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Effect of ultrasonic irradiation on precipitation of lead oxalate from aqueous solution

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Abstract

A precipitation reaction between a lead-nitrate solution and oxalic acid was carried out with and without ultrasound, and the effect of ultrasonic irradiation in solution was investigated. The oxalate precipitates were a mixture of Pb oxalate and an X-phase, which seems to be a lead salt containing C2O 2−4 NO −3 , and OH−. It was found that irradiation with ultrasound during the precipitation reaction accelerated the formation of the X-phase.

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Authors and Affiliations

  1. Research Laboratory of Engineering Materials, Tokyo Institute of Technology, 4259 Nagatsuta, Midori, 227, Yokohama, Japan

    Hee Lack Choi, Naoya Enomoto & Zenbe E Nakagawa

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  1. Hee Lack Choi
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  2. Naoya Enomoto
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  3. Zenbe E Nakagawa
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Choi, H.L., Enomoto, N. & Nakagawa, Z.E. Effect of ultrasonic irradiation on precipitation of lead oxalate from aqueous solution. JOURNAL OF MATERIALS SCIENCE 29, 3239–3242 (1994). https://doi.org/10.1007/BF00356669

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  • DOI: https://doi.org/10.1007/BF00356669

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