##############################################################################
#                                                                            #
# This CIF contains the data in a paper accepted for publication in          #
# Acta Crystallographica Section E. It conforms to the requirements of       #
# Notes for Authors for Acta Crystallographica Section E, and has been       #
# peer reviewed under the auspices of the IUCr Commission on Journals.       #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic.                                       #
#                                                                            #
# Software is freely available for graphical display of the structure(s)     #
# in this CIF. For information consult the CIF software page                 #
# http://www.iucr.org/resources/cif/software.                                #
#                                                                            #
# This file may be used for bona fide research purposes within the           #
# scientific community so long as proper attribution is given to the journal # 
# article from which it was obtained.                                        #
#                                                                            #
##############################################################################
data_I
_audit_creation_method     SHELXL97
_chemical_name_systematic
;
Sodium N-bromo-2-chlorobenzenesulfonamidate sesquihydrate
;
_chemical_name_common     ?
_chemical_formula_moiety     'Na +, C6 H4 Br Cl N O2 S -, 1.5(H2 O)'
_chemical_formula_sum     'C6 H7 Br Cl N Na O3.5 S'
_chemical_formula_iupac     'Na + , C6 H4 Br Cl N O2 S - , 1.5H2 O'
_chemical_formula_weight     319.53
_chemical_melting_point     ?
_symmetry_cell_setting     monoclinic
_symmetry_space_group_name_H-M     'C 2/c'
_symmetry_space_group_name_HALL     '-C 2yc'
loop_
    _symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, y, -z+1/2'
    'x+1/2, y+1/2, z'
    '-x+1/2, y+1/2, -z+1/2'
    '-x, -y, -z'
    'x, -y, z-1/2'
    '-x+1/2, -y+1/2, -z'
    'x+1/2, -y+1/2, z-1/2'
_cell_length_a     11.200(2)
_cell_length_b     6.7280(10)
_cell_length_c     28.304(3)
_cell_angle_alpha     90.00
_cell_angle_beta     100.940(10)
_cell_angle_gamma     90.00
_cell_volume     2094.0(5)
_cell_formula_units_Z     8
_cell_measurement_reflns_used     4107
_cell_measurement_theta_min     2.93
_cell_measurement_theta_max     27.84
_cell_measurement_temperature     293(2)
_exptl_crystal_description     prism
_exptl_crystal_colour     yellow
_exptl_crystal_size_max     0.34
_exptl_crystal_size_mid     0.30
_exptl_crystal_size_min     0.14
_exptl_crystal_density_diffrn     2.027
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000     1256
_exptl_absorpt_coefficient_mu     4.406
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details     '(CrysAlis RED; Oxford Diffraction, 2009)'
_exptl_absorpt_correction_T_min     0.3158
_exptl_absorpt_correction_T_max     0.5775
_exptl_special_details
;
CrysAlis RED (Oxford Diffraction, 2009)
Empirical absorption correction using spherical harmonics, implemented in
SCALE3 ABSPACK scaling algorithm.
;
_diffrn_ambient_temperature     293(2)
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_source     'fine-focus sealed tube'
_diffrn_radiation_monochromator     graphite
_diffrn_measurement_device_type
    'Oxford Diffraction Xcalibur diffractometer with Sapphire CCD area detector'
_diffrn_measurement_method     'rotation method data acquisition using ω'
_diffrn_detector_area_resol_mean     ?
_diffrn_reflns_number     7442
_diffrn_reflns_av_R_equivalents     0.0179
_diffrn_reflns_av_sigmaI/netI     0.0158
_diffrn_reflns_theta_min     2.93
_diffrn_reflns_theta_max     26.36
_diffrn_reflns_theta_full     26.36
_diffrn_measured_fraction_theta_max     1.000
_diffrn_measured_fraction_theta_full     1.000
_diffrn_reflns_limit_h_min     -13
_diffrn_reflns_limit_h_max     13
_diffrn_reflns_limit_k_min     -8
_diffrn_reflns_limit_k_max     7
_diffrn_reflns_limit_l_min     -35
_diffrn_reflns_limit_l_max     35
_diffrn_standards_number     ?
