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TiOx/Cr2O3 Heating Coatings for Injection Molding of Polyamide

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Enhanced Material, Parts Optimization and Process Intensification (EMPOrIA 2020)

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Abstract

Variotherm injection molding processes are used to increase the quality of molded parts. Currently, tempering systems exhibit low temperature gradients or require additional process steps. A heating system applied directly on the cavity surface of the mold tool combines two benefits: high temperature gradients without additional process steps. In this study, a heating coating made of TiOx/Cr2O3 was applied on the surface of a tooling steel to control the cavity temperature by Joule heating. The heating coating is electrically insulated from the substrate by an Al2O3 coating. Homogeneity of temperature distribution was investigated as well as thermal durability for processing polyamide in the temperature range from 70 °C to 220 °C. The coating system withstood 5,000 thermal cycles at high heating rates and without degradation.

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References

  1. Bonten, C.: Kunststofftechnik: Einführung und Grundlagen (Plastics Technology: Introduction and Basics). Einführung und Grundlagen, 1st edn. Carl Hanser Fachbuchverlag, München (2014)

    Google Scholar 

  2. Johannaber, F., Michaeli, W.: Handbuch Spritzgießen. Carl Hanser Verlag GmbH & Co. KG, München (2004)

    Google Scholar 

  3. Moayyedian, M., Abhary, K., Marian, R.: Gate design and filling process analysis of the cavity in injection molding process. Adv. Manuf. (2016). https://doi.org/10.1007/s40436-016-0138-5

    Article  Google Scholar 

  4. Tredoux, L., Satoh, I.: Investigation of wave-like flow marks in injection molding: flow visualization and micro-geometry. Polymer Eng. Sci. 39, 2233–2241 (1999)

    Article  CAS  Google Scholar 

  5. Giessauf, J., Pillwein, G., Steinbichler, G.: Werkzeugtemperierung: die variotherme temperierung wird produktionstauglich (mold temperature control: variotherm temperature control is fit for production). Kunststoffe 98, 87–92 (2008)

    Google Scholar 

  6. Prudenziati, M.: Development and the Implementation of High-Temperature Reliable Heaters in Plasma Spray Technology. J. Therm. Spray Technol. (2008). https://doi.org/10.1007/s11666-008-9164-6

    Article  Google Scholar 

  7. Luth, J., Winkelmann, M., Wüst, F., Hartmann, S., Trenkle, F., Krieg, P., Killinger, A.: Thin, metallic heating coatings, manufactured by means of suspension spraying. Thermal Spray Bull. 12, 72–76 (2019)

    Google Scholar 

  8. Scheitz, S., Toma, F.-L., Berger, L.-M., Puschmann, R., Sauchuck, V., Kusnezoff, M.: Thermally sprayed multilayer ceramic heating elements. Thermal Spray Bull. 11, 88–92 (2011)

    Google Scholar 

  9. Berger, L.-M., Toma, F.-L., Scheitz, S., Trache, R., Börner, T.: Thermisch gespritzte Schichten im System Al2O3-Cr2O3-TiO2 - ein Update. Mat.-wiss. u. Werkstofftech (2014). https://doi.org/10.1002/mawe.201400260

  10. Trache, R., Berger, L.-M., Toma, F.-L., Saaro, S., Lima, R., Marple, B.: Electrical resistivity of thermally sprayed Cr2O3-TiO2 coatings. In: Conference Proceedings: Int. Thermal Spray Conference, 27–29 September 2011, Hamburg (2011)

    Google Scholar 

  11. Hayfield, P.C.S.: Electrode material, electrode and electrochemical cell Patent US4422917, 27 December 1983

    Google Scholar 

  12. Berger, L.-M., Stahr, C.C., Saaro, S., Thiele, S., Woydt, M., Kelling, N.: Dry sliding up to 7.5 m/s and 800 °C of thermally sprayed coatings of the TiO2–Cr2O3 system and (Ti,Mo)(C,N)–Ni(Co). Wear (2009). https://doi.org/https://doi.org/10.1016/j.wear.2008.12.105

  13. Wang, C.C., Akbar, S.A., Madou, M.J.: Ceramic Based Resistive Sensors. J. Electroceram. 2, 273–282 (1998)

    Article  CAS  Google Scholar 

  14. Bobzin, K., Wietheger, W., Knoch, M.A., Schacht, A.: Heating behaviour of plasma sprayed TiOx/Cr2O3 coatings for injection moulding. Surf. Coat. Technol. (2020). https://doi.org/10.1016/j.surfcoat.2020.126199

    Article  Google Scholar 

  15. Liu, Y., West, A.R.: Semiconductor-Insulator Transition in Undoped Rutile, TiO2 Ceramics. J. Am. Ceram. Soc. (2013). https://doi.org/10.1111/jace.12025

    Article  Google Scholar 

Download references

Acknowledgement

The presented investigations were carried out at RWTH Aachen University within the framework of the Collaborative Research Centre SFB1120-236616214 “Precision Melt Engineering” and funded by the Deutsche Forschungsgemeinschaft e.V. (DFG, German Research Foundation). The sponsorship and support is gratefully acknowledged.

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Correspondence to Andreas Schacht .

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Bobzin, K., Wietheger, W., Heinemann, H., Schacht, A. (2021). TiOx/Cr2O3 Heating Coatings for Injection Molding of Polyamide. In: Reisgen, U., Drummer, D., Marschall, H. (eds) Enhanced Material, Parts Optimization and Process Intensification. EMPOrIA 2020. Lecture Notes in Mechanical Engineering. Springer, Cham. https://doi.org/10.1007/978-3-030-70332-5_8

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  • DOI: https://doi.org/10.1007/978-3-030-70332-5_8

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  • Publisher Name: Springer, Cham

  • Print ISBN: 978-3-030-70331-8

  • Online ISBN: 978-3-030-70332-5

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