# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' dk_tfb in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 241.99 _exptl_crystal_F_000 592.00 _reflns_d_resolution_high 0.8000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.4710 _cell_length_b 10.4957 _cell_length_c 11.9774 _cell_angle_alpha 84.941 _cell_angle_beta 83.633 _cell_angle_gamma 69.084 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24951.09 22679.90 241.19 o 3 0 0 7050.24 7345.66 100.37 o 4 0 0 5434.48 5957.73 93.61 o 5 0 0 9622.86 9777.59 83.62 o 6 0 0 942.45 931.59 26.43 o 7 0 0 3188.31 3221.08 44.97 o 8 0 0 338.97 366.16 23.02 o 9 0 0 2066.33 2102.57 48.14 o 10 0 0 418.62 447.31 30.27 o 11 0 0 232.40 207.23 20.50 o 12 0 0 255.15 251.66 28.24 o -11 1 0 5.64 7.39 16.31 o -10 1 0 936.21 1007.87 45.04 o -9 1 0 214.35 220.27 21.40 o -8 1 0 3027.97 3139.50 69.53 o -7 1 0 705.20 752.89 31.05 o -6 1 0 1089.95 1077.74 34.83 o -5 1 0 3399.98 3676.68 45.69 o -4 1 0 171.98 206.43 11.87 o -3 1 0 14665.18 14577.48 113.99 o -2 1 0 334.73 457.72 15.11 o -1 1 0 17587.06 17695.29 204.37 o 2 1 0 31690.49 28646.29 219.16 o 3 1 0 665.46 769.05 9.56 o 4 1 0 10721.02 11060.47 134.04 o 5 1 0 1938.95 2200.24 35.17 o 6 1 0 4136.67 4268.36 49.87 o 7 1 0 1964.65 1975.43 26.08 o 8 1 0 2115.36 2060.43 34.54 o 9 1 0 1964.35 1965.85 39.69 o 10 1 0 41.63 18.69 8.82 o 11 1 0 651.81 640.92 24.64 o 12 1 0 29.80 24.81 18.96 o -11 2 0 326.36 381.11 32.33 o -10 2 0 526.94 529.81 34.53 o -9 2 0 385.18 444.25 29.60 o -8 2 0 1501.36 1544.48 69.97 o -7 2 0 62.02 70.56 6.00 o -6 2 0 5532.79 5235.33 66.26 o -5 2 0 1201.17 1172.53 20.59 o -4 2 0 7447.89 7085.28 61.90 o -3 2 0 3841.18 3928.50 36.13 o -2 2 0 3250.43 3416.45 25.18 o -1 2 0 23869.69 21978.65 133.49 o 0 2 0 21966.12 20046.58 145.38 o 1 2 0 25858.73 23102.85 583.83 o 2 2 0 106.09 190.26 5.51 o 3 2 0 9850.83 10052.64 55.85 o 4 2 0 4923.45 4983.27 34.68 o 5 2 0 9113.54 9450.11 60.46 o 6 2 0 3378.35 3390.02 29.73 o 7 2 0 122.77 131.46 6.47 o 8 2 0 4106.81 4229.31 60.89 o 9 2 0 122.33 136.38 6.64 o 10 2 0 1355.26 1535.90 35.86 o 11 2 0 410.16 441.27 21.00 o 12 2 0 158.17 156.90 33.25 o -10 3 0 4.16 1.16 15.71 o -9 3 0 1371.05 1472.90 52.93 o -8 3 0 197.77 212.47 21.27 o -7 3 0 1309.13 1332.24 34.74 o -6 3 0 1502.27 1421.75 47.23 o -5 3 0 1668.59 1750.09 26.14 o -4 3 0 9845.86 9601.64 116.38 o -3 3 0 717.30 848.45 13.99 o -2 3 0 10306.53 10849.87 90.44 o -1 3 0 3472.51 3225.17 30.57 o 0 3 0 5845.63 6052.87 47.20 o 1 3 0 11927.39 11965.88 72.18 