_diffrn_standards_interval_count     ?
_diffrn_standards_interval_time     ?
_diffrn_standards_decay_%     0
_refine_special_details
;
Refinement of F² against ALL reflections. The weighted R-factor
wR and goodness of fit S are based on F², conventional
R-factors R are based on F, with F set to zero for
negative F². The threshold expression of F² >
σ(F²) is used only for calculating R-factors(gt) etc.
and is not relevant to the choice of reflections for refinement.
R-factors based on F² are statistically about twice as large
as those based on F, and R-factors based on ALL data will be
even larger.
;
_reflns_number_total     2147
_reflns_number_gt     1955
_reflns_threshold_expression     I>2σ(I)
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.0519
_refine_ls_R_factor_gt     0.0485
_refine_ls_wR_factor_gt     0.1271
_refine_ls_wR_factor_ref     0.1280
_refine_ls_goodness_of_fit_ref     1.251
_refine_ls_restrained_S_all     1.249
_refine_ls_number_reflns     2147
_refine_ls_number_parameters     141
_refine_ls_number_restraints     4
_refine_ls_hydrogen_treatment     mixed
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
      'calc w = 1/[σ²(Fo²)+(0.0182P)²+43.7119P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     0.001
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     2.265
_refine_diff_density_min     -1.186
_refine_ls_extinction_method     none
_refine_ls_extinction_coef     ?
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Br' 'Br' -0.2901 2.4595
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'N' 'N' 0.0061 0.0033
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Na' 'Na' 0.0362 0.0249
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0106 0.0060
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'S' 'S' 0.1246 0.1234
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Cl' 'Cl' 0.1484 0.1585
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection     'CrysAlis CCD (Oxford Diffraction, 2009)'
_computing_cell_refinement     'CrysAlis RED (Oxford Diffraction, 2009)'
_computing_data_reduction     'CrysAlis RED (Oxford Diffraction, 2009)'
_computing_structure_solution     'SHELXS97 (Sheldrick, 2008)'
_computing_structure_refinement     'SHELXL97 (Sheldrick, 2008)'
_computing_molecular_graphics     'PLATON (Spek, 2009)'
_computing_publication_material     'SHELXL97 (Sheldrick, 2008)'
loop_
    _atom_site_type_symbol
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_refinement_flags
    _atom_site_occupancy
    _atom_site_symmetry_multiplicity
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    C C1 0.8143(5) -0.3307(9) 0.6083(2) 0.0205(12) Uani d . 1 1 . .
    C C2 0.6903(6) -0.3509(11) 0.5927(2) 0.0311(14) Uani d . 1 1 . .
    H H2 0.6375 -0.3101 0.6125 0.037 Uiso calc R 1 1 . .
    C C3 0.6437(7) -0.4309(13) 0.5480(3) 0.0433(19) Uani d . 1 1 . .
    H H3 0.5600 -0.4409 0.5377 0.052 Uiso calc R 1 1 . .
    C C4 0.7209(8) -0.4957(12) 0.5187(3) 0.044(2) Uani d . 1 1 . .
    H H4 0.6892 -0.5508 0.4888 0.053 Uiso calc R 1 1 . .
    C C5 0.8449(8) -0.4791(11) 0.5336(3) 0.0374(17) Uani d . 1 1 . .
    H H5 0.8971 -0.5243 0.5140 0.045 Uiso calc R 1 1 . .
    C C6 0.8919(6) -0.3942(9) 0.5782(2) 0.0249(13) Uani d . 1 1 . .
    Br Br1 0.88260(6) 0.14784(10) 0.62206(2) 0.0312(2) Uani d . 1 1 . .
    N N1 0.9583(5) -0.0535(8) 0.66407(18) 0.0247(11) Uani d . 1 1 . .
    Na Na1 1.1437(2) -0.5132(4) 0.73529(9) 0.0303(6) Uani d . 1 1 . .
