##############################################################################
###                                                                        ###
###        Electronic paper (Acta Crystallographica Section E)             ###
###                                                                        ###
##############################################################################
#                                                                            #
# This CIF contains the data in a paper accepted for publication in Acta     #
# Crystallographica Section E. It conforms to the requirements of Notes      #
# for Authors for Section E, and has been peer reviewed under the auspices   #
# of the IUCr Commission on Journals.                                        #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic. The current version number is 2.4.    #
#                                                                            #
# Software is freely available for graphical display of the structure(s) in  #
# this CIF.  For information consult the CIF home page http://www.iucr.org/  #
# cif/home.html                                                              #
#                                                                            #
# This file may be used for bona fide research purposes within the           #
# scientific community so long as proper attribution is given to the journal # 
# article from which it was obtained.                                        #
#                                                                            #
##############################################################################
                                             
data_global
_audit_creation_method     SHELXL-97
_journal_date_recd_electronic     2008-04-09
_journal_date_accepted     2008-04-18
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2008
_journal_volume     64
_journal_issue      5
_journal_page_first     m703
_journal_page_last     m703
_journal_paper_category     QM
_journal_coeditor_code     CV2399
_publ_contact_author
;
     Dr. Seik Weng Ng
     Department of Chemistry
     University of Malaya
     50603 Kuala Lumpur
     Malaysia
;
_publ_contact_author_email     seikweng@um.edu.my
_publ_contact_author_fax     '03 7967 4193'
_publ_contact_author_phone     '03 7967 6778'
_publ_section_title
;
Bis[1,3-bis(diphenylphosphino)propane-κ²P:P']silver(I)
bis(chlorodifluoroacetato-κO)triphenylstannate(IV)
;
loop_
    _publ_author_name
    _publ_author_address
    'Teo, Yin Yin'
;
     Department of Chemistry
     University of Malaya
     50603 Kuala Lumpur
     Malaysia
;
    'Lo, Kong Mun'
;
     Department of Chemistry
     University of Malaya
     50603 Kuala Lumpur
     Malaysia
;
    'Ng, Seik Weng'
;
     Department of Chemistry
     University of Malaya
     50603 Kuala Lumpur
     Malaysia
;
data_I
_audit_creation_method     SHELXL-97
_chemical_name_systematic
;
Bis[1,3-bis(diphenylphosphino)propane-κ²P:P']silver(I)
bis(chlorodifluoroacetato-\kO)triphenylstannate(IV)
;
_chemical_name_common     ?
_chemical_formula_moiety     'C54 H52 Ag1 P4 +, C22 H15 Cl2 F4 O4 Sn -'
_chemical_formula_sum     'C76 H67 Ag Cl2 F4 O4 P4 Sn'
_chemical_formula_iupac     '[Ag (C27 H26 P2)2] [Sn (C6 H5)3 (C2 Cl F2 O2)]'
_chemical_formula_weight     1541.64
_chemical_melting_point     ?
_symmetry_cell_setting     triclinic
_symmetry_space_group_name_H-M     'P -1'
_symmetry_space_group_name_Hall     '-P 1'
loop_
    _symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, -y, -z'
_cell_length_a     10.5554(2)
_cell_length_b     17.6600(4)
_cell_length_c     19.1383(4)
_cell_angle_alpha     91.5810(10)
_cell_angle_beta     94.9310(10)
_cell_angle_gamma     104.5350(10)
_cell_volume     3436.10(10)
_cell_formula_units_Z     2
_cell_measurement_reflns_used     4777
_cell_measurement_theta_min     2.2
_cell_measurement_theta_max     24.
_cell_measurement_temperature     100(2)
_exptl_crystal_description     Block
_exptl_crystal_colour     Colourless
_exptl_crystal_size_max     0.18
_exptl_crystal_size_mid     0.12
_exptl_crystal_size_min     0.05
_exptl_crystal_density_diffrn     1.490
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000     1564
_exptl_absorpt_coefficient_mu     0.880
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details     '(SADABS; Sheldrick, 1996)'
_exptl_absorpt_correction_T_min     0.8577
_exptl_absorpt_correction_T_max     0.9573
_diffrn_ambient_temperature     100(2)
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_source     'fine-focus sealed tube'
_diffrn_radiation_monochromator     graphite
_diffrn_measurement_device_type     'Bruker SMART APEX'
_diffrn_measurement_method     ω
_diffrn_detector_area_resol_mean     ?
_diffrn_reflns_number     35712
_diffrn_reflns_av_R_equivalents     0.0648
_diffrn_reflns_av_sigmaI/netI     0.1025
_diffrn_reflns_theta_min     1.07
_diffrn_reflns_theta_max     27.50
_diffrn_reflns_theta_full     27.50
_diffrn_measured_fraction_theta_max     0.975
_diffrn_measured_fraction_theta_full     0.975
_diffrn_reflns_limit_h_min     -13
_diffrn_reflns_limit_h_max     13
_diffrn_reflns_limit_k_min     -22
_diffrn_reflns_limit_k_max     18
_diffrn_reflns_limit_l_min     -24
_diffrn_reflns_limit_l_max     24
_diffrn_standards_number     0
_diffrn_standards_interval_count     0
_diffrn_standards_interval_time     0
_diffrn_standards_decay_%     0
_reflns_number_total     15398
_reflns_number_gt     10993
_reflns_threshold_expression     I>2σ(I)
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.0764
_refine_ls_R_factor_gt     0.0489
_refine_ls_wR_factor_gt     0.0972
_refine_ls_wR_factor_ref     0.1123
_refine_ls_goodness_of_fit_ref     1.048
_refine_ls_restrained_S_all     1.052
_refine_ls_number_reflns     15398
_refine_ls_number_parameters     829
_refine_ls_number_restraints     48
_refine_ls_hydrogen_treatment     constr
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
                      'calc w=1/[σ²(Fo²)+1.3097P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     0.001
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     0.861
_refine_diff_density_min     -0.762
_refine_ls_extinction_method     none
_refine_ls_extinction_coef     ?
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0106 0.0060
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'F' 'F' 0.0171 0.0103
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'P' 'P' 0.1023 0.0942
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Cl' 'Cl' 0.1484 0.1585
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Ag' 'Ag' -0.8971 1.1015
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Sn' 'Sn' -0.6537 1.4246
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection     'APEX2 (Bruker, 2007)'
_computing_cell_refinement     'SAINT (Bruker, 2007)'
_computing_data_reduction     'SAINT (Bruker, 2007)'
_computing_structure_solution     'SHELXS97 (Sheldrick, 2008)'
_computing_structure_refinement     'SHELXL97 (Sheldrick, 2008)'
_computing_molecular_graphics     'X-SEED (Barbour, 2001)'
_computing_publication_material     'publCIF (Westrip, 2008)'
loop_
    _atom_site_type_symbol
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_refinement_flags
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    Sn Sn1 0.02753(3) 0.730942(18) 0.273935(14) 0.01420(8) Uani d . 1 . .
    Ag Ag1 0.41787(3) 0.227571(19) 0.254989(15) 0.01370(8) Uani d . 1 . .
    Cl Cl1 -0.23532(11) 0.56238(7) 0.09181(6) 0.0289(3) Uani d . 1 . .
    Cl Cl2 0.08334(11) 0.88104(8) 0.50499(6) 0.0294(3) Uani d . 1 . .
    P P1 0.21513(10) 0.14129(7) 0.19532(5) 0.0140(2) Uani d . 1 . .
    P P2 0.30050(10) 0.27516(7) 0.34838(5) 0.0164(2) Uani d . 1 . .
    P P3 0.56274(10) 0.32427(7) 0.18763(6) 0.0154(2) Uani d . 1 . .
    P P4 0.59289(10) 0.17736(7) 0.31680(6) 0.0153(2) Uani d . 1 . .
    F F1 -0.0366(3) 0.56467(16) 0.02666(12) 0.0289(6) Uani d . 1 . .
