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Phase Formation of Zinc Titanate Precursor Powders Prepared by a Hydrothermal Process in Various pH Environments

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Abstract

For the precursor, powders were calcined at 773 K (500 °C) for 1 hour. The anatase TiO2 and ZnO appear as the predominant and minor phases, respectively, when the precursor powders are obtained at pH 5. The phases of Zn2Ti3O8, anatase TiO2, and ZnO coexist for the precursor powders obtained at pH 7. In addition, the Zn2Ti3O8 and ZnO are the predominant and minor phases, respectively, for the precursor powders obtained at pH 9.

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The authors sincerely thank the National Science Council of Taiwan for its financial support under NSC 100-2221-E-037-001. The authors also gratefully acknowledge Professor K. C. Lee of Department of Fragrance and Cosmetic Science, for his suggestions regarding the manuscript preparation, and the help of Mr. S. Y. Yao for assistance with the TEM.

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Authors and Affiliations

  1. Department of Materials Science and Engineering, National Cheng Kung University, 1 Ta-Hsueh Road, Tainan, 70101, Taiwan ROC

    Cheng-Li Wang (Graduate Student), Weng-Sing Hwang (Professor), Hsueh-Liang Chu (Graduate Student) & Wang-Long Li (Professor)

  2. Institute of Nanotechnology and Microsystems Engineering, National Cheng Kung University, 1 Ta-Hsueh Road, Tainan, 70101, Taiwan ROC

    Weng-Sing Hwang (Professor) & Wang-Long Li (Professor)

  3. Department of Fragrance and Cosmetic Science, Kaohsiung Medical University, 100 Shih-Chuan 1st Road, Kaohsiung, 80782, Taiwan ROC

    Horng-Huey Ko (Professor) & Moo-Chin Wang (Professor)

  4. Department of Materials Science and Engineering, National United University, 1 Lein-Da, Kung-Ching Li, Miao-Li, 36003, Taiwan ROC

    Chi-Shiung Hsi (Professor)

  5. Department of Mechanical Engineering, National Kaohsiung University of Applied Sciences, 415 Chien-Kung Road, Kaohsiung, 80782, Taiwan ROC

    Kuo-Ming Chang (Professor)

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  1. Cheng-Li Wang
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  2. Weng-Sing Hwang
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  3. Hsueh-Liang Chu
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  4. Horng-Huey Ko
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  5. Chi-Shiung Hsi
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  6. Wang-Long Li
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  7. Kuo-Ming Chang
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  8. Moo-Chin Wang
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Correspondence to Moo-Chin Wang.

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Manuscript submitted December 15, 2013.

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Wang, CL., Hwang, WS., Chu, HL. et al. Phase Formation of Zinc Titanate Precursor Powders Prepared by a Hydrothermal Process in Various pH Environments. Metall Mater Trans A 45, 2689–2698 (2014). https://doi.org/10.1007/s11661-014-2282-5

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