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Application of dicarbonyl-rhodium-trifluoroacetyl-d-camphorate to special problems of olefin analysis by gas-liquid chromatography

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Summary

The title compound, dissolved in squalane, has been used as stationary phase in g.l.c. for purity determinations of olefins. High resolution open tubular columns have been prepared with the same phase. C2H4, C2D4 and the isomeric butenes were efficiently separated.

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Literature

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Author notes

  1. V. Schurig

    Present address: Chemisches Institut der Universität Tübingen, Auf der Morgenstelle, D-74, Tübingen 1, Germany

Authors and Affiliations

  1. Chemistry Department, University of Houston, Houston, Texas, USA

    V. Schurig, R. C. Chang & A. Zlatkis

  2. Department of Chemistry, The Weizmann Institute of Science, Rehovot, Israel

    E. Gil-Av & F. Mikeš

Authors
  1. V. Schurig
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  2. R. C. Chang
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  3. A. Zlatkis
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  4. E. Gil-Av
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  5. F. Mikeš
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Schurig, V., Chang, R.C., Zlatkis, A. et al. Application of dicarbonyl-rhodium-trifluoroacetyl-d-camphorate to special problems of olefin analysis by gas-liquid chromatography. Chromatographia 6, 223–225 (1973). https://doi.org/10.1007/BF02311729

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  • DOI: https://doi.org/10.1007/BF02311729

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