    F F2 -0.0553(3) 0.49132(16) 0.11555(13) 0.0301(6) Uani d . 1 . .
    F F3 -0.1207(3) 0.92144(19) 0.46015(14) 0.0399(8) Uani d . 1 . .
    F F4 0.0540(3) 0.97475(16) 0.41018(14) 0.0335(7) Uani d . 1 . .
    O O1 -0.0013(3) 0.62288(17) 0.20477(14) 0.0173(6) Uani d . 1 . .
    O O2 0.0963(3) 0.68053(19) 0.11296(15) 0.0253(7) Uani d . 1 . .
    O O3 0.0474(3) 0.83204(18) 0.34826(14) 0.0202(7) Uani d . 1 . .
    O O4 -0.1681(3) 0.8079(2) 0.36239(16) 0.0278(8) Uani d . 1 . .
    C C1 -0.0392(4) 0.6519(3) 0.3528(2) 0.0168(9) Uani d . 1 . .
    C C2 -0.1432(4) 0.5862(3) 0.3396(2) 0.0245(10) Uani d . 1 . .
    H H2 -0.1891 0.5759 0.2940 0.029 Uiso calc R 1 . .
    C C3 -0.1815(4) 0.5347(3) 0.3923(2) 0.0291(11) Uani d . 1 . .
    H H3 -0.2541 0.4902 0.3829 0.035 Uiso calc R 1 . .
    C C4 -0.1132(5) 0.5486(3) 0.4585(2) 0.0265(11) Uani d . 1 . .
    H H4 -0.1382 0.5136 0.4947 0.032 Uiso calc R 1 . .
    C C5 -0.0085(5) 0.6138(3) 0.4714(2) 0.0277(11) Uani d . 1 . .
    H H5 0.0394 0.6232 0.5164 0.033 Uiso calc R 1 . .
    C C6 0.0270(4) 0.6650(3) 0.4197(2) 0.0237(10) Uani d . 1 . .
    H H6 0.0982 0.7101 0.4297 0.028 Uiso calc R 1 . .
    C C7 0.2352(4) 0.7673(3) 0.2721(2) 0.0147(9) Uani d . 1 . .
    C C8 0.3074(4) 0.7132(3) 0.2625(2) 0.0228(10) Uani d . 1 . .
    H H8 0.2638 0.6592 0.2548 0.027 Uiso calc R 1 . .
    C C9 0.4436(4) 0.7373(3) 0.2641(2) 0.0243(10) Uani d . 1 . .
    H H9 0.4927 0.6994 0.2599 0.029 Uiso calc R 1 . .
    C C10 0.5081(4) 0.8157(3) 0.2717(2) 0.0223(10) Uani d . 1 . .
    H H10 0.6009 0.8319 0.2714 0.027 Uiso calc R 1 . .
    C C11 0.4365(4) 0.8706(3) 0.2799(2) 0.0211(10) Uani d . 1 . .
    H H11 0.4795 0.9249 0.2843 0.025 Uiso calc R 1 . .
    C C12 0.3011(4) 0.8455(3) 0.2815(2) 0.0185(9) Uani d . 1 . .
    H H12 0.2526 0.8831 0.2893 0.022 Uiso calc R 1 . .
    C C13 -0.0893(4) 0.7739(3) 0.1972(2) 0.0152(9) Uani d . 1 . .
    C C14 -0.2241(4) 0.7448(3) 0.1842(2) 0.0241(10) Uani d . 1 . .
    H H14 -0.2683 0.7057 0.2130 0.029 Uiso calc R 1 . .
    C C15 -0.2964(4) 0.7710(3) 0.1308(2) 0.0263(11) Uani d . 1 . .
    H H15 -0.3890 0.7504 0.1236 0.032 Uiso calc R 1 . .
    C C16 -0.2335(4) 0.8270(3) 0.0883(2) 0.0286(12) Uani d . 1 . .
    H H16 -0.2824 0.8442 0.0507 0.034 Uiso calc R 1 . .
    C C17 -0.0999(5) 0.8582(3) 0.1001(2) 0.0344(13) Uani d . 1 . .
    H H17 -0.0568 0.8977 0.0712 0.041 Uiso calc R 1 . .
    C C18 -0.0276(4) 0.8320(3) 0.1543(2) 0.0277(11) Uani d . 1 . .
    H H18 0.0646 0.8538 0.1622 0.033 Uiso calc R 1 . .
    C C19 0.0206(4) 0.6297(3) 0.1401(2) 0.0171(9) Uani d . 1 . .
    C C20 -0.0680(4) 0.5614(3) 0.0928(2) 0.0212(10) Uani d . 1 . .
    C C21 -0.0532(4) 0.8413(3) 0.3756(2) 0.0185(9) Uani d . 1 . .
    C C22 -0.0145(4) 0.9070(3) 0.4342(2) 0.0228(10) Uani d . 1 . .
    C C23 0.1159(4) 0.1904(3) 0.1391(2) 0.0155(9) Uani d . 1 . .
    C C24 0.1817(4) 0.2448(3) 0.0947(2) 0.0197(10) Uani d . 1 . .
    H H24 0.2749 0.2567 0.0967 0.024 Uiso calc R 1 . .
    C C25 0.1131(4) 0.2815(3) 0.0481(2) 0.0256(11) Uani d . 1 . .
    H H25 0.1588 0.3180 0.0175 0.031 Uiso calc R 1 . .
    C C26 -0.0226(4) 0.2651(3) 0.0458(2) 0.0264(11) Uani d . 1 . .
    H H26 -0.0700 0.2904 0.0136 0.032 Uiso calc R 1 . .
    C C27 -0.0893(4) 0.2119(3) 0.0902(2) 0.0229(10) Uani d . 1 . .
    H H27 -0.1823 0.2017 0.0892 0.028 Uiso calc R 1 . .
    C C28 -0.0209(4) 0.1735(3) 0.1364(2) 0.0192(9) Uani d . 1 . .
    H H28 -0.0670 0.1360 0.1660 0.023 Uiso calc R 1 . .
    C C29 0.2263(4) 0.0595(3) 0.1382(2) 0.0158(9) Uani d . 1 . .
    C C30 0.1691(4) 0.0471(3) 0.0691(2) 0.0195(10) Uani d . 1 . .
    H H30 0.1166 0.0800 0.0512 0.023 Uiso calc R 1 . .
    C C31 0.1881(4) -0.0129(3) 0.0260(2) 0.0251(11) Uani d . 1 . .
    H H31 0.1506 -0.0197 -0.0214 0.030 Uiso calc R 1 . .
    C C32 0.2605(4) -0.0625(3) 0.0513(2) 0.0246(10) Uani d . 1 . .
    H H32 0.2705 -0.1045 0.0220 0.030 Uiso calc R 1 . .
    C C33 0.3193(4) -0.0510(3) 0.1201(2) 0.0249(11) Uani d . 1 . .
    H H33 0.3708 -0.0846 0.1376 0.030 Uiso calc R 1 . .
    C C34 0.3023(4) 0.0096(3) 0.1626(2) 0.0223(10) Uani d . 1 . .
    H H34 0.3431 0.0174 0.2094 0.027 Uiso calc R 1 . .
    C C35 0.1064(4) 0.0964(3) 0.2607(2) 0.0182(9) Uani d . 1 . .
    H H35 0.0774 0.0413 0.2641 0.022 Uiso calc R 1 . .
    C C36 0.0654(4) 0.1549(3) 0.3099(2) 0.0204(10) Uani d . 1 . .
    H H36A 0.0431 0.1963 0.2810 0.025 Uiso calc R 1 . .
    H H36B -0.0159 0.1269 0.3298 0.025 Uiso calc R 1 . .
    C C37 0.1649(4) 0.1948(3) 0.3706(2) 0.0193(10) Uani d . 1 . .
    H H37A 0.2029 0.1546 0.3931 0.023 Uiso calc R 1 . .
    H H37B 0.1172 0.2154 0.4060 0.023 Uiso calc R 1 . .
