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The Study of Properties of Mechanochemical and Ultrasonic Treated BaO/ZrO2 Composites

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Nanomaterials and Nanocomposites, Nanostructure Surfaces, and Their Applications

Abstract

Nanosized BaO/ZrO2 = 1:1 compositions were successfully synthesized by mechanochemical (MChT for 4 h) and ultrasonic (UST for 1 and 2 h) treatment methods from oxides taken in molecular ratio 1:1. XRD and TEM results showed that obtained samples consist the particles about 15 nm after MChT and 1 h UST and 35 nm after 2 h UST. The isotropic destruction of zirconia, mesoporous powder formation and particle agglomeration with irregular shape occur. The photocatalytic properties of barium/zirconium oxide mixtures were examined in the water solution of prometryn degradation reaction. The activity of studied samples was increased after their MChT and USD activation.

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Acknowledgements

This work was supported by NASU Programs: Fundamental Research “New Functional Substances and Materials for Chemical Engineering” (projects 07-17/18, 13-(19-21)) and Program for Young Scientists Discovery Project “Synthesis of selective catalysts for obtaining of pure hydrogen from ethanol at low temperatures” (project 22/02-(2020-21(2))).

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Correspondence to Olena Sachuk .

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Sachuk, O. et al. (2023). The Study of Properties of Mechanochemical and Ultrasonic Treated BaO/ZrO2 Composites. In: Fesenko, O., Yatsenko, L. (eds) Nanomaterials and Nanocomposites, Nanostructure Surfaces, and Their Applications . Springer Proceedings in Physics, vol 279. Springer, Cham. https://doi.org/10.1007/978-3-031-18096-5_11

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