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Effect of Annealing Temperature on Phase Transformation of NiCr2O4 Nanoparticles and Evaluated Its Structural and Magnetic Properties

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Advances in Functional and Smart Materials

Part of the book series: Lecture Notes in Mechanical Engineering ((LNME))

Abstract

Tetragonal nickel chromite (NiCr2O4) nanoparticles were synthesized using the wet chemical method and investigated their structural and magnetic properties at different annealing temperatures. Structural properties of as-prepared were determined using X-ray diffraction (XRD), Fourier-transform infra-red (FTIR) spectroscopy, and Raman spectroscopy technique. XRD results demonstrated that NiCr2O4 nanoparticles annealed at 800 and 900 °C led to the multi-phase compound formation of rhombohedral chromium oxide (Cr2O3) and tetragonal NiCr2O4 phase. However, a complete transformation of multi-phase to single NiCr2O4 tetragonal phase was achieved at 1000 °C. Raman and FTIR spectra also confirmed the formation of a single nickel chromite phase at an annealing temperature of 1000 °C. Some weak traces of characteristics modes of Cr2O3 phase were demonstrated at the lower annealing temperature. Magnetic properties of NiCr2O4 nanoparticles at different annealing temperatures were determined using a vibrating sample magnetometer (VSM). Multi-phase compound nanoparticles exhibited a mixed antiferromagnetic and paramagnetic behavior, whereas single-phase compound was ascribed to paramagnetic ones only.

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Author information

Authors and Affiliations

  1. Department of Mechanical Engineering, K.R. Mangalam University, Gurugram, 122103, India

    Jarnail Singh & Kaushal Kumar

  2. Department of Material Science and Engineering, National Institute of Technology Hamirpur, Hamirpur, 177005, India

    Pankaj Bhardwaj, Ravi Kumar & Vikram Verma

  3. School of Management and Commerce, K.R. Mangalam University, Gurugram, 122103, India

    Saurav Dixit

  4. Division of Research and Innovation, Uttaranchal University, Dehradun, India

    Saurav Dixit

Authors
  1. Jarnail Singh
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  2. Pankaj Bhardwaj
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  3. Ravi Kumar
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  4. Kaushal Kumar
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  5. Saurav Dixit
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  6. Vikram Verma
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Corresponding author

Correspondence to Jarnail Singh .

Editor information

Editors and Affiliations

  1. School of Mechanical Engineering, Lovely Professional University, Phagwara, India

    Chander Prakash

  2. Centre for Nanofibers and Nanotechnology, National University of Singapore, Singapore, Singapore

    Sunpreet Singh

  3. Department of Mechanical Engineering, Opole University of Technology, Opole, Poland

    Grzegorz Krolczyk

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© 2023 The Author(s), under exclusive license to Springer Nature Singapore Pte Ltd.

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Singh, J., Bhardwaj, P., Kumar, R., Kumar, K., Dixit, S., Verma, V. (2023). Effect of Annealing Temperature on Phase Transformation of NiCr2O4 Nanoparticles and Evaluated Its Structural and Magnetic Properties. In: Prakash, C., Singh, S., Krolczyk, G. (eds) Advances in Functional and Smart Materials. Lecture Notes in Mechanical Engineering. Springer, Singapore. https://doi.org/10.1007/978-981-19-4147-4_7

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  • DOI: https://doi.org/10.1007/978-981-19-4147-4_7

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  • Publisher Name: Springer, Singapore

  • Print ISBN: 978-981-19-4146-7

  • Online ISBN: 978-981-19-4147-4

  • eBook Packages: EngineeringEngineering (R0)

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