    C C38 0.2178(4) 0.3504(3) 0.3206(2) 0.0174(9) Uani d . 1 . .
    C C39 0.2053(4) 0.3658(3) 0.2501(2) 0.0208(10) Uani d . 1 . .
    H H39 0.2414 0.3380 0.2171 0.025 Uiso calc R 1 . .
    C C40 0.1405(4) 0.4214(3) 0.2269(2) 0.0220(10) Uani d . 1 . .
    H H40 0.1303 0.4303 0.1782 0.026 Uiso calc R 1 . .
    C C41 0.0911(4) 0.4635(3) 0.2747(2) 0.0260(11) Uani d . 1 . .
    H H41 0.0482 0.5022 0.2593 0.031 Uiso calc R 1 . .
    C C42 0.1047(5) 0.4489(3) 0.3456(2) 0.0372(14) Uani d . 1 . .
    H H42 0.0715 0.4781 0.3788 0.045 Uiso calc R 1 . .
    C C43 0.1659(5) 0.3927(3) 0.3679(2) 0.0324(13) Uani d . 1 . .
    H H43 0.1728 0.3825 0.4164 0.039 Uiso calc R 1 . .
    C C44 0.3843(4) 0.3140(3) 0.4337(2) 0.0210(10) Uani d DU 1 . .
    C C45 0.4909(5) 0.3775(3) 0.4357(2) 0.0566(18) Uani d DU 1 . .
    H H45A 0.4607 0.4195 0.4114 0.068 Uiso calc R 1 . .
    H H45B 0.5550 0.3625 0.4069 0.068 Uiso calc R 1 . .
    C C46 0.5602(5) 0.4111(3) 0.4991(3) 0.085(3) Uani d DU 1 . .
    H H46 0.6336 0.4552 0.4994 0.102 Uiso calc R 1 . .
    C C47 0.5213(5) 0.3798(3) 0.5610(2) 0.0516(16) Uani d DU 1 . .
    H H47 0.5683 0.4022 0.6044 0.062 Uiso calc R 1 . .
    C C48 0.4156(4) 0.3168(3) 0.5608(2) 0.0359(13) Uani d DU 1 . .
    H H48 0.3890 0.2955 0.6038 0.043 Uiso calc R 1 . .
    C C49 0.3468(4) 0.2837(3) 0.4974(2) 0.0298(11) Uani d DU 1 . .
    H H49 0.2733 0.2398 0.4976 0.036 Uiso calc R 1 . .
    C C50 0.6527(4) 0.0962(3) 0.2826(2) 0.0179(9) Uani d . 1 . .
    C C51 0.6416(4) 0.0806(3) 0.2098(2) 0.0214(10) Uani d . 1 . .
    H H51 0.5998 0.1103 0.1792 0.026 Uiso calc R 1 . .
    C C52 0.6915(4) 0.0218(3) 0.1824(3) 0.0275(11) Uani d . 1 . .
    H H52 0.6850 0.0119 0.1331 0.033 Uiso calc R 1 . .
    C C53 0.7504(4) -0.0222(3) 0.2263(3) 0.0293(12) Uani d . 1 . .
    H H53 0.7842 -0.0624 0.2071 0.035 Uiso calc R 1 . .
    C C54 0.7605(4) -0.0080(3) 0.2983(3) 0.0295(12) Uani d . 1 . .
    H H54 0.8009 -0.0388 0.3285 0.035 Uiso calc R 1 . .
    C C55 0.7116(4) 0.0513(3) 0.3266(2) 0.0220(10) Uani d . 1 . .
    H H55 0.7188 0.0609 0.3761 0.026 Uiso calc R 1 . .
    C C56 0.5544(4) 0.1494(3) 0.4043(2) 0.0180(9) Uani d . 1 . .
    C C57 0.4425(4) 0.0884(3) 0.4092(2) 0.0232(10) Uani d . 1 . .
    H H57 0.3946 0.0617 0.3676 0.028 Uiso calc R 1 . .
    C C58 0.4006(4) 0.0663(3) 0.4738(2) 0.0278(11) Uani d . 1 . .
    H H58 0.3255 0.0239 0.4763 0.033 Uiso calc R 1 . .
    C C59 0.4674(5) 0.1057(3) 0.5348(2) 0.0315(12) Uani d . 1 . .
    H H59 0.4372 0.0911 0.5791 0.038 Uiso calc R 1 . .
    C C60 0.5778(5) 0.1660(3) 0.5311(2) 0.0327(12) Uani d . 1 . .
    H H60 0.6246 0.1928 0.5730 0.039 Uiso calc R 1 . .
    C C61 0.6211(4) 0.1882(3) 0.4658(2) 0.0245(10) Uani d . 1 . .
    H H61 0.6970 0.2301 0.4637 0.029 Uiso calc R 1 . .
    C C62 0.7435(4) 0.2573(3) 0.3283(2) 0.0179(9) Uani d . 1 . .
    H H62A 0.7277 0.3002 0.3579 0.022 Uiso calc R 1 . .
    H H62B 0.8141 0.2381 0.3536 0.022 Uiso calc R 1 . .
    C C63 0.7910(4) 0.2905(3) 0.2587(2) 0.0165(9) Uani d . 1 . .
    H H63A 0.8878 0.3107 0.2652 0.020 Uiso calc R 1 . .
    H H63B 0.7703 0.2470 0.2224 0.020 Uiso calc R 1 . .
    C C64 0.7316(4) 0.3561(3) 0.2311(2) 0.0183(9) Uani d . 1 . .
    H H64A 0.7893 0.3852 0.1974 0.022 Uiso calc R 1 . .
    H H64B 0.7321 0.3931 0.2710 0.022 Uiso calc R 1 . .
    C C65 0.5173(4) 0.4162(3) 0.1735(2) 0.0160(9) Uani d . 1 . .
    C C66 0.4562(4) 0.4311(3) 0.1095(2) 0.0223(10) Uani d . 1 . .
    H H66 0.4427 0.3941 0.0709 0.027 Uiso calc R 1 . .
    C C67 0.4145(4) 0.5001(3) 0.1019(2) 0.0245(11) Uani d . 1 . .
    H H67 0.3748 0.5105 0.0580 0.029 Uiso calc R 1 . .
    C C68 0.4318(5) 0.5522(3) 0.1582(3) 0.0305(12) Uani d . 1 . .
    H H68 0.4023 0.5985 0.1533 0.037 Uiso calc R 1 . .
    C C69 0.4916(5) 0.5385(3) 0.2223(2) 0.0310(12) Uani d . 1 . .
    H H69 0.5044 0.5755 0.2609 0.037 Uiso calc R 1 . .
    C C70 0.5325(4) 0.4702(3) 0.2293(2) 0.0227(10) Uani d . 1 . .
    H H70 0.5720 0.4603 0.2734 0.027 Uiso calc R 1 . .
    C C71 0.5872(4) 0.2907(3) 0.0999(2) 0.0154(9) Uani d . 1 . .
    C C72 0.6675(4) 0.3406(3) 0.0568(2) 0.0187(9) Uani d . 1 . .
    H H72 0.7113 0.3925 0.0735 0.022 Uiso calc R 1 . .
    C C73 0.6833(4) 0.3150(3) -0.0097(2) 0.0214(10) Uani d . 1 . .
    H H73 0.7363 0.3496 -0.0390 0.026 Uiso calc R 1 . .
    C C74 0.6222(4) 0.2389(3) -0.0339(2) 0.0245(11) Uani d . 1 . .
    H H74 0.6349 0.2212 -0.0794 0.029 Uiso calc R 1 . .
    C C75 0.5432(4) 0.1889(3) 0.0076(2) 0.0225(10) Uani d . 1 . .
    H H75 0.5011 0.1367 -0.0092 0.027 Uiso calc R 1 . .
    C C76 0.5250(4) 0.2150(3) 0.0746(2) 0.0180(9) Uani d . 1 . .
    H H76 0.4696 0.1807 0.1031 0.022 Uiso calc R 1 . .