o 2 3 0 3058.31 3274.99 27.28 o 3 3 0 8697.95 8968.13 50.00 o 4 3 0 3.60 28.23 3.39 o 5 3 0 10754.98 10994.75 65.89 o 6 3 0 683.78 744.60 16.77 o 7 3 0 2968.37 2967.86 31.85 o 8 3 0 2315.05 2281.08 31.43 o 9 3 0 344.41 336.08 11.05 o 10 3 0 1858.93 1915.99 53.78 o 11 3 0 7.74 -0.08 10.93 o 12 3 0 603.14 589.53 29.25 o -10 4 0 338.52 370.35 31.03 o -9 4 0 494.26 502.51 49.14 o -8 4 0 254.78 274.05 23.82 o -7 4 0 1739.39 1743.74 41.90 o -6 4 0 235.58 202.67 11.45 o -5 4 0 6622.15 6333.14 148.53 o -4 4 0 675.67 703.49 18.56 o -3 4 0 6126.00 5994.82 111.65 o -2 4 0 5433.79 5594.84 60.31 o -1 4 0 4589.77 4439.76 36.71 o 0 4 0 26114.22 25781.44 162.09 o 1 4 0 20.79 42.17 3.55 o 2 4 0 16380.23 15680.59 91.70 o 3 4 0 313.64 330.09 7.87 o 4 4 0 11036.46 10907.76 81.46 o 5 4 0 3737.62 3611.34 31.98 o 6 4 0 961.31 961.65 15.22 o 7 4 0 4167.89 4136.29 65.74 o 8 4 0 58.26 64.65 5.42 o 9 4 0 3213.43 3364.44 81.94 o 10 4 0 448.31 354.42 20.67 o 11 4 0 618.41 659.15 29.40 o 12 4 0 302.09 271.89 21.30 o -9 5 0 2.62 -9.25 14.93 o -8 5 0 1002.58 1056.49 50.60 o -7 5 0 227.75 245.73 17.70 o -6 5 0 1006.19 1019.17 19.48 o -5 5 0 1045.95 999.18 22.67 o -4 5 0 1051.49 1139.25 28.96 o -3 5 0 6404.37 6247.17 92.52 o -2 5 0 5.02 30.59 6.42 o -1 5 0 9511.17 9603.76 75.85 o 0 5 0 5343.79 5387.06 42.14 o 1 5 0 8940.55 8900.44 103.51 o 2 5 0 9692.07 9458.82 58.33 o 3 5 0 3319.83 3677.62 30.64 o 4 5 0 8450.86 8420.66 72.40 o 5 5 0 3.99 23.50 5.73 o 6 5 0 6344.35 6499.38 81.63 o 7 5 0 908.54 835.29 17.84 o 8 5 0 3195.17 3317.61 47.40 o 9 5 0 2986.08 2964.99 46.95 o 10 5 0 327.77 308.69 19.45 o 11 5 0 930.73 920.07 38.07 o 12 5 0 0.37 -2.71 12.39 o 13 5 0 445.96 485.31 40.19 o -8 6 0 437.31 465.99 22.79 o -7 6 0 238.74 262.37 16.61 o -6 6 0 1087.55 1098.16 35.74 o -5 6 0 84.84 80.45 9.77 o -4 6 0 2086.59 2101.37 50.12 o -3 6 0 880.71 896.48 19.35 o -2 6 0 2822.76 2817.04 30.54 o -1 6 0 3578.91 3763.64 46.05 o 0 6 0 2750.59 2850.36 29.03 o 1 6 0 9561.29 9347.27 71.43 o 2 6 0 354.07 347.24 10.01 o 3 6 0 7415.54 7407.44 84.94 o 4 6 0 680.70 707.46 15.56 o 5 6 0 6818.98 6867.92 74.83 o 6 6 0 5153.60 5098.14 62.53 o 7 6 0 1341.54 1283.96 28.34 o 8 6 0 2185.60 2235.26 49.10 o 9 6 0 22.55 6.10 8.82 o 10 6 0 2023.82 2005.72 48.92 o 11 6 0 286.37 285.63 21.33 o 12 6 0 298.94 313.66 23.06 o -7 7 0 752.98 738.34 33.03 o -6 7 0 268.63 217.49 14.92 o -5 7 0 657.09 685.70 22.31 o -4 7 0 2108.92 2045.72 37.44 o -3 7 0 636.00 625.03 18.87 o -2 7 0 3674.06 3636.27 56.02 o -1 7 0 0.75 -3.69 