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The Role of Processing Temperature in Equal Channel Angular Extrusion: Microstructure Mechanical Properties and Corrosion Resistance

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Proceedings of ICDMC 2019

Abstract

Equal channel angular extrusion, patented in Russia by V. M. Segal in 1977, has become a promising technique to enhance tensile strength and corrosion resistance of Mg alloys. It is believed that the processing temperature ensures the production of ECAE-processed billet without surface defects. Indeed, ECAE processing temperature affects microstructure, tensile behavior, and corrosion resistance of the material. Therefore, this chapter investigates the impact of ECAE pressing temperature on microstructure, mechanical behavior, and corrosion resistance of AZ80 Mg alloys. The processing temperature of 533 and 663 K was selected based on the recrystallization temperature of Mg alloys. As a result, the processing temperature has a substantial impact on material properties. The axial tensile strength and hardness decrease by 25.45% and 6.56%, respectively, due to thermal softening of materials. The corrosion resistance increases by 84% due to grain size reduction and distribution of secondary phases, when the ECAP-4P processing temperature is increased from 533 K to 663 K.

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References

  1. Song GL, Atrens A (1999) Corrosion mechanisms of magnesium alloys. Adv Eng Mater 1(1):11–33

    Article  Google Scholar 

  2. Kulekci MK (2008) Magnesium and its alloys applications in automotive industry. Int J Adv Manuf Technol 39(9–10):851–865

    Article  Google Scholar 

  3. Wu G, Fan Y, Gao H, Zhai C, Zhu YP (2005) The effect of Ca and rare earth elements on the microstructure, mechanical properties and corrosion behavior of AZ91D. Mater Sci Eng, A 408(1–2):255–263

    Article  Google Scholar 

  4. Chen B, Lin DL, Jin L, Zeng XQ, Lu C (2008) Equal-channel angular pressing of magnesium alloy AZ91 and its effects on microstructure and mechanical properties. Mater Sci Eng, A 483:113–116

    Article  Google Scholar 

  5. Kim WJ, Hong SI, Kim YS, Min SH, Jeong HT, Lee JD (2003) Texture development and its effect on mechanical properties of an AZ61 Mg alloy fabricated by equal channel angular pressing. Acta Mater 51(11):3293–3307

    Article  Google Scholar 

  6. Shaeri MH, Shaeri M, Ebrahimi M, Salehi MT, Seyyedein SH (2016) Effect of ECAP temperature on microstructure and mechanical properties of Al–Zn–Mg–Cu alloy. Prog Nat Sci: Mater Int 26(2):182–191

    Article  Google Scholar 

  7. Valiev RZ, Langdon TG (2006) Principles of equal-channel angular pressing as a processing tool for grain refinement. Prog Mater Sci 51(7):881–981

    Article  Google Scholar 

  8. Estrin Y, Vinogradov A (2013) Extreme grain refinement by severe plastic deformation: a wealth of challenging science. Acta Mater 61(3):782–817

    Article  Google Scholar 

  9. Avvari M, Narendranath S (2014) Influence of Route-R on wrought magnesium AZ61 alloy mechanical properties through equal channel angular pressing. J Magnes Alloys 2(2):159–164

    Article  Google Scholar 

  10. Sklenicka V, Dvorak J, Svoboda M, Kral P, Kvapilova M (2012) Equal-channel angular pressing and creep in ultrafine-grained aluminium and its alloys. In: Aluminium alloys-new trends in fabrication and applications (InTech)

    Google Scholar 

  11. Avvari M, Narendranath S (2018) Effect of secondary Mg 17 Al 12 phase on AZ80 alloy processed by equal channel angular pressing (ECAP). Silicon 10(1):39–47

    Article  Google Scholar 

  12. Parshikov RA, Rudskoy AI, Zolotov AM, Tolochko OV (2013) Technological problems of equal channel angular pressing. Rev Adv Mater Sci 34:26–36

    Google Scholar 

  13. Naik GM, Gote GD, Narendranath S, Kumar SS (2018) The impact of homogenization treatment on microstructure microhardness and corrosion behavior of wrought AZ80 magnesium alloys in 3.5 wt% NaCl solution. Mater Res Express 5(8):5

    Google Scholar 

  14. Naik GM, Gote GD, Narendranath S (2018) Microstructural and Hardness evolution of AZ80 alloy after ECAP and post-ECAP processes. Mater Today: Proc 5(9):17763–17768

    Google Scholar 

  15. Naik GM, Narendranath S, Kumar SS (2019) Effect of ECAP Die Angles on Microstructure Mechanical Properties and Corrosion Behavior of AZ80 Mg Alloy. J Mater Eng Perform 28(5):2610–2619

    Article  Google Scholar 

  16. Naik GM, Gote GD, Narendranath S, Kumar SS (2018) Effect of grain refinement on the performance of AZ80 Mg alloys during wear and corrosion. Adv Mater Res 7(2):105

    Google Scholar 

  17. Naik GM, Narendranath S, Kumar SS, Sahu S (2019) Effect of Annealing and Aging Treatment on Pitting Corrosion Resistance of Fine-Grained Mg-8% Al-0.5% Zn Alloy. JOM 71(12):4758–4768

    Article  Google Scholar 

  18. Gajanan MN, Narendranath S, Satheesh Kumar SS (2019) Influence of ECAP processing routes on microstructure mechanical properties and corrosion behavior of AZ80 Mg alloy. In: AIP Conference Proceedings, vol 2082(1), pp 030016

    Google Scholar 

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Acknowledgements

This work was supported by DRDO-NRB, Government of India, under grant number NRB/4003/PG/366.

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Correspondence to Gajanan M. Naik .

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Naik, G.M., Narendranath, S., Satheesh Kumar, S.S. (2020). The Role of Processing Temperature in Equal Channel Angular Extrusion: Microstructure Mechanical Properties and Corrosion Resistance. In: Yang, LJ., Haq, A., Nagarajan, L. (eds) Proceedings of ICDMC 2019. Lecture Notes in Mechanical Engineering. Springer, Singapore. https://doi.org/10.1007/978-981-15-3631-1_25

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  • DOI: https://doi.org/10.1007/978-981-15-3631-1_25

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