Skip to main content
Log in

Gas-Chromatographic Identification and Determination of the Content of Normalakanes in Fuels for Jet Engines

  • 55 YEARS OF CHEMMOTOLOGY
  • Published:
Chemistry and Technology of Fuels and Oils Aims and scope

A new method was developed for the identification and quantitative determination of normal alkanes in jet fuels and kerosene fractions on the basis of simulated distillation. Normal alkanes were identified on the chromatogram by their retention times, and their concentrations were calculated by absolute calibration, the results of which correspond to the results obtained by standard addition and internal standard methods. The developed method is simple and productive and can be carried out using standard analytical equipment.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1.
Fig. 2.
Fig. 3.

Similar content being viewed by others

References

  1. E. T. Denisov, G. I. Kovalov, Oxidation and Stabilization of Jet Engine Fuels [in Russian], Khimiya, Moscow (1983), 272 pp.

    Google Scholar 

  2. Aviation Fuels Technical Review, Chevron Corporation (2007), 90 pp.

  3. A. P. P. Pires, Y. Han, J. Kramlich, et al., BioResources, 13(2), 2632-2657 (2018).

    Article  CAS  Google Scholar 

  4. E. A. Konyaev, M. L. Nemchikov, M. G. Golubeva, Chemmotology of Jet Engine Fuels [in Russian], MGTU GA. Moscow (2009), 66 pp.

    Google Scholar 

  5. D. J. Cookson, Latten J. L., Shaw I. M., et al., Fuel, 64, 509-519 (1985).

    Article  CAS  Google Scholar 

  6. O. Yu. Kuznetsova, G. M. Balak, A. N. Privalenko, Mezhdunarodnyi Tekhniko-Ekonomicheskoi Zhurnal, No. 6, 100-108 (2015).

  7. Jet Fuel Analysis by High Resolution TOFMS: The Combined Power of El, Cl, and Accurate Mass, LECO CORPORATION, Form No. 203-821-448, pp. 1-3 (2013).

  8. Yu. V. Pokonova, Neft’i Nefteprodukty [in Russian], Mir i Sem’ya, St. Petersburg (2003), 904 pp.

    Google Scholar 

  9. Ch. L. Stuckey, Anal. Chim. Acta., 60, 47-56 (1972).

    Article  CAS  Google Scholar 

  10. G. C. Blytas, D. L. Peterson, Analytical Chemistry, 39(12), 1434-1437 (1967).

    Article  CAS  Google Scholar 

  11. G. I. Safonova, L. M. Bulekova, Khimiya i Tekhnologiya Topliv i Masel, No. 10, 21-27 (1969).

  12. P. Cardinael, V. Peulon-Agasse, G. Coquerel, et al., J. Sep. Sci., 24, 109-115 (2001).

    Article  CAS  Google Scholar 

  13. A. F. Akhmetov, M. U. Imasheva, L. F. Korzhova, Bashkirskii Khimicheskii Zhurnal, 21, No. 1, 82-86 (2014).

    CAS  Google Scholar 

  14. N. Halim, A Kuntom, Determination of Hydrocarbons (n-Alkanes) in Oil Matrix, http://mpob.goy.my

  15. F. Islam, O. Granot, J. S. Mclndoe, Analytical Letters, 50(10), 1593-1601.

  16. U. Keshet, A. B. Fialkov, T Alon, et al., Chromatographia, 79, 741-754 (2016).

    Article  CAS  Google Scholar 

  17. K. M. Geem, S. P. Van Pyl, M. F. Reyniers, et al., J. Chromatogr. A, 1217(43), 6623-6633 (2010).

    Article  CAS  PubMed  Google Scholar 

  18. Y. Briker, Z. Ring, A. Iacchelli, et al., Energy&Fuel, 15, 996-1002 (2001).

    CAS  Google Scholar 

  19. K. D. Dietzel, J. L. Campbell, M. G. Bartlett, et al., J. Chromatogr. A, 1093(1-2), 11-20 (2005).

    Article  CAS  PubMed  Google Scholar 

  20. R. van der Westhuizen, M. Ajama, P. De Coning, et al., J. Chromatogr. A, 1218(28). 4478-4486 (2011).

    Article  CAS  PubMed  Google Scholar 

  21. Quantitative Detailed Analysis of a Petroleum Fraction Using GCxGC-TOFMS, LECO Corporation, Form No 203-821-254, pp. 1-3.

  22. W. Wang, Y. Liu, Z. Liu, et al., Energy&Fuels, 30,968-974 (2016).

    CAS  Google Scholar 

  23. Y. Li, R. Zhang, T. Wang, et al., Chemosphere, 158,154-162 (2016).

    Article  CAS  PubMed  Google Scholar 

  24. F. David, D. R. Gere, F. Scanlan, et al., J. Chromatogr. A., 842 (1,2), 309-319 (1999).

    Article  CAS  Google Scholar 

  25. J. Krupcik, D. Repka, S. Korenkiva, Petroleum and Coal, 40,183-187 (1998).

    CAS  Google Scholar 

  26. D. Papazova, A. Pavlova, J. Chromatogr. Science, 37,1-4 (1999).

    Article  CAS  Google Scholar 

  27. S. V. Cherepitsa, S. M. Bychkov, A, N. Kovalenko, et al., Khimiya i Tekhnologiya Topliv i Masel, No. 6, 45-48 (2002).

  28. O. Yu. Kuznetsova, G. M. Balak, A. N. Privalenko, et al., Fundamental’nye Issledovaniya, No. 8-2, 264-269 (2017).

  29. O. Yu. Kuznetsova, G. M. Balak, A. N. Privalenko, Identification of Fuels for Jet Engines and their Components by Simulated Distillation [in Russian], ITrudy 25 GosNII MO RF, No. 58,327-337 (2018).

  30. V. F. Apraksin, Quantitative Gas Chromatographic Analysis: Procedural Guidelines to Fulfilment of Laboratory Works in Course of Physicochemical Methods of Analysis [in Russian], CPKhFA, St. Petersburg (1999), 25 pp.

    Google Scholar 

  31. I. G. Zenkevich, D. V. Prokof’ev, Sorbtsionnye i Khromatograficheskie Protsessy, 17, No. 2,228-242 (2017).

    CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to G. M. Balak.

Additional information

Translated from Khimiya i Tekhnologiya Topliv i Masel, No. 3, pp. 9 — 15, May — June, 2019.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Balak, G.M., Kuznetsova, O.Y. & Privalenko, A.N. Gas-Chromatographic Identification and Determination of the Content of Normalakanes in Fuels for Jet Engines. Chem Technol Fuels Oils 55, 221–231 (2019). https://doi.org/10.1007/s10553-019-01025-5

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10553-019-01025-5

Key words

Navigation