    O O1 0.7549(4) -0.1730(8) 0.68272(16) 0.0324(11) Uani d . 1 1 . .
    O O2 0.9370(4) -0.3782(7) 0.69654(15) 0.0286(10) Uani d . 1 1 . .
    O O3 1.2055(4) -0.1890(8) 0.70471(17) 0.0335(11) Uani d D 1 1 . .
    H H31 1.246(5) -0.241(12) 0.687(2) 0.040 Uiso d D 1 1 . .
    H H32 1.1325(19) -0.199(12) 0.695(2) 0.040 Uiso d D 1 1 . .
    O O4 1.0000 -0.7830(10) 0.7500 0.0336(16) Uani d SD 1 2 . .
    H H41 0.979(7) -0.861(9) 0.728(2) 0.040 Uiso d D 1 1 . .
    S S1 0.86584(13) -0.2281(2) 0.66713(5) 0.0198(3) Uani d . 1 1 . .
    Cl Cl1 1.04842(16) -0.3824(3) 0.59503(7) 0.0414(5) Uani d . 1 1 . .
loop_
    _atom_site_aniso_label
    _atom_site_aniso_U_11
    _atom_site_aniso_U_22
    _atom_site_aniso_U_33
    _atom_site_aniso_U_12
    _atom_site_aniso_U_13
    _atom_site_aniso_U_23
    C1 0.023(3) 0.017(3) 0.021(3) 0.001(2) 0.003(2) 0.002(2)
    C2 0.026(3) 0.033(4) 0.033(3) 0.004(3) 0.003(3) 0.000(3)
    C3 0.030(4) 0.050(5) 0.045(4) -0.004(4) -0.007(3) -0.009(4)
    C4 0.056(5) 0.043(5) 0.027(4) -0.005(4) -0.009(3) -0.010(3)
    C5 0.055(5) 0.032(4) 0.028(4) -0.001(3) 0.017(3) -0.005(3)
    C6 0.030(3) 0.020(3) 0.026(3) 0.000(3) 0.009(3) 0.002(2)
    Br1 0.0358(4) 0.0245(3) 0.0342(4) 0.0033(3) 0.0092(3) 0.0072(3)
    N1 0.022(3) 0.025(3) 0.025(3) 0.003(2) 0.001(2) 0.002(2)
    Na1 0.0299(14) 0.0312(14) 0.0320(14) 0.0047(11) 0.0114(11) -0.0007(11)
    O1 0.030(2) 0.040(3) 0.030(2) 0.001(2) 0.0131(19) -0.006(2)
    O2 0.033(2) 0.028(2) 0.023(2) 0.002(2) 0.0021(18) 0.0075(19)
    O3 0.027(2) 0.039(3) 0.034(3) 0.002(2) 0.006(2) -0.003(2)
    O4 0.044(4) 0.024(4) 0.030(4) 0.000 0.000(3) 0.000
    S1 0.0209(7) 0.0215(7) 0.0170(7) 0.0005(6) 0.0038(5) 0.0002(6)
    Cl1 0.0280(8) 0.0478(11) 0.0522(11) 0.0018(8) 0.0174(8) -0.0107(9)
_geom_special_details
;
All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell e.s.d.'s are taken
into account individually in the estimation of e.s.d.'s in distances, angles
and torsion angles; correlations between e.s.d.'s in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s.
planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    C1 C2 . 1.382(9) ?
    C1 C6 . 1.393(8) ?
    C1 S1 . 1.793(6) ?
    C2 C3 . 1.383(10) ?
    C2 H2 . 0.9300 ?
    C3 C4 . 1.378(12) ?
    C3 H3 . 0.9300 ?
    C4 C5 . 1.378(11) ?
    C4 H4 . 0.9300 ?
    C5 C6 . 1.396(9) ?
    C5 H5 . 0.9300 ?
    C6 Cl1 . 1.729(7) ?
    Br1 N1 . 1.893(5) ?
    N1 S1 . 1.579(6) ?