3.69 o 0 7 0 4792.79 4699.92 41.98 o 1 7 0 1821.81 1814.14 21.20 o 2 7 0 5114.86 5052.97 52.16 o 3 7 0 4100.44 4045.51 42.59 o 4 7 0 674.40 677.65 14.16 o 5 7 0 8654.11 8628.88 73.92 o 6 7 0 137.60 101.16 18.50 o 7 7 0 4975.25 4962.31 62.08 o 8 7 0 832.20 783.23 24.02 o 9 7 0 1336.82 1283.63 41.18 o 10 7 0 1496.97 1450.07 36.13 o 11 7 0 82.63 100.95 14.89 o 12 7 0 692.85 686.48 33.43 o -6 8 0 117.74 112.50 15.27 o -5 8 0 1132.49 1126.94 37.96 o -4 8 0 122.32 83.90 13.98 o -3 8 0 2356.17 2338.55 49.81 o -2 8 0 902.08 937.57 31.85 o -1 8 0 1857.28 1910.26 26.34 o 0 8 0 3051.84 3084.53 32.41 o 1 8 0 166.92 202.89 7.29 o 2 8 0 4046.03 4129.21 53.12 o 3 8 0 134.31 138.00 7.76 o 4 8 0 5266.86 5368.39 82.88 o 5 8 0 1384.69 1355.74 26.56 o 6 8 0 2292.72 2253.35 47.58 o 7 8 0 2041.26 2081.82 40.73 o 8 8 0 36.98 51.46 11.79 o 9 8 0 1814.52 1837.10 39.91 o 10 8 0 117.98 101.44 12.09 o 11 8 0 911.85 933.71 36.21 o 12 8 0 191.95 183.62 20.25 o -5 9 0 296.61 253.94 20.75 o -4 9 0 589.57 586.70 27.64 o -3 9 0 1468.31 1493.51 41.30 o -2 9 0 145.15 138.10 11.12 o -1 9 0 2097.76 2047.57 40.66 o 0 9 0 224.52 228.83 16.76 o 1 9 0 3405.54 3383.99 62.88 o 2 9 0 1149.50 1213.21 37.01 o 3 9 0 2638.25 2601.74 55.31 o 4 9 0 3087.39 3164.17 51.59 o 5 9 0 877.80 874.31 27.38 o 6 9 0 4578.38 4572.58 83.22 o 7 9 0 6.45 13.64 11.33 o 8 9 0 2467.20 2473.47 47.81 o 9 9 0 1113.34 1061.08 32.18 o 10 9 0 579.53 572.96 29.30 o 11 9 0 839.88 781.93 43.18 o -4 10 0 682.55 726.49 50.20 o -3 10 0 48.29 40.05 21.08 o -2 10 0 1131.77 1160.13 39.29 o -1 10 0 660.68 629.22 34.65 o 0 10 0 866.94 810.26 31.94 o 1 10 0 3113.00 3140.56 73.94 o 2 10 0 190.97 152.94 15.73 o 3 10 0 2500.41 2553.53 57.72 o 4 10 0 5.36 -12.95 12.95 o 5 10 0 3430.02 3389.95 56.94 o 6 10 0 1513.13 1556.39 38.49 o 7 10 0 1085.66 1089.08 32.68 o 8 10 0 2035.35 2037.53 45.78 o 9 10 0 72.40 95.01 13.79 o 10 10 0 1672.10 1636.38 42.59 o 11 10 0 48.69 48.12 14.93 o -2 11 0 754.26 789.84 45.57 o -1 11 0 33.65 20.11 13.62 o 0 11 0 1528.35 1559.21 47.36 o 1 11 0 102.84 83.34 14.90 o 2 11 0 1878.15 1928.24 52.81 o 3 11 0 1009.68 1068.47 44.12 o 4 11 0 879.73 884.62 36.54 o 5 11 0 2349.36 2479.99 60.81 o 6 11 0 111.65 127.23 16.48 o 7 11 0 2247.65 2260.45 49.68 o 8 11 0 39.49 42.13 12.28 o 9 11 0 1460.20 1447.39 41.10 o 10 11 0 472.35 442.38 24.81 o 0 12 0 413.16 420.20 50.58 o 1 12 0 453.90 447.08 34.43 o 2 12 0 1217.15 1263.26 45.26 o 3 12 0 58.62 54.47 16.91 o 4 12 0 1644.92 1697.46 52.73 o 5 12 0 166.91 177.02 28.31 