Abstract
1-D nanostructures are deemed to be important building blocks for future optical and optoelectronic nanodevices. We have used electrospinning methods to synthesize nanofibers and freestanding, non-woven nanofibers membranes of single phase yttrium titanate and ErxY2−xTi2O7 (x = 0–12 %) with diameters less than 150 nm and have characterized the physical, thermal and optical properties. We have demonstrated that such fibers can be synthesized at a relatively low cost and high production volume with a narrow diameter range. No clear phases are observed up to a calcination temperature of 700 °C and pyrochlore phase appear at 725 °C which are also confirmed by the TGA. Single pyrochlore phase is observed at temperatures greater than 900 °C. No other oxide phases are present.
References
Vassen R, Sebold D, Stoever D (2008) Ceram Eng Sci Proc 28:27
Ren W, Trolier-McKinstry S, Randall CA, Shrout TR (2001) J Appl Phys 89:767
Wuensch BJ, Eberman KW, Heremans C et al (2000) Solid State Ionics 129:111
Ewing RC, Weber WJ, Lian J (2004) J Appl Phys 95:5949
Johnson MB, James DD, Bourque A et al (2009) J Solid State Chem 182:725–729
Goldschmidt D, Tuller HL (1986) Phys Rev B 34:5558
Matteuccci F, Cruciani G, Dondi M, Baldi G, Barzanti A (2007) Acta Mater 55:2229
Abe R, Higashi M, Sayama K, Abe Y, Sugihara H (2006) J Phys Chem B 110:2219–2226
Tao TT, Wang LX, Zhang QT (2009) J Alloys Compd 486:606
Langlet M, Jenouvrier P, Fick J et al (2003) J Sol–Gel Sci Tech 26:985–988
Chen C, Gong W, Chen T et al (2012) Mater Lett 68:137–139
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The corresponding author is a member of the Materials Technology Center at Illinois University, Carbondale.
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Mondal, K., Hartman, K., Dasgupta, D. et al. Synthesis and characterization of Y2Ti2O7 and ErxY2−xTi2O7 nanofibers. J Sol-Gel Sci Technol 73, 265–269 (2015). https://doi.org/10.1007/s10971-014-3574-3
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DOI: https://doi.org/10.1007/s10971-014-3574-3