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    Sn1 C1 . 2.128(4) ?
    Sn1 C7 . 2.128(4) ?
    Sn1 C13 . 2.115(4) ?
    Sn1 O1 . 2.233(3) ?
    Sn1 O3 . 2.208(3) ?
    Ag1 P1 . 2.4600(10)
                      ?
    Ag1 P2 . 2.5010(10)
                      ?
    Ag1 P3 . 2.4630(10)
                      ?
    Ag1 P4 . 2.4700(10)
                      ?
    Cl1 C20 . 1.769(4) ?
    Cl2 C22 . 1.773(4) ?
    P1 C29 . 1.821(4) ?
    P1 C23 . 1.822(4) ?
    P1 C35 . 1.833(4) ?
    P2 C44 . 1.818(4) ?
    P2 C38 . 1.831(4) ?
    P2 C37 . 1.834(5) ?
    P3 C65 . 1.825(4) ?
    P3 C71 . 1.827(4) ?
    P3 C64 . 1.845(4) ?
    P4 C56 . 1.810(4) ?
    P4 C50 . 1.831(4) ?
    P4 C62 . 1.835(4) ?
    F1 C20 . 1.334(5) ?
    F2 C20 . 1.358(5) ?
    F3 C22 . 1.342(4) ?
    F4 C22 . 1.348(5) ?
    O1 C19 . 1.282(4) ?
    O2 C19 . 1.204(5) ?
    O3 C21 . 1.268(4) ?
    O4 C21 . 1.209(5) ?
    C1 C2 . 1.382(6) ?
    C1 C6 . 1.390(6) ?
    C2 C3 . 1.395(6) ?
    C2 H2 . 0.9500 ?
    C3 C4 . 1.386(6) ?
    C3 H3 . 0.9500 ?
    C4 C5 . 1.381(7) ?
    C4 H4 . 0.9500 ?
    C5 C6 . 1.371(6) ?
    C5 H5 . 0.9500 ?
    C6 H6 . 0.9500 ?
    C7 C12 . 1.380(6) ?
    C7 C8 . 1.382(5) ?
    C8 C9 . 1.391(6) ?
    C8 H8 . 0.9500 ?
    C9 C10 . 1.378(6) ?
    C9 H9 . 0.9500 ?
    C10 C11 . 1.384(6) ?
    C10 H10 . 0.9500 ?
    C11 C12 . 1.390(5) ?
    C11 H11 . 0.9500 ?
    C12 H12 . 0.9500 ?
    C13 C14 . 1.384(6) ?
    C13 C18 . 1.398(6) ?
    C14 C15 . 1.382(6) ?
    C14 H14 . 0.9500 ?
    C15 C16 . 1.375(7) ?
    C15 H15 . 0.9500 ?
    C16 C17 . 1.376(6) ?
    C16 H16 . 0.9500 ?
    C17 C18 . 1.393(6) ?
    C17 H17 . 0.9500 ?
    C18 H18 . 0.9500 ?
    C19 C20 . 1.543(6) ?
    C21 C22 . 1.544(6) ?
    C23 C24 . 1.392(6) ?
    C23 C28 . 1.394(5) ?
    C24 C25 . 1.378(5) ?
    C24 H24 . 0.9500 ?
    C25 C26 . 1.385(6) ?
    C25 H25 . 0.9500 ?
    C26 C27 . 1.385(6) ?
    C26 H26 . 0.9500 ?
    C27 C28 . 1.390(5) ?
    C27 H27 . 0.9500 ?
    C28 H28 . 0.9500 ?
    C29 C30 . 1.394(6) ?
    C29 C34 . 1.396(5) ?
    C30 C31 . 1.389(6) ?
    C30 H30 . 0.9500 ?
    C31 C32 . 1.371(6) ?
    C31 H31 . 0.9500 ?
    C32 C33 . 1.393(6) ?
    C32 H32 . 0.9500 ?
    C33 C34 . 1.384(6) ?
    C33 H33 . 0.9500 ?
    C34 H34 . 0.9500 ?
    C35 C36 . 1.543(6) ?
    C35 H35 . 0.9500 ?
    C36 C37 . 1.524(6) ?
    C36 H36A . 0.9900 ?
    C36 H36B . 0.9900 ?
    C37 H37A . 0.9900 ?
    C37 H37B . 0.9900 ?
    C38 C39 . 1.385(5) ?
    C38 C43 . 1.390(6) ?
    C39 C40 . 1.392(6) ?
    C39 H39 . 0.9500 ?
    C40 C41 . 1.379(6) ?
    C40 H40 . 0.9500 ?
    C41 C42 . 1.390(6) ?
    C41 H41 . 0.9500 ?
    C42 C43 . 1.373(6) ?
    C42 H42 . 0.9500 ?
    C43 H43 . 0.9500 ?
    C44 C45 . 1.373(6) ?
    C44 C49 . 1.394(6) ?
    C45 C46 . 1.396(6) ?
    C45 H45A . 0.9900 ?
    C45 H45B . 0.9900 ?
    C46 C47 . 1.373(6) ?
    C46 H46 . 0.9500 ?
    C47 C48 . 1.363(6) ?
    C47 H47 . 0.9500 ?
    C48 C49 . 1.391(5) ?
    C48 H48 . 0.9500 ?
    C49 H49 . 0.9500 ?
    C50 C55 . 1.386(5) ?
    C50 C51 . 1.403(6) ?
    C51 C52 . 1.386(6) ?
    C51 H51 . 0.9500 ?
    C52 C53 . 1.371(6) ?
    C52 H52 . 0.9500 ?
    C53 C54 . 1.385(7) ?
    C53 H53 . 0.9500 ?
    C54 C55 . 1.396(6) ?
    C54 H54 . 0.9500 ?
    C55 H55 . 0.9500 ?
    C56 C61 . 1.386(6) ?
    C56 C57 . 1.396(6) ?
    C57 C58 . 1.381(6) ?
    C57 H57 . 0.9500 ?
    C58 C59 . 1.382(7) ?
    C58 H58 . 0.9500 ?
    C59 C60 . 1.376(7) ?
    C59 H59 . 0.9500 ?
    C60 C61 . 1.399(6) ?
    C60 H60 . 0.9500 ?
    C61 H61 . 0.9500 ?
    C62 C63 . 1.542(5) ?
    C62 H62A . 0.9900 ?
    C62 H62B . 0.9900 ?
    C63 C64 . 1.535(5) ?
    C63 H63A . 0.9900 ?
    C63 H63B . 0.9900 ?
    C64 H64A . 0.9900 ?
    C64 H64B . 0.9900 ?
    C65 C70 . 1.383(6) ?
    C65 C66 . 1.396(6) ?
    C66 C67 . 1.402(6) ?
    C66 H66 . 0.9500 ?
    C67 C68 . 1.368(6) ?
    C67 H67 . 0.9500 ?
    C68 C69 . 1.386(6) ?
    C68 H68 . 0.9500 ?
    C69 C70 . 1.385(6) ?
    C69 H69 . 0.9500 ?
    C70 H70 . 0.9500 ?
    C71 C76 . 1.385(6) ?
    C71 C72 . 1.400(6) ?
    C72 C73 . 1.375(6) ?
    C72 H72 . 0.9500 ?
    C73 C74 . 1.384(7) ?
    C73 H73 . 0.9500 ?
    C74 C75 . 1.375(7) ?
    C74 H74 . 0.9500 ?
    C75 C76 . 1.396(5) ?
    C75 H75 . 0.9500 ?
    C76 H76 . 0.9500 ?
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    C1 Sn1 C7 . . 115.2(2) ?
    C1 Sn1 C13 . . 127.2(2) ?
    C1 Sn1 O1 . . 84.90(10)
                          ?
    C1 Sn1 O3 . . 90.80(10)
                          ?
    C7 Sn1 C13 . . 117.6(2) ?
    C7 Sn1 O1 . . 95.80(10)
                          ?
