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Rapid and quantitative pentafluorobenzoylation of nitrophenols and other phenolic compounds in water for gas-chromatographic determination with electron capture detection

Schnelle und quantitative Pentafluorobenzoylierung von Nitrophenolen und anderen Phenolen im Wasser für ihre gas-chromatographische Bestimmung mit Elektroneneinfangdetektion

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Summary

Derivatization of nitrophenols in water with pentafluorobenzoylchloride for a gas-chromatographic determination with electron capture detection is achieved by phase transfer reaction using dicyclohexyl-18-crown-6 as catalyst.

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Authors and Affiliations

  1. Fraunhofer Institut für Toxikologie und Aerosolforschung, Nikolai-Fuchs-Strasse 1, D 3000, Hannover 61, Federal Republic of Germany

    H. D. Winkeler & K. Levsen

Authors
  1. H. D. Winkeler
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  2. K. Levsen
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Winkeler, H.D., Levsen, K. Rapid and quantitative pentafluorobenzoylation of nitrophenols and other phenolic compounds in water for gas-chromatographic determination with electron capture detection. Z. Anal. Chem. 334, 340–343 (1989). https://doi.org/10.1007/BF00488479

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  • DOI: https://doi.org/10.1007/BF00488479

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