    Na1 O1 3_545 2.371(5) ?
    Na1 O2 2_756 2.455(5) ?
    Na1 O3 4_746 2.459(5) ?
    Na1 O3 . 2.493(6) ?
    Na1 O4 . 2.512(6) ?
    Na1 O2 . 2.534(5) ?
    Na1 S1 2_756 3.381(3) ?
    Na1 H32 . 2.40(9) ?
    O1 S1 . 1.444(5) ?
    O1 Na1 3_455 2.371(5) ?
    O2 S1 . 1.448(5) ?
    O2 Na1 2_756 2.455(5) ?
    O3 Na1 4_756 2.459(5) ?
    O3 H31 . 0.82(2) ?
    O3 H32 . 0.81(2) ?
    O4 Na1 2_756 2.512(6) ?
    O4 H41 . 0.82(2) ?
    S1 Na1 2_756 3.381(3) ?
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    C2 C1 C6 . . 118.6(6) ?
    C2 C1 S1 . . 117.5(5) ?
    C6 C1 S1 . . 123.9(5) ?
    C1 C2 C3 . . 120.9(6) ?
    C1 C2 H2 . . 119.6 ?
    C3 C2 H2 . . 119.6 ?
    C4 C3 C2 . . 120.2(7) ?
    C4 C3 H3 . . 119.9 ?
    C2 C3 H3 . . 119.9 ?
    C5 C4 C3 . . 120.1(7) ?
    C5 C4 H4 . . 120.0 ?
    C3 C4 H4 . . 120.0 ?
    C4 C5 C6 . . 119.7(7) ?
    C4 C5 H5 . . 120.2 ?
    C6 C5 H5 . . 120.2 ?
    C1 C6 C5 . . 120.5(6) ?
    C1 C6 Cl1 . . 122.4(5) ?
    C5 C6 Cl1 . . 117.1(5) ?
    S1 N1 Br1 . . 110.3(3) ?
    O1 Na1 O2 3_545 2_756 167.5(2) ?
    O1 Na1 O3 3_545 4_746 80.89(18) ?
    O2 Na1 O3 2_756 4_746 86.70(18) ?
    O1 Na1 O3 3_545 . 88.03(19) ?
    O2 Na1 O3 2_756 . 96.71(18) ?
    O3 Na1 O3 4_746 . 117.45(15) ?
    O1 Na1 O4 3_545 . 101.87(19) ?
    O2 Na1 O4 2_756 . 78.11(16) ?
    O3 Na1 O4 4_746 . 85.18(16) ?
    O3 Na1 O4 . . 156.70(19) ?
    O1 Na1 O2 3_545 . 115.86(19) ?
    O2 Na1 O2 2_756 . 76.42(19) ?
    O3 Na1 O2 4_746 . 157.31(19) ?
    O3 Na1 O2 . . 80.02(17) ?
    O4 Na1 O2 . . 76.68(15) ?
    O1 Na1 S1 3_545 2_756 150.64(16) ?
    O2 Na1 S1 2_756 2_756 22.28(11) ?
    O3 Na1 S1 4_746 2_756 80.37(14) ?
    O3 Na1 S1 . 2_756 80.85(13) ?
    O4 Na1 S1 . 2_756 98.86(11) ?
    O2 Na1 S1 . 2_756 88.99(13) ?
    O1 Na1 H32 3_545 . 94.9(14) ?
    O2 Na1 H32 2_756 . 93.2(15) ?
    O3 Na1 H32 4_746 . 136.1(7) ?
    O3 Na1 H32 . . 19.0(5) ?
    O4 Na1 H32 . . 137.7(5) ?
    O2 Na1 H32 . . 61.1(5) ?
    S1 Na1 H32 2_756 . 83.3(15) ?
    S1 O1 Na1 . 3_455 153.3(3) ?
    S1 O2 Na1 . 2_756 117.7(3) ?
    S1 O2 Na1 . . 149.0(3) ?
    Na1 O2 Na1 2_756 . 88.25(17) ?