    C7 Sn1 O3 . . 86.90(10)
                          ?
    C13 Sn1 O3 . . 93.20(10)
                           ?
    C13 Sn1 O1 . . 88.70(10)
                           ?
    O1 Sn1 O3 . . 175.60(10)
                           ?
    P1 Ag1 P2 . . 93.58(4) ?
    P1 Ag1 P3 . . 119.54(4) ?
    P1 Ag1 P4 . . 122.91(4) ?
    P2 Ag1 P3 . . 118.95(4) ?
    P2 Ag1 P4 . . 106.23(4) ?
    P3 Ag1 P4 . . 96.64(4) ?
    C29 P1 C23 . . 102.35(18) ?
    C29 P1 C35 . . 104.7(2) ?
    C23 P1 C35 . . 104.52(18) ?
    C29 P1 Ag1 . . 119.20(13) ?
    C23 P1 Ag1 . . 115.03(15) ?
    C35 P1 Ag1 . . 109.63(14) ?
    C44 P2 C38 . . 103.21(19) ?
    C44 P2 C37 . . 103.13(19) ?
    C38 P2 C37 . . 103.20(19) ?
    C44 P2 Ag1 . . 121.75(12) ?
    C38 P2 Ag1 . . 114.10(13) ?
    C37 P2 Ag1 . . 109.46(14) ?
    C65 P3 C71 . . 103.91(18) ?
    C65 P3 C64 . . 103.5(2) ?
    C71 P3 C64 . . 103.10(18) ?
    C65 P3 Ag1 . . 116.75(13) ?
    C71 P3 Ag1 . . 115.99(15) ?
    C64 P3 Ag1 . . 112.00(14) ?
    C56 P4 C50 . . 103.42(19) ?
    C56 P4 C62 . . 106.1(2) ?
    C50 P4 C62 . . 102.09(19) ?
    C56 P4 Ag1 . . 111.49(12) ?
    C50 P4 Ag1 . . 124.14(14) ?
    C62 P4 Ag1 . . 108.08(13) ?
    C19 O1 Sn1 . . 119.0(3) ?
    C21 O3 Sn1 . . 119.3(3) ?
    C2 C1 C6 . . 118.3(4) ?
    C2 C1 Sn1 . . 122.7(3) ?
    C6 C1 Sn1 . . 118.9(3) ?
    C1 C2 C3 . . 120.9(4) ?
    C1 C2 H2 . . 119.6 ?
    C3 C2 H2 . . 119.6 ?
    C4 C3 C2 . . 119.8(5) ?
    C4 C3 H3 . . 120.1 ?
    C2 C3 H3 . . 120.1 ?
    C5 C4 C3 . . 119.3(4) ?
    C5 C4 H4 . . 120.4 ?
    C3 C4 H4 . . 120.4 ?
    C6 C5 C4 . . 120.6(4) ?
    C6 C5 H5 . . 119.7 ?
    C4 C5 H5 . . 119.7 ?
    C5 C6 C1 . . 121.1(5) ?
    C5 C6 H6 . . 119.5 ?
    C1 C6 H6 . . 119.5 ?
    C12 C7 C8 . . 118.5(4) ?
    C12 C7 Sn1 . . 120.7(3) ?
    C8 C7 Sn1 . . 120.8(3) ?
    C7 C8 C9 . . 120.3(4) ?
    C7 C8 H8 . . 119.8 ?
    C9 C8 H8 . . 119.8 ?
    C10 C9 C8 . . 120.7(4) ?
    C10 C9 H9 . . 119.7 ?
    C8 C9 H9 . . 119.7 ?
    C9 C10 C11 . . 119.4(4) ?
    C9 C10 H10 . . 120.3 ?
    C11 C10 H10 . . 120.3 ?
    C10 C11 C12 . . 119.3(4) ?
    C10 C11 H11 . . 120.3 ?
    C12 C11 H11 . . 120.3 ?
    C7 C12 C11 . . 121.6(4) ?
    C7 C12 H12 . . 119.2 ?
    C11 C12 H12 . . 119.2 ?
    C14 C13 C18 . . 117.4(4) ?
    C14 C13 Sn1 . . 123.6(3) ?
    C18 C13 Sn1 . . 118.9(3) ?
    C15 C14 C13 . . 122.1(4) ?
    C15 C14 H14 . . 118.9 ?
    C13 C14 H14 . . 118.9 ?
    C16 C15 C14 . . 119.6(4) ?
    C16 C15 H15 . . 120.2 ?
    C14 C15 H15 . . 120.2 ?
    C15 C16 C17 . . 120.1(4) ?
    C15 C16 H16 . . 120.0 ?
    C17 C16 H16 . . 120.0 ?
    C16 C17 C18 . . 120.1(4) ?
    C16 C17 H17 . . 120.0 ?
    C18 C17 H17 . . 120.0 ?
    C17 C18 C13 . . 120.7(4) ?
    C17 C18 H18 . . 119.6 ?
    C13 C18 H18 . . 119.6 ?
    O2 C19 O1 . . 129.8(4) ?
    O2 C19 C20 . . 118.3(4) ?
    O1 C19 C20 . . 111.9(4) ?
    F1 C20 F2 . . 106.7(3) ?
    F1 C20 C19 . . 111.8(4) ?
    F2 C20 C19 . . 111.0(3) ?
    F1 C20 Cl1 . . 108.0(3) ?
    F2 C20 Cl1 . . 108.2(3) ?
    C19 C20 Cl1 . . 111.0(3) ?
    O4 C21 O3 . . 130.4(4) ?
    O4 C21 C22 . . 118.8(4) ?
    O3 C21 C22 . . 110.9(4) ?
    F3 C22 F4 . . 107.1(4) ?
    F3 C22 C21 . . 111.6(4) ?
    F4 C22 C21 . . 111.4(3) ?
    F3 C22 Cl2 . . 107.4(3) ?
    F4 C22 Cl2 . . 108.2(3) ?
    C21 C22 Cl2 . . 110.9(3) ?
    C24 C23 C28 . . 119.4(4) ?
    C24 C23 P1 . . 117.1(3) ?
    C28 C23 P1 . . 123.4(3) ?
    C25 C24 C23 . . 120.7(4) ?
    C25 C24 H24 . . 119.6 ?
    C23 C24 H24 . . 119.6 ?
    C24 C25 C26 . . 119.8(4) ?
    C24 C25 H25 . . 120.1 ?
    C26 C25 H25 . . 120.1 ?
    C27 C26 C25 . . 120.1(4) ?
    C27 C26 H26 . . 119.9 ?
    C25 C26 H26 . . 119.9 ?
    C26 C27 C28 . . 120.3(4) ?
    C26 C27 H27 . . 119.9 ?
    C28 C27 H27 . . 119.9 ?
    C27 C28 C23 . . 119.6(4) ?
    C27 C28 H28 . . 120.2 ?
    C23 C28 H28 . . 120.2 ?
    C30 C29 C34 . . 118.0(4) ?
    C30 C29 P1 . . 122.8(3) ?
    C34 C29 P1 . . 119.1(3) ?
    C31 C30 C29 . . 120.7(4) ?
    C31 C30 H30 . . 119.7 ?
    C29 C30 H30 . . 119.7 ?
    C32 C31 C30 . . 120.6(4) ?
    C32 C31 H31 . . 119.7 ?
    C30 C31 H31 . . 119.7 ?
    C31 C32 C33 . . 119.7(4) ?
    C31 C32 H32 . . 120.1 ?
    C33 C32 H32 . . 120.1 ?
    C34 C33 C32 . . 119.7(4) ?
    C34 C33 H33 . . 120.2 ?
    C32 C33 H33 . . 120.2 ?
    C33 C34 C29 . . 121.3(4) ?
    C33 C34 H34 . . 119.4 ?
    C29 C34 H34 . . 119.4 ?
    C36 C35 P1 . . 114.9(3) ?
    C36 C35 H35 . . 122.5 ?
    P1 C35 H35 . . 122.5 ?