o 6 12 0 1440.78 1381.84 40.40 o 7 12 0 715.43 740.27 30.41 o 8 12 0 528.15 526.27 26.63 o 9 12 0 903.38 910.89 34.69 o 4 13 0 608.94 612.88 34.40 o 5 13 0 577.66 560.08 33.47 o -8 -12 1 718.91 809.43 37.19 o -7 -12 1 964.52 943.96 39.24 o -6 -12 1 316.89 331.04 24.42 o -5 -12 1 1658.83 1605.98 73.57 o -4 -12 1 2.59 -10.93 27.13 o -3 -12 1 1245.36 1352.87 55.79 o -2 -12 1 344.61 330.84 29.71 o -1 -12 1 607.34 730.99 51.10 o 0 -12 1 620.18 606.28 38.54 o -10 -11 1 744.43 724.00 34.81 o -9 -11 1 123.55 115.30 16.38 o -8 -11 1 1516.38 1589.12 48.11 o -7 -11 1 2.63 3.36 11.39 o -6 -11 1 2122.15 2222.85 49.20 o -5 -11 1 519.01 499.93 24.11 o -4 -11 1 1252.20 1291.79 42.75 o -3 -11 1 1072.41 987.55 60.09 o -2 -11 1 342.21 365.86 29.79 o -1 -11 1 1606.38 1566.51 58.16 o 0 -11 1 14.16 2.67 15.39 o 1 -11 1 1066.37 1117.98 52.43 o 2 -11 1 300.32 287.18 22.66 o -11 -10 1 821.03 784.98 45.51 o -10 -10 1 5.71 23.99 13.22 o -9 -10 1 1674.10 1703.24 67.42 o -8 -10 1 882.11 841.28 29.56 o -7 -10 1 882.73 936.08 30.72 o -6 -10 1 1735.59 1766.66 41.51 o -5 -10 1 682.85 627.87 25.03 o -4 -10 1 2739.35 2766.60 63.88 o -3 -10 1 58.50 71.59 14.12 o -2 -10 1 3416.28 3600.52 69.19 o -1 -10 1 868.58 824.90 39.12 o 0 -10 1 1673.84 1717.06 69.09 o 1 -10 1 981.35 960.46 43.20 o 2 -10 1 193.31 196.40 17.75 o 3 -10 1 1254.45 1234.81 77.69 o 4 -10 1 16.73 5.58 18.11 o -11 -9 1 336.56 353.11 25.26 o -10 -9 1 878.58 867.00 29.14 o -9 -9 1 1750.57 1811.48 40.10 o -8 -9 1 87.92 83.81 11.74 o -7 -9 1 1870.30 1969.97 41.89 o -6 -9 1 502.12 538.08 21.80 o -5 -9 1 3278.07 3390.45 54.74 o -4 -9 1 1697.30 1664.46 39.51 o -3 -9 1 1268.74 1259.37 36.83 o -2 -9 1 2222.13 2140.69 48.86 o -1 -9 1 563.77 552.04 16.82 o 0 -9 1 4030.29 4012.92 58.56 o 1 -9 1 69.35 55.92 12.25 o 2 -9 1 1565.84 1571.72 34.39 o 3 -9 1 530.79 548.57 25.73 o 4 -9 1 655.18 707.89 30.47 o 5 -9 1 713.47 767.12 33.18 o -12 -8 1 473.04 502.68 29.39 o -11 -8 1 120.54 134.43 17.90 o -10 -8 1 1710.33 1655.91 38.93 o -9 -8 1 111.26 111.26 11.86 o -8 -8 1 2438.24 2438.31 39.65 o -7 -8 1 2039.14 1962.59 34.02 o -6 -8 1 855.36 802.69 25.05 o -5 -8 1 2826.03 2824.75 44.78 o -4 -8 1 127.54 145.66 7.51 o -3 -8 1 4646.07 4707.54 58.30 o -2 -8 1 54.93 49.97 9.31 o -1 -8 1 4626.97 4795.14 54.39 o 0 -8 1 711.82 740.49 23.14 o 1 -8 1 866.80 883.19 25.94 o 2 -8 1 2547.91 2580.89 42.65 o 3 -8 1 263.37 259.24 17.66 o 4 -8 1 2006.85 2073.56 79.34 o 5 -8 1 22.65 -5.08 13.40 o 6 -8 1 697.02 674.68 31.78 o -12 -7 1 44.17 41.12 17.34 