    Na1 O3 Na1 4_756 . 112.4(2) ?
    Na1 O3 H31 4_756 . 104(5) ?
    Na1 O3 H31 . . 94(6) ?
    Na1 O3 H32 4_756 . 142(5) ?
    Na1 O3 H32 . . 74(6) ?
    H31 O3 H32 . . 112(4) ?
    Na1 O4 Na1 . 2_756 87.5(3) ?
    Na1 O4 H41 . . 116(6) ?
    Na1 O4 H41 2_756 . 119(6) ?
    O1 S1 O2 . . 114.5(3) ?
    O1 S1 N1 . . 115.9(3) ?
    O2 S1 N1 . . 104.8(3) ?
    O1 S1 C1 . . 103.8(3) ?
    O2 S1 C1 . . 108.1(3) ?
    N1 S1 C1 . . 109.5(3) ?
    O1 S1 Na1 . 2_756 74.5(2) ?
    N1 S1 Na1 . 2_756 126.1(2) ?
    C1 S1 Na1 . 2_756 119.0(2) ?
loop_
    _geom_torsion_atom_site_label_1
    _geom_torsion_atom_site_label_2
    _geom_torsion_atom_site_label_3
    _geom_torsion_atom_site_label_4
    _geom_torsion_site_symmetry_1
    _geom_torsion_site_symmetry_2
    _geom_torsion_site_symmetry_3
    _geom_torsion_site_symmetry_4
    _geom_torsion
    _geom_torsion_publ_flag
    C6 C1 C2 C3 . . . . -0.5(10) ?
    S1 C1 C2 C3 . . . . -179.3(6) ?
    C1 C2 C3 C4 . . . . 1.4(12) ?
    C2 C3 C4 C5 . . . . -0.7(13) ?
    C3 C4 C5 C6 . . . . -0.8(12) ?
    C2 C1 C6 C5 . . . . -1.0(10) ?
    S1 C1 C6 C5 . . . . 177.7(5) ?
    C2 C1 C6 Cl1 . . . . -178.1(5) ?
    S1 C1 C6 Cl1 . . . . 0.6(8) ?
    C4 C5 C6 C1 . . . . 1.6(11) ?
    C4 C5 C6 Cl1 . . . . 178.9(6) ?
    O1 Na1 O2 S1 3_545 . . . -74.9(6) ?
    O2 Na1 O2 S1 2_756 . . . 107.4(5) ?
    O3 Na1 O2 S1 4_746 . . . 150.4(5) ?
    O3 Na1 O2 S1 . . . . 8.0(6) ?
    O4 Na1 O2 S1 . . . . -171.8(6) ?
    S1 Na1 O2 S1 2_756 . . . 88.9(6) ?
    O1 Na1 O2 Na1 3_545 . . 2_756 136.66(17) ?
    O2 Na1 O2 Na1 2_756 . . 2_756 -41.0(2) ?
    O3 Na1 O2 Na1 4_746 . . 2_756 2.0(6) ?
    O3 Na1 O2 Na1 . . . 2_756 -140.47(18) ?
    O4 Na1 O2 Na1 . . . 2_756 39.77(14) ?
    S1 Na1 O2 Na1 2_756 . . 2_756 -59.58(15) ?
    O1 Na1 O3 Na1 3_545 . . 4_756 -108.3(2) ?
    O2 Na1 O3 Na1 2_756 . . 4_756 60.1(2) ?
    O3 Na1 O3 Na1 4_746 . . 4_756 -29.7(2) ?
    O4 Na1 O3 Na1 . . . 4_756 135.6(4) ?
    O2 Na1 O3 Na1 . . . 4_756 135.0(2) ?
    S1 Na1 O3 Na1 2_756 . . 4_756 44.40(17) ?
    O1 Na1 O4 Na1 3_545 . . 2_756 -152.81(18) ?
    O2 Na1 O4 Na1 2_756 . . 2_756 39.93(12) ?
    O3 Na1 O4 Na1 4_746 . . 2_756 127.57(16) ?
