39.
Lepakova, O.K., Raskolenko, L.G., Kitler, V.D., and Maksimov, Yu.M., RF Patent 2060938,Byull. Izobret., 1996, no. 15.
Lepakova, O.K., Raskolenko, L.G., and Kitler, V.D., RF Patent 2109684,Byull. Izobret., 1998, no. 12.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Lepakova, O.K., Raskolenko, L.G. & Maksimov, Y.M. Titanium borides prepared by self-propagating high-temperature synthesis. Inorg Mater 36, 568–575 (2000). https://doi.org/10.1007/BF02757955
Received:
Revised:
Issue Date:
DOI: https://doi.org/10.1007/BF02757955