o -11 -7 1 957.97 987.02 37.83 o -10 -7 1 621.04 603.65 29.34 o -9 -7 1 960.67 895.43 31.84 o -8 -7 1 1968.26 1961.68 42.37 o -7 -7 1 21.93 32.54 7.14 o -6 -7 1 8226.62 8195.00 73.30 o -5 -7 1 621.68 639.97 16.49 o -4 -7 1 6038.83 6040.77 69.23 o -3 -7 1 2217.20 2323.44 24.87 o -2 -7 1 1571.27 1643.82 25.74 o -1 -7 1 6242.61 6224.16 61.50 o 0 -7 1 572.18 563.08 16.46 o 1 -7 1 4042.45 3964.12 48.68 o 2 -7 1 788.45 759.58 16.14 o 3 -7 1 2622.96 2582.91 51.12 o 4 -7 1 1308.68 1337.77 34.63 o 5 -7 1 797.60 769.36 24.23 o 6 -7 1 927.48 908.16 34.65 o 7 -7 1 6.59 10.91 12.68 o -12 -6 1 216.00 222.50 21.48 o -11 -6 1 730.28 754.55 36.07 o -10 -6 1 77.35 64.99 12.93 o -9 -6 1 3846.45 4032.36 81.51 o -8 -6 1 379.01 382.47 28.72 o -7 -6 1 4108.11 3937.72 53.02 o -6 -6 1 3155.60 3269.17 51.07 o -5 -6 1 3626.79 3601.26 47.02 o -4 -6 1 8410.03 8524.75 60.32 o -3 -6 1 402.03 372.04 9.69 o -2 -6 1 8220.45 8361.75 68.70 o -1 -6 1 1266.41 1419.16 23.62 o 0 -6 1 4907.65 4977.89 51.72 o 1 -6 1 4771.35 4794.91 48.69 o 2 -6 1 1395.62 1379.95 21.39 o 3 -6 1 3303.44 3348.36 47.86 o 4 -6 1 29.33 13.77 7.36 o 5 -6 1 2116.21 2026.46 52.36 o 6 -6 1 259.77 271.39 15.52 o 7 -6 1 1079.12 1120.47 32.10 o 8 -6 1 412.14 414.39 21.66 o -12 -5 1 585.98 576.06 30.30 o -11 -5 1 126.73 104.88 14.84 o -10 -5 1 1186.43 1155.08 37.47 o -9 -5 1 1511.45 1478.89 41.50 o -8 -5 1 196.69 176.23 8.61 o -7 -5 1 4081.86 4068.95 69.56 o -6 -5 1 274.20 270.47 10.07 o -5 -5 1 11727.72 11528.15 187.56 o -4 -5 1 1491.11 1604.97 20.40 o -3 -5 1 6623.47 6812.85 48.96 o -2 -5 1 7805.54 7713.75 50.63 o -1 -5 1 9448.14 9400.03 104.18 o 0 -5 1 11137.67 10882.22 84.54 o 1 -5 1 8.44 20.65 4.63 o 2 -5 1 5373.03 5169.02 57.55 o 3 -5 1 345.65 332.60 15.87 o 4 -5 1 4143.71 4101.90 66.77 o 5 -5 1 1561.69 1486.82 30.31 o 6 -5 1 353.77 332.89 13.16 o 7 -5 1 1768.35 1807.55 57.90 o 8 -5 1 27.38 39.38 12.66 o 9 -5 1 713.60 759.90 33.66 o -12 -4 1 383.94 355.45 24.78 o -11 -4 1 192.50 190.67 18.41 o -10 -4 1 1690.88 1768.75 48.71 o -9 -4 1 117.41 90.61 11.30 o -8 -4 1 3385.93 3503.53 123.50 o -7 -4 1 446.02 459.43 13.34 o -6 -4 1 1874.65 1758.09 28.28 o -5 -4 1 3198.29 3394.21 34.29 o -4 -4 1 2049.02 1997.83 24.42 o -3 -4 1 10303.77 10618.17 64.07 o -2 -4 1 39.05 50.18 2.92 o -1 -4 1 21631.86 21602.62 156.33 o 0 -4 1 2070.77 2270.70 33.07 o 1 -4 1 12540.18 12645.49 79.72 o 2 -4 1 4868.57 5067.54 40.30 o 3 -4 1 900.22 826.48 13.94 o 4 -4 1 6413.55 6458.92 114.17 o 5 -4 1 144.50 122.13 5.96 o 6 -4 1 3199.54 3034.23 