    O3 Na1 O4 Na1 . . . 2_756 -39.3(4) ?
    O2 Na1 O4 Na1 . . . 2_756 -38.72(11) ?
    S1 Na1 O4 Na1 2_756 . . 2_756 48.11(6) ?
    Na1 O1 S1 O2 3_455 . . . 73.2(8) ?
    Na1 O1 S1 N1 3_455 . . . -49.0(8) ?
    Na1 O1 S1 C1 3_455 . . . -169.1(7) ?
    Na1 O1 S1 Na1 3_455 . . 2_756 74.1(7) ?
    Na1 O2 S1 O1 2_756 . . . 1.2(4) ?
    Na1 O2 S1 O1 . . . . -142.6(5) ?
    Na1 O2 S1 N1 2_756 . . . 129.4(3) ?
    Na1 O2 S1 N1 . . . . -14.4(6) ?
    Na1 O2 S1 C1 2_756 . . . -113.9(3) ?
    Na1 O2 S1 C1 . . . . 102.3(6) ?
    Na1 O2 S1 Na1 . . . 2_756 -143.8(7) ?
    Br1 N1 S1 O1 . . . . -57.6(4) ?
    Br1 N1 S1 O2 . . . . 175.1(3) ?
    Br1 N1 S1 C1 . . . . 59.4(4) ?
    Br1 N1 S1 Na1 . . . 2_756 -146.92(16) ?
    C2 C1 S1 O1 . . . . -5.0(6) ?
    C6 C1 S1 O1 . . . . 176.3(5) ?
    C2 C1 S1 O2 . . . . 117.0(5) ?
    C6 C1 S1 O2 . . . . -61.7(6) ?
    C2 C1 S1 N1 . . . . -129.4(5) ?
    C6 C1 S1 N1 . . . . 51.9(6) ?
    C2 C1 S1 Na1 . . . 2_756 74.7(5) ?
    C6 C1 S1 Na1 . . . 2_756 -103.9(5) ?
loop_
    _geom_hbond_atom_site_label_D
    _geom_hbond_atom_site_label_H
    _geom_hbond_atom_site_label_A
    _geom_hbond_site_symmetry_A
    _geom_hbond_distance_DH
    _geom_hbond_distance_HA
    _geom_hbond_distance_DA
    _geom_hbond_angle_DHA
    O3 H31 Br1 3_545 0.82(2) 2.70(2) 3.518(5) 171(8)
    O3 H32 N1 . 0.81(2) 2.21(5) 2.934(7) 149(8)
    O3 H32 O2 . 0.81(2) 2.51(5) 3.232(7) 148(8)
    O4 H41 N1 1_545 0.82(2) 2.20(3) 3.002(7) 168(8)
data_global
_journal_date_recd_electronic     2011-05-19
_journal_date_accepted     2011-05-30
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2011
_journal_volume     67
_journal_issue      7
_journal_page_first     m870
_journal_page_last     m870
_journal_paper_category     QM
_journal_coeditor_code     RZ2602
_publ_contact_author_name     'Professor B. Thimme Gowda'
_publ_contact_author_address
;
Department of Chemistry
Mangalore University
Mangalagangotri 574 199
Mangalore
India
;
_publ_contact_author_email     gowdabt@yahoo.com
_publ_contact_author_fax     '91 824 2287367'
_publ_contact_author_phone     '91 824 2287262'
_publ_section_title
;
Sodium N-bromo-2-chlorobenzenesulfonamidate sesquihydrate
;
loop_
    _publ_author_name
    _publ_author_address
    'B. Thimme Gowda'
;
Department of Chemistry
Mangalore University
Mangalagangotri 574 199
Mangalore
India
;
    'Sabine Foro'
;
Institute of Materials Science
Darmstadt University of Technology
Petersenstrasse 23
D-64287 Darmstadt
Germany
;
    'K. Shakuntala'
;
Department of Chemistry
Mangalore University
Mangalagangotri 574 199
Mangalore
India
;
