Conclusions
The reaction of N, N-dimethylurea with bromoacetone in the presence of glacial AcOH leads to a mixture of 4-methyl-2-dimethylaminooxazole and its dimer, and specifically 4-methyl-4-(4′-methyl-2′-dimethylamino-5′-oxazolyl)-2-dimethylamino-Δ2,3-oxazoline.
Literature cited
H. Dworschak and F. Weygand, Ber.,101, 302 (1968).
H. Najer, R. Guidicelli, and J. Menin, Bull. Soc. Chim. France, 2040 (1967).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 7, pp. 1680–1682, July, 1977.
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Kondrat'eva, G.Y., Bogdanov, V.S., Ivanova, Z.N. et al. Noncyclic dimer of 4-methyl-2-dimethylaminooxazole. Russ Chem Bull 26, 1552–1553 (1977). https://doi.org/10.1007/BF00928561
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DOI: https://doi.org/10.1007/BF00928561