108.58 o 7 -4 1 68.29 95.79 12.15 o 8 -4 1 1385.88 1379.24 49.16 o 9 -4 1 554.56 568.06 29.12 o 10 -4 1 151.46 151.14 19.35 o -11 -3 1 1141.34 1142.02 58.87 o -10 -3 1 357.10 336.71 20.67 o -9 -3 1 1475.54 1411.51 41.15 o -8 -3 1 3102.73 3284.00 85.58 o -7 -3 1 331.40 357.86 18.84 o -6 -3 1 7204.40 7467.53 147.41 o -5 -3 1 302.05 369.62 11.57 o -4 -3 1 19453.49 19531.91 138.66 o -3 -3 1 3414.14 3601.20 39.33 o -2 -3 1 14379.35 13913.37 92.22 o -1 -3 1 7020.34 7088.00 52.96 o 0 -3 1 3550.66 3756.99 27.37 o 1 -3 1 16202.30 15852.71 83.49 o 2 -3 1 662.48 718.90 9.33 o 3 -3 1 6073.41 5812.77 51.14 o 4 -3 1 1718.86 1680.24 18.05 o 5 -3 1 5147.77 4746.98 73.89 o 6 -3 1 2853.91 2815.19 54.34 o 7 -3 1 864.14 923.01 36.27 o 8 -3 1 1168.99 1132.31 47.64 o 9 -3 1 20.19 28.20 14.03 o 10 -3 1 731.53 782.19 42.02 o -12 -2 1 435.30 508.80 28.48 o -11 -2 1 486.17 466.95 26.81 o -10 -2 1 383.40 421.46 23.64 o -9 -2 1 2519.77 2557.55 80.23 o -7 -2 1 4551.32 4501.51 103.88 o -6 -2 1 2337.71 2467.14 70.99 o -5 -2 1 9690.12 10068.33 303.24 o -4 -2 1 27380.39 26959.06 369.84 o -3 -2 1 3893.31 3937.54 60.18 o -2 -2 1 23318.04 22364.34 193.36 o -1 -2 1 351.41 393.28 5.28 o 0 -2 1 16714.63 16404.91 116.95 o 1 -2 1 2609.88 2821.98 19.51 o 2 -2 1 6724.63 6646.31 49.15 o 3 -2 1 10335.42 10530.47 55.39 o 4 -2 1 973.08 914.80 21.78 o 5 -2 1 5505.43 5730.58 52.22 o 6 -2 1 1.57 2.08 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31.03 6.04 o -6 0 1 3740.04 3760.28 70.39 o -5 0 1 410.61 468.25 12.36 o -4 0 1 25954.16 25629.12 435.39 o -3 0 1 16153.46 16346.87 83.63 o -2 0 1 3840.89 3863.03 45.97 o 2 0 1 780.24 944.73 18.40 o 3 0 1 7934.42 8236.44 87.54 o 4 0 1 8287.91 8273.48 82.46 o 5 0 1 741.53 829.39 16.91 o 6 0 1 6510.30 6625.13 74.76 o 7 0 1 54.73 56.12 9.60 o 8 0 1 3896.77 3949.34 102.73 o 9 0 1 362.62 370.25 14.57 o 10 0 1 919.03 964.85 30.27 o 11 0 1 452.70 440.58 32.32 o 12 0 1 60.17 17.29 15.70 o -11 1 1 493.84 529.37 33.27 o -10 1 1 36.34 45.57 18.35 o -9 1 1 1591.78 1681.03 130.41 o -8 1 1 810.58 724.35 56.59 o -7 1 1 1756.29 1745.81 54.89 o -6 1 1 2389.09 2537.22 38.11 o -5 1 1 580.73 613.66 12.05 o -4 1 1 16131.48 16100.09 108.73 o -3 1 1 193.23 210.93 5.46 o -2 1 1 22627.97 22242.39 206.56 o -1 1 1 11455.69 10736.62 68.47 o 2 1 1 278.06 364.70 8.70 o 3 1 1 2120.62 2287.08 22.98 o 4 1 1 5.07 33.37 3.44 o 5 1 1 13985.21 14513.47 125.42 o 6 1 1 1459.49 1472.04 17.86 o 7 1 1 1602.36 1663.08 28.07 o 8 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