    C37 C36 C35 . . 117.3(3) ?
    C37 C36 H36A . . 108.0 ?
    C35 C36 H36A . . 108.0 ?
    C37 C36 H36B . . 108.0 ?
    C35 C36 H36B . . 108.0 ?
    H36A C36 H36B . . 107.2 ?
    C36 C37 P2 . . 116.3(3) ?
    C36 C37 H37A . . 108.2 ?
    P2 C37 H37A . . 108.2 ?
    C36 C37 H37B . . 108.2 ?
    P2 C37 H37B . . 108.2 ?
    H37A C37 H37B . . 107.4 ?
    C39 C38 C43 . . 118.5(4) ?
    C39 C38 P2 . . 119.3(3) ?
    C43 C38 P2 . . 122.2(3) ?
    C38 C39 C40 . . 120.9(4) ?
    C38 C39 H39 . . 119.6 ?
    C40 C39 H39 . . 119.6 ?
    C41 C40 C39 . . 119.9(4) ?
    C41 C40 H40 . . 120.1 ?
    C39 C40 H40 . . 120.1 ?
    C40 C41 C42 . . 119.5(4) ?
    C40 C41 H41 . . 120.3 ?
    C42 C41 H41 . . 120.3 ?
    C43 C42 C41 . . 120.4(4) ?
    C43 C42 H42 . . 119.8 ?
    C41 C42 H42 . . 119.8 ?
    C42 C43 C38 . . 120.9(4) ?
    C42 C43 H43 . . 119.6 ?
    C38 C43 H43 . . 119.6 ?
    C45 C44 C49 . . 117.7(4) ?
    C45 C44 P2 . . 118.1(3) ?
    C49 C44 P2 . . 124.3(3) ?
    C44 C45 C46 . . 121.6(4) ?
    C44 C45 H45A . . 106.9 ?
    C46 C45 H45A . . 106.9 ?
    C44 C45 H45B . . 106.9 ?
    C46 C45 H45B . . 106.9 ?
    H45A C45 H45B . . 106.7 ?
    C47 C46 C45 . . 119.3(5) ?
    C47 C46 H46 . . 120.3 ?
    C45 C46 H46 . . 120.3 ?
    C48 C47 C46 . . 120.4(5) ?
    C48 C47 H47 . . 119.8 ?
    C46 C47 H47 . . 119.8 ?
    C47 C48 C49 . . 119.9(4) ?
    C47 C48 H48 . . 120.0 ?
    C49 C48 H48 . . 120.0 ?
    C48 C49 C44 . . 121.0(4) ?
    C48 C49 H49 . . 119.5 ?
    C44 C49 H49 . . 119.5 ?
    C55 C50 C51 . . 119.2(4) ?
    C55 C50 P4 . . 121.8(3) ?
    C51 C50 P4 . . 119.0(3) ?
    C52 C51 C50 . . 120.1(4) ?
    C52 C51 H51 . . 120.0 ?
    C50 C51 H51 . . 120.0 ?
    C53 C52 C51 . . 120.4(4) ?
    C53 C52 H52 . . 119.8 ?
    C51 C52 H52 . . 119.8 ?
    C52 C53 C54 . . 120.1(4) ?
    C52 C53 H53 . . 119.9 ?
    C54 C53 H53 . . 119.9 ?
    C53 C54 C55 . . 120.2(4) ?
    C53 C54 H54 . . 119.9 ?
    C55 C54 H54 . . 119.9 ?
    C50 C55 C54 . . 120.0(4) ?
    C50 C55 H55 . . 120.0 ?
    C54 C55 H55 . . 120.0 ?
    C61 C56 C57 . . 118.3(4) ?
    C61 C56 P4 . . 124.7(4) ?
    C57 C56 P4 . . 116.7(3) ?
    C58 C57 C56 . . 120.9(4) ?
    C58 C57 H57 . . 119.6 ?
    C56 C57 H57 . . 119.6 ?
    C57 C58 C59 . . 120.4(5) ?
    C57 C58 H58 . . 119.8 ?
    C59 C58 H58 . . 119.8 ?
    C60 C59 C58 . . 119.6(4) ?
    C60 C59 H59 . . 120.2 ?
    C58 C59 H59 . . 120.2 ?
    C59 C60 C61 . . 120.1(5) ?
    C59 C60 H60 . . 119.9 ?
    C61 C60 H60 . . 119.9 ?
    C56 C61 C60 . . 120.6(5) ?
    C56 C61 H61 . . 119.7 ?
    C60 C61 H61 . . 119.7 ?
    C63 C62 P4 . . 113.8(3) ?
    C63 C62 H62A . . 108.8 ?
    P4 C62 H62A . . 108.8 ?
    C63 C62 H62B . . 108.8 ?
    P4 C62 H62B . . 108.8 ?
    H62A C62 H62B . . 107.7 ?
    C64 C63 C62 . . 115.4(3) ?
    C64 C63 H63A . . 108.4 ?
    C62 C63 H63A . . 108.4 ?
    C64 C63 H63B . . 108.4 ?
    C62 C63 H63B . . 108.4 ?
    H63A C63 H63B . . 107.5 ?
    C63 C64 P3 . . 115.7(3) ?
    C63 C64 H64A . . 108.4 ?
    P3 C64 H64A . . 108.4 ?
    C63 C64 H64B . . 108.4 ?
    P3 C64 H64B . . 108.4 ?
    H64A C64 H64B . . 107.4 ?
    C70 C65 C66 . . 118.3(4) ?
    C70 C65 P3 . . 119.4(3) ?
    C66 C65 P3 . . 122.1(3) ?
    C65 C66 C67 . . 120.6(4) ?
    C65 C66 H66 . . 119.7 ?
    C67 C66 H66 . . 119.7 ?
    C68 C67 C66 . . 119.3(4) ?
    C68 C67 H67 . . 120.3 ?
    C66 C67 H67 . . 120.3 ?
    C67 C68 C69 . . 121.1(4) ?
    C67 C68 H68 . . 119.5 ?
    C69 C68 H68 . . 119.5 ?
    C70 C69 C68 . . 119.1(5) ?
    C70 C69 H69 . . 120.5 ?
    C68 C69 H69 . . 120.5 ?
    C65 C70 C69 . . 121.6(4) ?
    C65 C70 H70 . . 119.2 ?
    C69 C70 H70 . . 119.2 ?
    C76 C71 C72 . . 118.9(4) ?
    C76 C71 P3 . . 120.1(3) ?
    C72 C71 P3 . . 121.0(4) ?
    C73 C72 C71 . . 120.5(4) ?
    C73 C72 H72 . . 119.8 ?
    C71 C72 H72 . . 119.8 ?
    C72 C73 C74 . . 120.1(4) ?
    C72 C73 H73 . . 119.9 ?
    C74 C73 H73 . . 119.9 ?
    C75 C74 C73 . . 120.4(4) ?
    C75 C74 H74 . . 119.8 ?
    C73 C74 H74 . . 119.8 ?
    C74 C75 C76 . . 119.7(5) ?
    C74 C75 H75 . . 120.2 ?
    C76 C75 H75 . . 120.2 ?
    C71 C76 C75 . . 120.5(4) ?
    C71 C76 H76 . . 119.8 ?
    C75 C76 H76 . . 119.8 ?
loop_
    _geom_torsion_atom_site_label_1
    _geom_torsion_atom_site_label_2
    _geom_torsion_atom_site_label_3
    _geom_torsion_atom_site_label_4
    _geom_torsion_site_symmetry_1
    _geom_torsion_site_symmetry_2
    _geom_torsion_site_symmetry_3
    _geom_torsion_site_symmetry_4
    _geom_torsion
    _geom_torsion_publ_flag
    P3 Ag1 P1 C29 . . . . 75.36(15) ?
    P4 Ag1 P1 C29 . . . . -46.32(16) ?
    P2 Ag1 P1 C29 . . . . -158.28(15) ?
    P3 Ag1 P1 C23 . . . . -46.74(14) ?
    P4 Ag1 P1 C23 . . . . -168.42(14) ?
    P2 Ag1 P1 C23 . . . . 79.62(14) ?
    P3 Ag1 P1 C35 . . . . -164.15(14) ?
    P4 Ag1 P1 C35 . . . . 74.18(15) ?
    P2 Ag1 P1 C35 . . . . -37.79(15) ?
    P1 Ag1 P2 C44 . . . . 156.14(18) ?
    P3 Ag1 P2 C44 . . . . -77.05(18) ?
    P4 Ag1 P2 C44 . . . . 30.32(18) ?
    P1 Ag1 P2 C38 . . . . -79.03(17) ?
    P3 Ag1 P2 C38 . . . . 47.78(17) ?
    P4 Ag1 P2 C38 . . . . 155.16(16) ?
    P1 Ag1 P2 C37 . . . . 36.01(14) ?
    P3 Ag1 P2 C37 . . . . 162.82(14) ?
    P4 Ag1 P2 C37 . . . . -89.80(14) ?
    P1 Ag1 P3 C65 . . . . 81.93(16) ?
    P4 Ag1 P3 C65 . . . . -144.06(16) ?
    P2 Ag1 P3 C65 . . . . -31.36(16) ?
    P1 Ag1 P3 C71 . . . . -41.11(14) ?
    P4 Ag1 P3 C71 . . . . 92.90(14) ?
    P2 Ag1 P3 C71 . . . . -154.41(13) ?
    P1 Ag1 P3 C64 . . . . -159.07(15) ?
    P4 Ag1 P3 C64 . . . . -25.07(15) ?
    P2 Ag1 P3 C64 . . . . 87.63(15) ?
    P1 Ag1 P4 C56 . . . . -81.76(17) ?
    P3 Ag1 P4 C56 . . . . 146.44(17) ?
    P2 Ag1 P4 C56 . . . . 23.66(17) ?
    P1 Ag1 P4 C50 . . . . 42.89(17) ?
    P3 Ag1 P4 C50 . . . . -88.92(17) ?
    P2 Ag1 P4 C50 . . . . 148.30(17) ?
    P1 Ag1 P4 C62 . . . . 162.07(14) ?
    P3 Ag1 P4 C62 . . . . 30.26(14) ?
    P2 Ag1 P4 C62 . . . . -92.52(14) ?
    C13 Sn1 O1 C19 . . . . 50.2(3) ?
    C7 Sn1 O1 C19 . . . . -67.4(3) ?
    C1 Sn1 O1 C19 . . . . 177.8(3) ?
    C13 Sn1 O3 C21 . . . . 67.1(3) ?
    C7 Sn1 O3 C21 . . . . -175.4(3) ?
    C1 Sn1 O3 C21 . . . . -60.2(3) ?
    C13 Sn1 C1 C2 . . . . 42.7(4) ?
    C7 Sn1 C1 C2 . . . . -135.7(3) ?
    O3 Sn1 C1 C2 . . . . 137.3(3) ?
    O1 Sn1 C1 C2 . . . . -41.7(3) ?
    C13 Sn1 C1 C6 . . . . -139.8(3) ?
    C7 Sn1 C1 C6 . . . . 41.9(4) ?
    O3 Sn1 C1 C6 . . . . -45.1(3) ?
    O1 Sn1 C1 C6 . . . . 135.8(3) ?
    C6 C1 C2 C3 . . . . 0.7(6) ?
    Sn1 C1 C2 C3 . . . . 178.2(3) ?
    C1 C2 C3 C4 . . . . -1.2(7) ?
    C2 C3 C4 C5 . . . . 0.4(7) ?
    C3 C4 C5 C6 . . . . 0.8(7) ?
    C4 C5 C6 C1 . . . . -1.4(7) ?
    C2 C1 C6 C5 . . . . 0.6(6) ?
    Sn1 C1 C6 C5 . . . . -177.0(3) ?
    C13 Sn1 C7 C12 . . . . 61.2(4) ?
    C1 Sn1 C7 C12 . . . . -120.2(3) ?
    O3 Sn1 C7 C12 . . . . -30.8(3) ?
    O1 Sn1 C7 C12 . . . . 152.7(3) ?
    C13 Sn1 C7 C8 . . . . -119.6(3) ?
    C1 Sn1 C7 C8 . . . . 58.9(4) ?
    O3 Sn1 C7 C8 . . . . 148.3(3) ?
    O1 Sn1 C7 C8 . . . . -28.2(3) ?
    C12 C7 C8 C9 . . . . 1.6(6) ?
    Sn1 C7 C8 C9 . . . . -177.5(3) ?
    C7 C8 C9 C10 . . . . -3.3(7) ?
    C8 C9 C10 C11 . . . . 1.8(7) ?
    C9 C10 C11 C12 . . . . 1.2(7) ?
    C8 C7 C12 C11 . . . . 1.5(6) ?
    Sn1 C7 C12 C11 . . . . -179.4(3) ?
    C10 C11 C12 C7 . . . . -2.9(6) ?
    C7 Sn1 C13 C14 . . . . 168.2(3) ?
    C1 Sn1 C13 C14 . . . . -10.1(4) ?
    O3 Sn1 C13 C14 . . . . -103.6(4) ?
    O1 Sn1 C13 C14 . . . . 72.4(4) ?
    C7 Sn1 C13 C18 . . . . -8.4(4) ?
    C1 Sn1 C13 C18 . . . . 173.3(3) ?
    O3 Sn1 C13 C18 . . . . 79.9(4) ?
    O1 Sn1 C13 C18 . . . . -104.2(4) ?
    C18 C13 C14 C15 . . . . 0.6(7) ?
    Sn1 C13 C14 C15 . . . . -176.0(3) ?
    C13 C14 C15 C16 . . . . 0.7(7) ?
    C14 C15 C16 C17 . . . . -1.7(8) ?
    C15 C16 C17 C18 . . . . 1.3(8) ?
    C16 C17 C18 C13 . . . . 0.1(8) ?
    C14 C13 C18 C17 . . . . -1.0(7) ?
    Sn1 C13 C18 C17 . . . . 175.8(4) ?
    Sn1 O1 C19 O2 . . . . 29.7(6) ?
    Sn1 O1 C19 C20 . . . . -149.2(2) ?
    O2 C19 C20 F1 . . . . 6.8(5) ?
    O1 C19 C20 F1 . . . . -174.1(3) ?
    O2 C19 C20 F2 . . . . 125.8(4) ?
    O1 C19 C20 F2 . . . . -55.1(4) ?
    O2 C19 C20 Cl1 . . . . -113.8(4) ?
    O1 C19 C20 Cl1 . . . . 65.3(4) ?
    Sn1 O3 C21 O4 . . . . -9.4(6) ?
    Sn1 O3 C21 C22 . . . . 171.0(2) ?
    O4 C21 C22 F3 . . . . -4.1(6) ?
    O3 C21 C22 F3 . . . . 175.5(3) ?
    O4 C21 C22 F4 . . . . -123.8(4) ?
    O3 C21 C22 F4 . . . . 55.8(4) ?
    O4 C21 C22 Cl2 . . . . 115.6(4) ?
    O3 C21 C22 Cl2 . . . . -64.8(4) ?
    C29 P1 C23 C24 . . . . -85.8(4) ?
    C35 P1 C23 C24 . . . . 165.2(3) ?
    Ag1 P1 C23 C24 . . . . 45.0(4) ?
    C29 P1 C23 C28 . . . . 91.3(4) ?
    C35 P1 C23 C28 . . . . -17.7(4) ?
    Ag1 P1 C23 C28 . . . . -137.9(3) ?
    C28 C23 C24 C25 . . . . -0.5(7) ?
    P1 C23 C24 C25 . . . . 176.7(3) ?
    C23 C24 C25 C26 . . . . 0.9(7) ?
    C24 C25 C26 C27 . . . . 0.0(7) ?
    C25 C26 C27 C28 . . . . -1.3(7) ?
    C26 C27 C28 C23 . . . . 1.7(7) ?
    C24 C23 C28 C27 . . . . -0.8(6) ?
    P1 C23 C28 C27 . . . . -177.8(3) ?
    C23 P1 C29 C30 . . . . 1.2(4) ?
    C35 P1 C29 C30 . . . . 110.0(4) ?
    Ag1 P1 C29 C30 . . . . -127.0(3) ?
    C23 P1 C29 C34 . . . . 176.8(3) ?
    C35 P1 C29 C34 . . . . -74.3(4) ?
    Ag1 P1 C29 C34 . . . . 48.6(4) ?
    C34 C29 C30 C31 . . . . -0.3(6) ?
    P1 C29 C30 C31 . . . . 175.4(3) ?
    C29 C30 C31 C32 . . . . 1.8(7) ?
    C30 C31 C32 C33 . . . . -2.2(7) ?
    C31 C32 C33 C34 . . . . 1.1(7) ?
    C32 C33 C34 C29 . . . . 0.4(7) ?
    C30 C29 C34 C33 . . . . -0.8(6) ?
    P1 C29 C34 C33 . . . . -176.7(4) ?
    C29 P1 C35 C36 . . . . -172.0(3) ?
    C23 P1 C35 C36 . . . . -64.8(3) ?
    Ag1 P1 C35 C36 . . . . 59.0(3) ?
    P1 C35 C36 C37 . . . . -78.9(4) ?
    C35 C36 C37 P2 . . . . 77.1(4) ?
    C44 P2 C37 C36 . . . . 173.6(3) ?
    C38 P2 C37 C36 . . . . 66.4(3) ?
    Ag1 P2 C37 C36 . . . . -55.4(3) ?
    C44 P2 C38 C39 . . . . 145.2(4) ?
    C37 P2 C38 C39 . . . . -107.6(4) ?
    Ag1 P2 C38 C39 . . . . 11.0(4) ?
    C44 P2 C38 C43 . . . . -35.2(5) ?
    C37 P2 C38 C43 . . . . 71.9(4) ?
    Ag1 P2 C38 C43 . . . . -169.4(4) ?
    C43 C38 C39 C40 . . . . -1.0(7) ?
    P2 C38 C39 C40 . . . . 178.6(4) ?
    C38 C39 C40 C41 . . . . 1.9(7) ?
    C39 C40 C41 C42 . . . . -1.1(7) ?
    C40 C41 C42 C43 . . . . -0.5(8) ?
    C41 C42 C43 C38 . . . . 1.4(9) ?
    C39 C38 C43 C42 . . . . -0.7(8) ?
    P2 C38 C43 C42 . . . . 179.8(4) ?
    C38 P2 C44 C45 . . . . -71.1(3) ?
    C37 P2 C44 C45 . . . . -178.3(3) ?
    Ag1 P2 C44 C45 . . . . 58.6(3) ?
    C38 P2 C44 C49 . . . . 108.5(3) ?
    C37 P2 C44 C49 . . . . 1.3(3) ?
    Ag1 P2 C44 C49 . . . . -121.9(3) ?
    C49 C44 C45 C46 . . . . 0.1(2) ?
    P2 C44 C45 C46 . . . . 179.7(3) ?
    C44 C45 C46 C47 . . . . 0.2(3) ?
    C45 C46 C47 C48 . . . . -0.3(5) ?
    C46 C47 C48 C49 . . . . 0.2(6) ?
    C47 C48 C49 C44 . . . . 0.0(6) ?
    C45 C44 C49 C48 . . . . -0.2(4) ?
    P2 C44 C49 C48 . . . . -179.7(3) ?
    C56 P4 C50 C55 . . . . -27.5(4) ?
    C62 P4 C50 C55 . . . . 82.5(4) ?
    Ag1 P4 C50 C55 . . . . -155.6(3) ?
    C56 P4 C50 C51 . . . . 154.2(3) ?
    C62 P4 C50 C51 . . . . -95.8(4) ?
    Ag1 P4 C50 C51 . . . . 26.1(4) ?
    C55 C50 C51 C52 . . . . -1.3(6) ?
    P4 C50 C51 C52 . . . . 177.1(3) ?
    C50 C51 C52 C53 . . . . 0.9(7) ?
    C51 C52 C53 C54 . . . . -0.1(7) ?
    C52 C53 C54 C55 . . . . -0.4(7) ?
    C51 C50 C55 C54 . . . . 0.8(6) ?
    P4 C50 C55 C54 . . . . -177.5(3) ?
    C53 C54 C55 C50 . . . . 0.0(7) ?
    C50 P4 C56 C61 . . . . 112.9(4) ?
    C62 P4 C56 C61 . . . . 5.9(4) ?
    Ag1 P4 C56 C61 . . . . -111.5(3) ?
    C50 P4 C56 C57 . . . . -72.6(3) ?
    C62 P4 C56 C57 . . . . -179.7(3) ?
    Ag1 P4 C56 C57 . . . . 62.9(3) ?
    C61 C56 C57 C58 . . . . -1.1(6) ?
    P4 C56 C57 C58 . . . . -175.9(3) ?
    C56 C57 C58 C59 . . . . 1.5(7) ?
    C57 C58 C59 C60 . . . . -1.4(7) ?
    C58 C59 C60 C61 . . . . 0.8(7) ?
    C57 C56 C61 C60 . . . . 0.5(6) ?
    P4 C56 C61 C60 . . . . 174.9(3) ?
    C59 C60 C61 C56 . . . . -0.4(7) ?
    C56 P4 C62 C63 . . . . -178.9(3) ?
    C50 P4 C62 C63 . . . . 73.1(3) ?
    Ag1 P4 C62 C63 . . . . -59.2(3) ?
    P4 C62 C63 C64 . . . . 87.4(4) ?
    C62 C63 C64 P3 . . . . -77.9(4) ?
    C65 P3 C64 C63 . . . . 172.3(3) ?
    C71 P3 C64 C63 . . . . -79.7(3) ?
    Ag1 P3 C64 C63 . . . . 45.7(3) ?
    C71 P3 C65 C70 . . . . -159.1(3) ?
    C64 P3 C65 C70 . . . . -51.7(4) ?
    Ag1 P3 C65 C70 . . . . 71.8(4) ?
    C71 P3 C65 C66 . . . . 26.9(4) ?
    C64 P3 C65 C66 . . . . 134.3(3) ?
    Ag1 P3 C65 C66 . . . . -102.2(3) ?
    C70 C65 C66 C67 . . . . 1.6(6) ?
    P3 C65 C66 C67 . . . . 175.7(3) ?
    C65 C66 C67 C68 . . . . -1.4(7) ?
    C66 C67 C68 C69 . . . . 1.1(7) ?
    C67 C68 C69 C70 . . . . -1.0(7) ?
    C66 C65 C70 C69 . . . . -1.5(7) ?
    P3 C65 C70 C69 . . . . -175.8(4) ?
    C68 C69 C70 C65 . . . . 1.2(7) ?
    C65 P3 C71 C76 . . . . -129.0(3) ?
    C64 P3 C71 C76 . . . . 123.3(3) ?
    Ag1 P3 C71 C76 . . . . 0.6(3) ?
    C65 P3 C71 C72 . . . . 50.4(3) ?
    C64 P3 C71 C72 . . . . -57.3(4) ?
    Ag1 P3 C71 C72 . . . . 180.0(3) ?
    C76 C71 C72 C73 . . . . 0.5(6) ?
    P3 C71 C72 C73 . . . . -178.9(3) ?
    C71 C72 C73 C74 . . . . -1.5(6) ?
    C72 C73 C74 C75 . . . . 1.3(6) ?
    C73 C74 C75 C76 . . . . -0.2(6) ?
    C72 C71 C76 C75 . . . . 0.6(6) ?
    P3 C71 C76 C75 . . . . 180.0(3) ?
    C74 C75 C76 C71 . . . . -0.8(6) ?
